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    Process for preparing (meth)acrolein by heterogeneously catalyzed gas phase partial oxidation
    61.
    发明授权
    Process for preparing (meth)acrolein by heterogeneously catalyzed gas phase partial oxidation 失效
    通过非均相催化气相部分氧化制备（甲基）丙烯醛的方法

    公开(公告)号：US08399711B2

    公开(公告)日：2013-03-19

    申请号：US12954770

    申请日：2010-11-26

    Applicant: Josef Macht ,  Andreas Raichle ,  Klaus Joachim Mueller-Engel ,  Ulrich Hammon

    Inventor： Josef Macht ,  Andreas Raichle ,  Klaus Joachim Mueller-Engel ,  Ulrich Hammon

    IPC: C07C45/35

    CPC classification number: B01J23/002 ,  B01J23/8885 ,  B01J35/023 ,  B01J37/04 ,  B01J37/08 ,  B01J2523/00 ,  C07C45/35 ,  C07C47/22 ,  B01J2523/13 ,  B01J2523/41 ,  B01J2523/54 ,  B01J2523/68 ,  B01J2523/69 ,  B01J2523/842 ,  B01J2523/845

    Abstract: A process for preparing (meth)acrolein by heterogeneously catalyzed gas phase partial oxidation of a precursor compound, in which the reaction gas mixture which comprises at least 3% by volume of precursor compound is passed through a fresh fixed catalyst bed whose active material is a multielement oxide which comprises the elements Mo, Fe and Bi and at least one of the elements Ni and Co, and the fixed catalyst bed is loaded with at least 40 l (STP)/l·h of precursor compound, and the precursor compound is converted to an extent of at least 90 mol %, wherein, over the first 8000 operating hours, during X=10 to 500 operating hours, the highest temperature of the reaction gas mixture in the fixed catalyst bed is 400 to 450° C. and, during the remaining 8000−X operating hours, is 300 to

    Abstract translation: 通过前体化合物的非均相催化气相部分氧化制备（甲基）丙烯醛的方法，其中将包含至少3体积％的前体化合物的反应气体混合物通过新鲜的固定催化剂床，活性材料为 包含元素Mo，Fe和Bi以及元素Ni和Co中的至少一种和固定催化剂床的多元素氧化物装载至少40μl（STP）/ l·h的前体化合物，前体化合物是 转化为至少90摩尔％的程度，其中，在第一个8000个工作小时内，在X = 10至500个操作小时期间，固定催化剂床中的反应气体混合物的最高温度为400至450℃， 在剩余的8000-X工作时间内，为300至<400℃，并且在X = 10至500个工作小时的时间内，平均有机前体化合物的固定催化剂床的负载大于 8000-X营业时间。

    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation
    62.
    发明授权
    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation 有权
    通过非均相催化气相部分氧化制备至少一种有机靶化合物的方法

    公开(公告)号：US08394345B2

    公开(公告)日：2013-03-12

    申请号：US12146807

    申请日：2008-06-26

    Applicant: Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    Inventor： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    IPC: B01J8/10

    CPC classification number: C07C51/252 ,  C07C57/04

    Abstract: A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalysts charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line.

    Abstract translation: 通过在两个平行操作的氧化反应器管线中的有机前体化合物与分子氧的非均相催化气相部分氧化来制备有机靶化合物的方法，并且从处理线中的产物气流的混合物中除去目标化合物， 其中氧化线之一的催化剂装料包括一部分催化剂，其上已经进行非均相催化的气相部分氧化比在另一个氧化反应器管线的催化剂装料的催化剂的部分长。

    PROCESS FOR PREPARING (METH)ACROLEIN BY HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION
    63.
    发明申请
    PROCESS FOR PREPARING (METH)ACROLEIN BY HETEROGENEOUSLY CATALYZED GAS PHASE PARTIAL OXIDATION 失效
    通过异源催化气相部分氧化制备（甲基）丙烯酸的方法

    公开(公告)号：US20110130596A1

    公开(公告)日：2011-06-02

    申请号：US12954770

    申请日：2010-11-26

    Applicant: Josef MACHT ,  Andreas Raichle ,  Klaus Joachim Müller-Engel ,  Ulrich Hammon

    Inventor： Josef MACHT ,  Andreas Raichle ,  Klaus Joachim Müller-Engel ,  Ulrich Hammon

    IPC: C07C45/35

    CPC classification number: B01J23/002 ,  B01J23/8885 ,  B01J35/023 ,  B01J37/04 ,  B01J37/08 ,  B01J2523/00 ,  C07C45/35 ,  C07C47/22 ,  B01J2523/13 ,  B01J2523/41 ,  B01J2523/54 ,  B01J2523/68 ,  B01J2523/69 ,  B01J2523/842 ,  B01J2523/845

