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1.发明申请PROCESS FOR REMOVAL OF ACRYLIC ACID FROM THE PRODUCT GAS MIXTURE OF A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF AT LEAST ONE C3 PRECURSOR COMPOUND 审中-公开从产品中除去丙烯酸的方法异氰酸酯化合物的异构催化部分气相氧化的气体混合物公开(公告)号：US20110036704A1
公开(公告)日：2011-02-17
申请号：US12827161
申请日：2010-06-30
申请人： Till BLUM , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jäger , Volker Schliephake , Klaus Joachim Müller-Engel , Ulrich Hammon , Frank Höfer
发明人： Till BLUM , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jäger , Volker Schliephake , Klaus Joachim Müller-Engel , Ulrich Hammon , Frank Höfer
CPC分类号： C07C51/252 , C07C51/44 , C07C57/04
摘要： A process for removal of a crude acrylic acid from a product gas mixture which comprises glyoxal as a by-product from a heterogeneously catalyzed partial gas phase oxidation of at least one C3 precursor compound, which comprises the absorption of the acrylic acid in a high-boiling absorbent and the rectificative workup of the resulting adsorbate, and in which absorbent present in the bottoms liquid withdrawn from the bottom space of the absorption column is distilled off in a distillation unit and recycled into the absorption, before high boilers which remain are discharged, and in which the glyoxal content of the crude acrylic acid is reduced by restricting the high boiler residence time in the distillation unit.
摘要翻译： 一种从产物气体混合物中除去粗丙烯酸的方法，该产物气体混合物包含乙二醛作为副产物从至少一种C3前体化合物的非均相催化的部分气相氧化，其包括丙烯酸在高温下的吸收， 沸腾的吸收剂和所得到的被吸附物的整理处理，其中存在于从吸收塔的底部空间排出的底部液体中的吸收剂在蒸馏单元中被蒸馏除去，并在剩余的高锅炉排出之前再循环到吸收中， 并且其中粗丙烯酸的乙二醛含量通过限制在蒸馏单元中的高锅炉停留时间而降低。
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2.发明申请PROCESS FOR SEPARATING ACRYLIC ACID PRESENT AS A MAIN CONSTITUENT AND GLYOXAL PRESENT AS A BY-PRODUCT IN A PRODUCT GAS MIXTURE OF A PARTIAL HETEROGENEOUSLY CATALYZED GAS PHASE OXIDATION OF A C3 PRECURSOR COMPOUND OF ACRYLIC ACID 有权分离出丙烯酸的方法作为主要成分和GLYOXAL存在作为产物中的副产物部分异构催化的气相混合丙烯酸C3前体化合物的气相氧化公开(公告)号：US20100022734A1
公开(公告)日：2010-01-28
申请号：US12509078
申请日：2009-07-24
申请人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jäger , Volker Schliephake , Klaus Joachim Müller-Engel , Ulrich Hammon , Jörg Heilek , Imke Britta Müller
发明人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jäger , Volker Schliephake , Klaus Joachim Müller-Engel , Ulrich Hammon , Jörg Heilek , Imke Britta Müller
CPC分类号： C07C51/252 , C07C51/43 , C07C57/04
摘要： A process for separating acrylic acid present as a main product and glyoxal present as a by-product in a product gas mixture of a partial gas phase oxidation of a C3 precursor compound, in which a liquid phase P is obtained, which consists of acrylic acid to an extent of at least 70% of its weight and, based on the molar amount of acrylic acid present therein, comprises at least 200 molar ppm of glyoxal, in which the glyoxal is separated from the acrylic acid in the liquid phase P by crystallization.
摘要翻译： 将作为主要成分存在的丙烯酸和作为副产物存在的乙二醛的方法分离在得到液相P的C3前体化合物的部分气相氧化的产物气体混合物中，该混合物由丙烯酸 至少其重量的70％的程度，并且基于其中存在的丙烯酸的摩尔量，包含至少200摩尔ppm的乙二醛，其中通过结晶将乙二醛与液相P中的丙烯酸分离 。
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3.发明授权Process for separating acrylic acid present as a main constituent and glyoxal present as a by-product in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a C3 precursor compound of acrylic acid 有权用于分离作为主要成分存在的丙烯酸和乙二醛作为副产物存在于丙烯酸的C3前体化合物的部分非均相催化气相氧化的产物气体混合物中公开(公告)号：US08299299B2
公开(公告)日：2012-10-30
申请号：US12509078
申请日：2009-07-24
申请人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
发明人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
IPC分类号： C07C51/42
CPC分类号： C07C51/252 , C07C51/43 , C07C57/04
摘要： A process for separating acrylic acid present as a main product and glyoxal present as a by-product in a product gas mixture of a partial gas phase oxidation of a C3 precursor compound, in which a liquid phase P is obtained, which consists of acrylic acid to an extent of at least 70% of its weight and, based on the molar amount of acrylic acid present therein, comprises at least 200 molar ppm of glyoxal, in which the glyoxal is separated from the acrylic acid in the liquid phase P by crystallization.
