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    Process for preparing (meth)acrylates of C17-alcohol mixtures
    3.
    发明授权
    Process for preparing (meth)acrylates of C17-alcohol mixtures 有权
    制备C17-醇混合物的（甲基）丙烯酸酯的方法

    公开(公告)号：US08664415B2

    公开(公告)日：2014-03-04

    申请号：US12952732

    申请日：2010-11-23

    申请人： Virginie Bette ,  Jochen Petzoldt ,  Boris Breitscheidel

    发明人： Virginie Bette ,  Jochen Petzoldt ,  Boris Breitscheidel

    IPC分类号： C09F7/00

    CPC分类号： C07C69/54 ,  C07C67/08 ,  C08F220/12 ,  C08F220/18

    摘要： A process for preparing (meth)acrylates of C17-alcohol mixtures by reacting (meth)acrylic acid with a C17-alcohol mixture in the presence of at least one acidic catalyst and of at least one polymerization inhibitor and in the presence of a solvent which, with water, forms an azeotrope in which the esterification is performed in a reactor with a circulation evaporator, the azeotrope is distilled off and condensed, and the condensate splits into an aqueous phase and an organic phase, wherein the C17-alcohol mixture has a mean degree of branching (iso index) of 2.8 to 3.7.

    摘要翻译： 一种通过使（甲基）丙烯酸与C17-醇混合物在至少一种酸性催化剂和至少一种聚合抑制剂存在下和在溶剂存在下使C17-醇混合物反应制备（甲基）丙烯酸酯的方法， 与水形成共沸物，其中在具有循环蒸发器的反应器中进行酯化，将共沸物蒸馏并冷凝，并将冷凝物分成水相和有机相，其中C17-醇混合物具有 平均分枝度（iso指数）为2.8〜3.7。

    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation
    4.
    发明授权
    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation 有权
    通过非均相催化气相部分氧化制备至少一种有机靶化合物的方法

    公开(公告)号：US08394345B2

    公开(公告)日：2013-03-12

    申请号：US12146807

    申请日：2008-06-26

    申请人： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    发明人： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    IPC分类号： B01J8/10

    CPC分类号： C07C51/252 ,  C07C57/04

    摘要： A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalysts charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line.

    摘要翻译： 通过在两个平行操作的氧化反应器管线中的有机前体化合物与分子氧的非均相催化气相部分氧化来制备有机靶化合物的方法，并且从处理线中的产物气流的混合物中除去目标化合物， 其中氧化线之一的催化剂装料包括一部分催化剂，其上已经进行非均相催化的气相部分氧化比在另一个氧化反应器管线的催化剂装料的催化剂的部分长。

    PROCESS FOR PREPARING SILOXY CARBOXYLATES
    5.
    发明申请
    PROCESS FOR PREPARING SILOXY CARBOXYLATES 审中-公开
    制备苯氧基羧酸酯的方法

    公开(公告)号：US20120157701A1

    公开(公告)日：2012-06-21

    申请号：US13329947

    申请日：2011-12-19

    申请人： Martin Gärtner ,  Jochen Petzoldt

    发明人： Martin Gärtner ,  Jochen Petzoldt

    IPC分类号： C07F7/18

    CPC分类号： C07F7/0876

    摘要： A process for preparing siloxy carboxylates is characterized by reaction of C2-C10-monocarboxylic acids with halosiloxanes of the general formula (I), Hal-(SiR2—O)x—SiR3  (I) in which Hal is the same or different and is fluorine, chlorine, bromine or iodine, R is hydrogen, C1-C10-alkyl or C6-C14-aryl and x is an integer from 1 to 20, to form hydrogen halide in the presence of an auxiliary base, in which the auxiliary base forms, with the hydrogen halide, a salt which forms two immiscible phases with the siloxy carboxylate or the solution of the siloxy carboxylate in a suitable solvent and is removed by a liquid-liquid separation. The process enables simple and economically viable preparation of siloxy carboxylates.