    Abstract: A process for preparing (meth)acrolein by heterogeneously catalyzed gas phase partial oxidation of a precursor compound, in which the reaction gas mixture which comprises at least 3% by volume of precursor compound is passed through a fresh fixed catalyst bed whose active material is a multielement oxide which comprises the elements Mo, Fe and Bi and at least one of the elements Ni and Co, and the fixed catalyst bed is loaded with at least 40 l (STP)/l·h of precursor compound, and the precursor compound is converted to an extent of at least 90 mol %, wherein, over the first 8000 operating hours, during X=10 to 500 operating hours, the highest temperature of the reaction gas mixture in the fixed catalyst bed is 400 to 450° C. and, during the remaining 8000−X operating hours, is 300 to

    Abstract translation: 通过前体化合物的非均相催化气相部分氧化制备（甲基）丙烯醛的方法，其中将包含至少3体积％的前体化合物的反应气体混合物通过新鲜的固定催化剂床，活性材料为 包含元素Mo，Fe和Bi以及元素Ni和Co中的至少一种和固定催化剂床的多元素氧化物装载至少40μl（STP）/ l·h的前体化合物，前体化合物是 转化为至少90摩尔％的程度，其中，在第一个8000个工作小时内，在X = 10至500个操作小时期间，固定催化剂床中的反应气体混合物的最高温度为400至450℃， 在剩余的8000-X工作时间内，为300至<400℃，并且在X = 10至500个工作小时的时间内，平均有机前体化合物的固定催化剂床的负载大于 8000-X营业时间。

    Method for the rectifying separation of fluids containing (meth)acryl monomers
    67.
    发明授权
    Method for the rectifying separation of fluids containing (meth)acryl monomers 有权
    含有（甲基）丙烯酸单体的流体的精馏分离方法

    公开(公告)号：US07520964B2

    公开(公告)日：2009-04-21

    申请号：US10515639

    申请日：2003-07-02

    Applicant: Ulrich Hammon ,  Joachim Thiel ,  Volker Schliephake ,  Juergen Schroeder

    Inventor： Ulrich Hammon ,  Joachim Thiel ,  Volker Schliephake ,  Juergen Schroeder

    IPC: B01D3/22 ,  B01D3/32

    CPC classification number: B01D3/22 ,  B01D3/225 ,  C07C51/44 ,  Y10S203/11 ,  Y10S203/22 ,  C07C57/04

    Abstract: A process for rectificatively separating at least one (meth)acrylic monomer-containing fluid by feeding the fluid into a rectification column containing at least one sieve tray without a runoff segment, wherein an elementary cell is obtained from a number of centers of passages in a sieve tray, and the cell shifts regularly and repeatedly along its edges, the lengths of two shifting vectors being the lengths of the edges of the cell along which the shifting is effected; an arrangement of the centers is such that the positions of an ideal center and a real center are separated by ≦1% of half of the sum of the lengths of the two shifting vectors; and an arrangement of the passages is such that the sum of non-overlapping surface areas of an ideal passage with a real passage and vice versa is ≦1% of the surface area of the ideal passage.

    Abstract translation: 将含有至少一种（甲基）丙烯酸系单体的流体通过将流体供给至含有至少一个不具有径流段的多孔塔的精馏塔的方法，其中从多个通道中心获得基本单元， 筛板，并且单元沿其边缘规则地且重复地移动，两个移动向量的长度是实现移位的单元的边缘的长度; 中心的布置使得理想中心和实心的位置被两个移位矢量的长度之和的一半的<= 1％分开; 并且通道的布置使得理想通道的非重叠表面面积与实际通道的总和相反，<=理想通道的表面积的1％。

    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation
    69.
    发明授权
    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation 有权
    通过非均相催化气相部分氧化制备至少一种有机靶化合物的方法

    公开(公告)号：US07439389B2

    公开(公告)日：2008-10-21

    申请号：US11357300

    申请日：2006-02-21

    Applicant: Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    Inventor： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    IPC: C07C51/16 ,  C07C69/52

    CPC classification number: C07C51/252 ,  C07C57/04

    Abstract: A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalyst charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line.

    Abstract translation: 通过在两个平行操作的氧化反应器管线中的有机前体化合物与分子氧的非均相催化气相部分氧化来制备有机靶化合物的方法，并且从处理线中的产物气流的混合物中除去目标化合物， 其中一个氧化线的催化剂装料包括催化剂的一部分，在该部分的催化剂上已经进行非均相催化的气相部分氧化比在另一个氧化反应器管线的催化剂装料的催化剂部分上的时间长。

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