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公开(公告)号：US09291925B2
公开(公告)日：2016-03-22
申请号：US13790290
申请日：2013-03-08
Applicant: XEROX CORPORATION
Inventor： Yu Liu , Yulin Wang , Frank Ping-Hay Lee , Ke Zhou
CPC classification number: G03G9/0804 , C08J3/07 , C08K3/20 , C08K5/05 , C08K5/07
Abstract: A method for preparing a latex or dispersion, the method comprising contacting at least one resin with an organic solvent to form a resin mixture; neutralizing the resin mixture with a neutralizing agent; and subjecting the resin mixture flow to steam flow in a continuous manner to form a dispersion. A method for forming toner, the method comprising: contacting a resin to an organic solvent and a neutralizing agent to form a resin mixture; subjecting the resin mixture flow to a steam flow in a continuous manner to form a dispersion; aggregating particles from a pre-toner mixture, the pre-toner mixture comprising the dispersion, an optional colorant, and an optional wax; and coalescing the aggregated particles to form toner particles. An apparatus that can perform the methods.
Abstract translation: 一种制备胶乳或分散体的方法，所述方法包括使至少一种树脂与有机溶剂接触以形成树脂混合物; 用中和剂中和树脂混合物; 并使树脂混合物流以连续的方式进行蒸汽流以形成分散体。 一种形成调色剂的方法，所述方法包括：使树脂与有机溶剂和中和剂接触以形成树脂混合物; 使树脂混合物流以连续的方式进行蒸汽流以形成分散体; 从预调色剂混合物聚集颗粒，预调色剂混合物包含分散体，任选的着色剂和任选的蜡; 并聚集聚集的颗粒以形成调色剂颗粒。 可以执行方法的装置。
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52.发明申请公开(公告)号：US20160026100A1
公开(公告)日：2016-01-28
申请号：US14340321
申请日：2014-07-24
Applicant: XEROX CORPORATION
Inventor： Harry P Latchman , Ke Zhou , Frank Ping-Hay Lee
CPC classification number: G03G9/0802 , B02C17/005 , G03G9/0804
Abstract: A system for pigment milling includes a pulsing direct current (DC) source that generates a DC pulse, an electromagnetic field generating subunit that includes an electromagnetic coil coupled to the pulsing DC source to receive the DC pulse and to generate a magnetic field, and a rotating container subunit that includes a container for holding magnetic particles and ink pigment particles in an ink carrier, and a rotating subunit to rotate the container. A portion of the container is disposed within the electromagnetic coil and generation of the magnetic field causing motion of the magnetic particles thereby dispersing the ink pigment particles within the ink carrier.
Abstract translation: 用于颜料研磨的系统包括产生DC脉冲的脉冲直流（DC）源，包括耦合到脉冲DC源的电磁线圈以接收DC脉冲并产生磁场的电磁场产生子单元，以及 旋转容器子单元，其包括用于在墨载体中保持磁性颗粒和油墨颜料颗粒的容器和旋转的子单元以旋转容器。 容器的一部分设置在电磁线圈内并产生磁场，引起磁性颗粒的运动，从而将油墨颜料颗粒分散在墨载体内。
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公开(公告)号：US20150290651A1
公开(公告)日：2015-10-15
申请号：US14249162
申请日：2014-04-09
Applicant: Xerox Corporation
Inventor： Ke Zhou , David John William Lawton , Johan Junginger , Jun Zhao , Harry P. Latchman , Frank Ping-Hay Lee
CPC classification number: B02C17/005 , B02C19/18 , C01P2004/51 , C01P2004/62 , C09C3/041
Abstract: Pigment dispersions are prepared by including magnetic particles in a reaction mixture. When placed in an alternating current magnetic field, milling of pigment particles occurs in the reaction mixture.
Abstract translation: 通过将磁性颗粒包括在反应混合物中来制备颜料分散体。 当置于交流磁场中时，颜料颗粒的研磨发生在反应混合物中。
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公开(公告)号：US09069272B2
公开(公告)日：2015-06-30
申请号：US14077024
申请日：2013-11-11
Applicant: XEROX CORPORATION
Inventor： Jordan H. Wosnick , Ke Zhou , Valerie M. Farrugia , Kentaro Morimitsu , Edward G. Zwartz
CPC classification number: G03G9/0821 , G03G9/0806 , G03G9/08755 , G03G9/08759 , G03G9/08782 , G03G9/08797 , G03G9/09733
Abstract: An emulsion aggregation (EA) toner includes an amorphous polymeric resin, optionally a colorant, and a small molecule crystalline organic compound having molecular weight less than 1,000 g/mol and melting point less than the fusing temperature of the EA toner, wherein a mixture of the resin and the small molecule compound is characterized by a reduction in glass transition temperature from that of the resin and by the lack of a significant solid to liquid phase transition peak for the small molecule compound as determined by differential scanning calorimetry, the enthalpy of fusion for the small molecule compound in the mixture being measured to be less than 10% of the enthalpy of fusion of the compound in pure form. Furthermore, the EA toner may be configured to have a crease fix minimum fusing temperature (MFT) less than or equal to the crease fix MFT of a benchmark ultra-low-melt emulsion aggregation toner.