摘要翻译： 将作为主要成分存在的丙烯酸和作为副产物存在的乙二醛的方法分离在得到液相P的C3前体化合物的部分气相氧化的产物气体混合物中，该混合物由丙烯酸 至少其重量的70％的程度，并且基于其中存在的丙烯酸的摩尔量，包含至少200摩尔ppm的乙二醛，其中通过结晶将乙二醛与液相P中的丙烯酸分离 。
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4.发明申请METHOD OF CHARGING CATALYST TUBES OF A BUNDLE OF CATALYST TUBES IN A STRUCTURED FASHION 审中-公开在结构化时装中的催化剂管的填充催化剂管的方法公开(公告)号：US20100197489A1
公开(公告)日：2010-08-05
申请号：US12756424
申请日：2010-04-08
CPC分类号： B01J8/0015 , B01J8/003 , B01J8/06 , B01J8/067 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/026 , B01J2208/00212 , B01J2208/00752 , B01J2208/00814 , B01J2208/025 , B01J2523/00 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion, in which uniformly predispensed portions of formulations of shaped catalyst bodies are used for producing a section of charge.
摘要翻译： 一种以结构方式装载一束催化剂管的催化剂管的方法，其中使用成形催化剂体的制剂的均匀预分配部分来产生一部分电荷。
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5.发明授权Safe operation of a continuous heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound 有权至少一种有机化合物的连续不均匀催化气相部分氧化的安全操作公开(公告)号：US07074955B2
公开(公告)日：2006-07-11
申请号：US10459782
申请日：2003-06-12
申请人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
发明人： Ulrich Hammon , Jochen Meschke , Ulrich Rauh , Klaus Joachim Müller-Engel , Peter Schlemmer , Volker Schliephake
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , C07C45/33 , C07C45/34 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A continuously operated heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound in an oxidation reactor is operated safely by a process in which an explosion diagram for the feed gas mixture is deposited as the basis of a cut-out mechanism in a computer.
摘要翻译： 在氧化反应器中连续操作的至少一种有机化合物的气相部分氧化被安全地通过其中沉积原料气体混合物的爆炸图作为计算机中的切断机构的基础的方法来操作 。
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6.发明授权Preparation of at least one organic compound by heterogeneously catalyzed partial gas-phase oxidation 有权通过非均相催化的部分气相氧化制备至少一种有机化合物公开(公告)号：US06958414B2
公开(公告)日：2005-10-25
申请号：US10667782
申请日：2003-09-23
申请人： Volker Schliephake , Ulrich Hammon , Ernst Lang , Carl-Ludwig Krüger , Jürgen Schröder , Klaus Joachim Müller-Engel
发明人： Volker Schliephake , Ulrich Hammon , Ernst Lang , Carl-Ludwig Krüger , Jürgen Schröder , Klaus Joachim Müller-Engel
IPC分类号： C07C51/25 , C07C253/26 , C07C255/08 , C07C51/16
CPC分类号： C07C253/26 , C07C51/252 , C07C57/04 , C07C255/08
摘要： Organic compounds are prepared by heterogeneously catalyzed partial gas-phase oxidation of precursor compounds by a process in which a portion of the reaction gas starting mixture is brought from a low initial pressure to a higher final pressure by means of a radial compressor.
摘要翻译： 通过使反应气体起始混合物的一部分通过径向压缩机从低初始压力升至较高的最终压力的方法，通过异构催化的前体化合物的部分气相氧化来制备有机化合物。
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7.发明授权Process for transporting in the tank of a tank truck or tanker ship a liquid monomer phase withdrawn from a storage vessel 有权在罐车或油罐车的罐中运输的过程是从储存容器中取出的液体单体相公开(公告)号：US08829134B2
公开(公告)日：2014-09-09
申请号：US12053158
申请日：2008-03-21
IPC分类号： C08F2/00 , B01D37/00 , C07C67/56 , C07C67/62 , C07C51/42 , C07C51/47 , C07C45/78 , C07C45/79 , C07C51/50
CPC分类号： C07C45/79 , C07C45/78 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , C07C67/62 , C07C47/22 , C07C57/04 , C07C69/54
摘要： A process for transporting a liquid monomer phase which has been withdrawn from a storage vessel and comprises methacrylic monomers to an extent of ≧90% by weight, in a tank truck or in a tanker ship, in which the liquid monomer phase is subjected to a separating operation on the route from the storage vessel into the tank of a tank truck or of a tanker ship in order to separate polymer of the monomer present in dissolved form in the liquid monomer phase.