    摘要翻译： 制备甲硅烷氧基羧酸盐的方法的特征在于C2-C10-一元羧酸与通式（I）的卤代硅氧烷，Hal相同或不同的Hal-（SiR2-O）x-SiR3（I））反应， 氟，氯，溴或碘，R是氢，C 1 -C 10 - 烷基或C 6 -C 14 - 芳基，x是1至20的整数，在辅助碱的存在下形成卤化氢，其中辅助碱 与卤化氢形成与甲硅烷氧基羧酸酯或甲硅烷氧基羧酸酯在合适溶剂中的溶液形成两个不混溶相的盐，并通过液 - 液分离除去。 该方法使得能够简单且经济地制备甲硅烷氧基羧酸盐。

    Heterogeneous catalyst for the preparation of acrolein by partial gas phase oxidation of propene
    6.
    发明授权
    Heterogeneous catalyst for the preparation of acrolein by partial gas phase oxidation of propene 有权
    通过丙烯的部分气相氧化制备丙烯醛的非均相催化剂

    公开(公告)号：US07772148B2

    公开(公告)日：2010-08-10

    申请号：US11627573

    申请日：2007-01-26

    申请人： Jochen Petzoldt ,  Klaus Joachim Mueller-Engel

    发明人： Jochen Petzoldt ,  Klaus Joachim Mueller-Engel

    IPC分类号： B01J27/192 ,  B01J21/00 ,  B01J23/00

    CPC分类号： B01J35/026 ,  B01J23/8885 ,  B01J35/0006 ,  C07C45/35 ,  C07C47/22

    摘要： An annular unsupported catalyst for the heterogeneously catalyzed partial gas phase oxidation of propene to acrolein at a propene hourly space velocity on the fixed catalyst bed of ≧120 1 (STP)/1·h and a total CO2 and saturated hydrocarbon content of the starting reaction gas mixture of below 15 mol %, the catalysts of the fixed catalyst bed are the annular unsupported catalysts whose active composition is a multimetal oxide in which the molar Co/Fe ratio=from 2 to 4 and the molar Co/Mo ratio=from 0.3 to 0.7.

    摘要翻译： 一种环状无载体催化剂，用于丙烯到丙烯醛的非均相催化部分气相氧化，丙烯醛在固定催化剂床上的丙烯小时空速为≥1201（STP）/ 1·h，起始反应的总CO 2和饱和烃含量为 低于15mol％的气体混合物，固定催化剂床的催化剂是环状无载体催化剂，其活性组成是多金属氧化物，其中Co / Fe比为2-4，Co / Mo摩尔比为0.3 至0.7。

    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation
    8.
    发明授权
    Process for preparing at least one organic target compound by heterogeneously catalyzed gas phase partial oxidation 有权
    通过非均相催化气相部分氧化制备至少一种有机靶化合物的方法

    公开(公告)号：US07439389B2

    公开(公告)日：2008-10-21

    申请号：US11357300

    申请日：2006-02-21

    申请人： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    发明人： Martin Dieterle ,  Klaus Joachim Mueller-Engel ,  Jochen Petzoldt ,  Ulrich Hammon

    IPC分类号： C07C51/16 ,  C07C69/52

    CPC分类号： C07C51/252 ,  C07C57/04

    摘要： A process for preparing an organic target compound by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound with molecular oxygen in two oxidation reactor lines operated in parallel and removal of the target compound from the mixture of the product gas streams in a workup line, wherein the catalyst charge of one of the oxidation lines comprises a portion of catalyst over which the heterogeneously catalyzed gas phase partial oxidation has already been carried out for longer than over the portions of catalyst of the catalyst charge of the other oxidation reactor line.

    摘要翻译： 通过在两个平行操作的氧化反应器管线中的有机前体化合物与分子氧的非均相催化气相部分氧化来制备有机靶化合物的方法，并且从处理线中的产物气流的混合物中除去目标化合物， 其中一个氧化线的催化剂装料包括催化剂的一部分，在该部分的催化剂上已经进行非均相催化的气相部分氧化比在另一个氧化反应器管线的催化剂装料的催化剂部分上的时间长。