Abstract translation: 乳液聚集（EA）调色剂包括无定形聚合物树脂，任选的着色剂和分子量小于1,000g / mol且熔点低于EA调色剂的熔融温度的小分子结晶有机化合物，其中混合物 树脂和小分子化合物的特征在于玻璃化转变温度从树脂的降低以及通过差示扫描量热法测定的小分子化合物的显着固体与液相转变峰的缺乏，熔融焓 因为被测量的混合物中的小分子化合物的含量小于纯化合物的熔融焓的10％。 此外，EA调色剂可以被配置为具有小于或等于基准超低熔点乳液聚集调色剂的折痕固定MFT的折痕固定最小定影温度（MFT）。
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公开(公告)号：US09068041B2
公开(公告)日：2015-06-30
申请号：US13718535
申请日：2012-12-18
Applicant: Xerox Corporation
Inventor： Valerie M Farrugia , Guerino G Sacripante , Ke Zhou , Sonja Hadzidedic
IPC: C08G63/48 , C08G63/181 , G03G9/087 , G03G9/093 , G03G9/08
CPC classification number: C08G63/181 , G03G9/0819 , G03G9/0827 , G03G9/08755 , G03G9/08795 , G03G9/08797 , G03G9/09371
Abstract: Methods of making a bio-based polyester resin by polycondensing a polyol with a polyacidic furan are described. The polyol can be a rosin diol obtained by reacting a rosin acid and a glycerol carbonate. The polyacidic furan is obtained from a bio-based product. The resin may be used in manufacturing toner for imaging devices.
Abstract translation: 描述了通过将多元醇与多酸呋喃缩聚制备生物基聚酯树脂的方法。 多元醇可以是松香酸和甘油碳酸酯反应得到的松香二醇。 多酸呋喃是从生物基产物获得的。 树脂可用于制造用于成像装置的调色剂。
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Patent Agency Ranking
公开(公告)号：US09034546B1
公开(公告)日：2015-05-19
申请号：US14076712
申请日：2013-11-11
Applicant: Xerox Corporation
Inventor： Jordan H. Wosnick , Ke Zhou , Kentaro Morimitsu , Michael S. Hawkins , Edward G. Zwartz , Valerie M. Farrugia
CPC classification number: G03G9/09741 , G03G9/0804 , G03G9/08795 , G03G9/08797 , G03G9/09775
Abstract: A toner includes a polymeric resin, optionally a colorant, and a small molecule crystalline imide having a molecular weight less than 1,000 g/mol. The polymeric resin may be an amorphous resin and a mixture of the amorphous resin and the crystalline imide may be characterized by a reduction in glass transition temperature from that of the resin and by the lack of a melting point for the crystalline imide as determined by differential scanning calorimetry, the enthalpy of fusion for the crystalline imide in the mixture being measured to be less than 10% of the enthalpy of fusion of the crystalline imide in pure form. Furthermore, the toner may be configured to have a crease fix minimum fusing temperature (MFT) less than or equal to the crease fix MFT of a benchmark ultra-low-melt emulsion aggregation toner. Suitable crystalline imides may include N-alkyl and N-aryl imides, such as N-benzylphthalimide.
Abstract translation: 调色剂包括聚合物树脂，任选的着色剂和分子量小于1,000g / mol的小分子结晶酰亚胺。 聚合物树脂可以是无定形树脂，并且无定形树脂和结晶酰亚胺的混合物的特征在于玻璃化转变温度从树脂的温度降低，并且结晶酰亚胺的熔点缺乏由差分测定 扫描量热法测定混合物中结晶酰亚胺的熔融焓低于纯形式的结晶酰亚胺熔融焓的10％。 此外，调色剂可以被配置为具有小于或等于基准超低熔点乳液聚集调色剂的折痕固定MFT的折痕固定最小定影温度（MFT）。 合适的结晶酰亚胺可以包括N-烷基和N-芳基酰亚胺，例如N-苄基邻苯二甲酰亚胺。
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公开(公告)号：US20150132692A1
公开(公告)日：2015-05-14
申请号：US14076712
申请日：2013-11-11
Applicant: XEROX CORPORATION
Inventor： JORDAN H. WOSNICK , Ke Zhou , Kentaro Morimitsu , Michael S. Hawkins , Edward G. Zwartz , Valerie M. Farrugia
IPC: G03G9/08
CPC classification number: G03G9/09741 , G03G9/0804 , G03G9/08795 , G03G9/08797 , G03G9/09775
Abstract: A toner includes a polymeric resin, optionally a colorant, and a small molecule crystalline imide having a molecular weight less than 1,000 g/mol. The polymeric resin may be an amorphous resin and a mixture of the amorphous resin and the crystalline imide may be characterized by a reduction in glass transition temperature from that of the resin and by the lack of a melting point for the crystalline imide as determined by differential scanning calorimetry, the enthalpy of fusion for the crystalline imide in the mixture being measured to be less than 10% of the enthalpy of fusion of the crystalline imide in pure form. Furthermore, the toner may be configured to have a crease fix minimum fusing temperature (MFT) less than or equal to the crease fix MFT of a benchmark ultra-low-melt emulsion aggregation toner. Suitable crystalline imides may include N-alkyl and N-aryl imides, such as N-benzylphthalimide.