摘要翻译： 一种运输液体单体相的方法，所述液体单体相已经从储存容器中取出并且包含甲基丙烯酸类单体至≥90重量％的程度，在油罐车或油罐船中，其中液体单体相经受 在从储存容器进入罐车或油罐船的罐的路线上分离操作，以将以溶解形式存在的单体的聚合物分离在液体单体相中。
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8.发明授权Process for storing a monomer phase which is liquid under the conditions of storage 有权在储存条件下储存液体的单体相的方法公开(公告)号：US07893178B2
公开(公告)日：2011-02-22
申请号：US12053268
申请日：2008-03-21
IPC分类号： C08F16/34 , C08F20/06 , C08F118/02 , F16K49/00 , F17D1/16 , F04B49/10 , F04B49/00 , C07C45/00 , C07C69/52 , C07C57/02
CPC分类号： C07C67/48 , C07C45/79 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , Y10T137/0391 , Y10T137/6579 , C07C57/04 , C07C69/54 , C07C47/22
摘要： A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed.
摘要翻译： 一种在储存条件下储存液体的单体相的方法，其包含甲基丙烯酸单体至95重量％的程度，并且通过在气相中冷凝或通过熔化结晶相获得，在储存容器 其中在从其产生到储存容器中的途径中，其中以液态单体相中溶解形式存在的单体的聚合物被从其中除去，以及从存在容器中的单体的聚合物的储存容器中取出液体单体相的方法 在单体相中溶解形式同样被除去。
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9.发明申请PROCESS FOR TRANSPORTING IN THE TANK OF A TANK TRUCK OR TANKER SHIP A LIQUID MONOMER PHASE WITHDRAWN FROM A STORAGE VESSEL 有权运输在坦克卡车或坦克的油罐的过程从储存船运送液体单体相公开(公告)号：US20080234446A1
公开(公告)日：2008-09-25
申请号：US12053158
申请日：2008-03-21
CPC分类号： C07C45/79 , C07C45/78 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , C07C67/62 , C07C47/22 , C07C57/04 , C07C69/54
摘要： A process for transporting a liquid monomer phase which has been withdrawn from a storage vessel and comprises methacrylic monomers to an extent of ≧90% by weight, in a tank truck or in a tanker ship, in which the liquid monomer phase is subjected to a separating operation on the route from the storage vessel into the tank of a tank truck or of a tanker ship in order to separate polymer of the monomer present in dissolved form in the liquid monomer phase.
摘要翻译： 运输液体单体相的方法，该液体单体相已经从储存容器中取出并且包含甲基丙烯酸单体至> 90重量％的程度，在油罐车或油罐船中，其中液体单体相经受 在从储存容器进入罐车或油罐船的罐的路线上的分离操作，以分离以溶解形式存在于液体单体相中的单体的聚合物。
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10.发明申请PROCESS FOR STORING A MONOMER PHASE WHICH IS LIQUID UNDER THE CONDITIONS OF STORAGE 有权存储根据存储条件液化的单体相的过程公开(公告)号：US20090221780A1
公开(公告)日：2009-09-03
申请号：US12053268
申请日：2008-03-21
CPC分类号： C07C67/48 , C07C45/79 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , Y10T137/0391 , Y10T137/6579 , C07C57/04 , C07C69/54 , C07C47/22
摘要： A process for storing a monomer phase which is liquid under the conditions of storage and comprises methacrylic monomers to an extent of ≧95% by weight and has been obtained by condensation out of a gaseous phase or by melting a crystalline phase, in a storage vessel, in which polymer of the monomer present in dissolved form in the liquid monomer phase is removed therefrom on the route from its generation into the storage vessel, and also a process for withdrawing liquid monomer phase from the storage vessel in which polymer of the monomer present in dissolved form in the monomer phase is likewise removed.
摘要翻译： 一种在储存条件下储存液体的单体相的方法，其包含甲基丙烯酸单体至> 95重量％的程度，并且通过在气相中冷凝或熔融结晶相获得， 容器，其中以其溶解形式存在于液体单体相中的单体的聚合物在其从其产生进入储存容器的路线上被除去，以及从存储容器中抽出液体单体相的方法，其中单体的聚合物 在单体相中以溶解形式存在，同样地被除去。
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