Abstract translation: 调色剂包括聚合物树脂，任选的着色剂和分子量小于1,000g / mol的小分子结晶酰亚胺。 聚合物树脂可以是无定形树脂，并且无定形树脂和结晶酰亚胺的混合物的特征在于玻璃化转变温度从树脂的温度降低，并且结晶酰亚胺的熔点缺乏由差分测定 扫描量热法测定混合物中结晶酰亚胺的熔融焓低于纯形式的结晶酰亚胺熔融焓的10％。 此外，调色剂可以被配置为具有小于或等于基准超低熔点乳液聚集调色剂的折痕固定MFT的折痕固定最小定影温度（MFT）。 合适的结晶酰亚胺可以包括N-烷基和N-芳基酰亚胺，例如N-苄基邻苯二甲酰亚胺。
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58.发明申请LATEX FORMING PROCESS COMPRISING CONCURRENT STEAM INJECTION EMULSIFICATION AND SOLVENT DISTILLATION 审中-公开包含相关蒸汽注射模拟和溶剂蒸馏的成型过程公开(公告)号：US20150086922A1
公开(公告)日：2015-03-26
申请号：US14035639
申请日：2013-09-24
Applicant: XEROX CORPORATION
Inventor： Yu Liu , Yulin Wang , Ke Zhou , Frank Ping-Hay Lee , Marko Saban , Shigang Qiu , Sonja Hadzidedic
CPC classification number: G03G9/0804 , G03G9/08755 , G03G9/08795 , G03G9/08797
Abstract: A process includes dissolving a polymer in an organic solvent to form a polymer solution and forming a latex from the polymer solution by contacting the polymer solution with steam while substantially simultaneously distilling the organic solvent.
Abstract translation: 一种方法包括将聚合物溶解在有机溶剂中以形成聚合物溶液，并通过使聚合物溶液与蒸汽接触而形成胶乳，同时基本上同时蒸馏有机溶剂。
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59.发明授权公开(公告)号：US08871420B1
公开(公告)日：2014-10-28
申请号：US13860474
申请日：2013-04-10
Applicant: Xerox Corporation
Inventor： Yu Liu , Ke Zhou , Yulin Wang , Frank Ping-Hay Lee
CPC classification number: B01F13/0809 , B01F13/0052 , B01F13/0818 , C08K5/05 , C08K5/07
Abstract: A method and system for magnetic actuated mixing which use magnetic particles and magnetic field to facilitate the mixing for preparing latex emulsion. In embodiments, a suitable process includes dissolving a resin in an organic solvent, optionally adding a surfactant, adding a neutralization agent and water, adding magnetic particles, and subjecting the mixture to a magnetic actuated mixing to form a latex emulsion. In embodiments, the latex emulsion thus produced may be utilized to form a toner.
Abstract translation: 一种用于磁致动混合的方法和系统，其使用磁性颗粒和磁场来促进混合以制备胶乳乳液。 在实施方案中，合适的方法包括将树脂溶解在有机溶剂中，任选地加入表面活性剂，加入中和剂和水，加入磁性颗粒，并使混合物进行磁致动混合以形成胶乳乳液。 在实施方案中，如此制备的胶乳乳液可用于形成调色剂。
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公开(公告)号：US20140200298A1
公开(公告)日：2014-07-17
申请号：US13741278
申请日：2013-01-14
Applicant: XEROX CORPORATION
Inventor： YU LIU , Yulin Wang , Frank Ping-Hay Lee , Ke Zhou , Shigang S. Qiu
Abstract: Processes for making toners, and in particular, emulsion aggregation (EA) toners. These toners exhibit a low melt temperature while simultaneously exhibiting excellent relative humidity sensitivity regarding charging properties. In embodiments, the process comprises the preparation of the latex emulsion comprising high ratio resin compositions by injection of steam and neutralization agent vapors into the latex emulsion.
Abstract translation: 制造调色剂的方法，特别是乳液聚集（EA）调色剂。 这些调色剂表现出低的熔融温度，同时对充电性能表现出优异的相对湿度敏感度。 在实施方案中，该方法包括通过将蒸汽和中和剂蒸气注入胶乳乳液中制备包含高比例树脂组合物的胶乳乳液。
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