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公开(公告)号：US11330818B2
公开(公告)日：2022-05-17
申请号：US16948917
申请日：2020-10-06
Applicant: ECOLAB USA INC.
Inventor： Brandon Herdt , Richard Staub , Thomas C. Rustad , Junzhong Li , David D. McSherry , Paul R. Kraus , Richard Walsh
IPC: B01J19/24 , B01J14/00 , C07C407/00 , A01N37/16 , C02F1/50 , A01N59/00 , B01J4/00 , B01J19/00 , A61L2/24 , C07C409/24 , A61L2/18 , C02F1/72 , A01N37/02 , C02F103/08
Abstract: Methods and systems for temperature-controlled, on-site generation of peracids, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions are disclosed. In particular, methods for using an adjustable biocide formulator or generator system overcome the limitations of temperature on the kinetics of the peracid generation and/or peracid decomposition inside an adjustable biocide formulator or generator system. The methods include the controlling of the temperature of at least one raw starting material, namely water, to improve upon methods of on-site generation of peracids. The methods allow for the generation of user-selected chemistry without regard to the ambient temperatures of the raw starting materials and/or the biocide formulator or generator system.
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公开(公告)号：US20210368787A1
公开(公告)日：2021-12-02
申请号：US17303409
申请日：2021-05-28
Applicant: ECOLAB USA INC.
Inventor： Junzhong Li , Joshua Luedtke , Jesse David Hines , John Paul Koehl , Richard Staub
Abstract: Biocide compositions efficacious for biofilm control, including treatment and/or prevention, comprising the synergistic combination of biocide(s) with a source of hydronium ions are disclosed. Methods of deactivating, removing and/or preventing biofilms with the compositions are also provided.
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公开(公告)号：US11026420B2
公开(公告)日：2021-06-08
申请号：US16559894
申请日：2019-09-04
Applicant: ECOLAB USA INC.
Inventor： Junzhong Li , Cynthia Bunders , Richard Staub , Paul Frazer Schacht , Caleb Power , Ramakrishnan Balasubramanian , Robert J. Ryther , Catherine Hanson
Abstract: Peroxyformic acid compositions for treatment and removal of biofilm growth and mineral deposits on membranes for energy services applications are disclosed. In particular, peroxyformic acid compositions are generated in situ or on site generation for the reduction and prevention, of biofilms and the mitigation of mineral buildup on the membranes. The compositions according to the invention are compatible with the membranes under application of use conditions.
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公开(公告)号：US10899707B2
公开(公告)日：2021-01-26
申请号：US16259009
申请日：2019-01-28
Applicant: ECOLAB USA INC.
Inventor： Ramakrishnan Balasubramanian , Junzhong Li , Richard Staub , Victor Keasler , Brian Bennett , Allison Brewster
IPC: C07C409/24 , C07C407/00 , A23L3/3508 , C23F11/14 , C23F11/10 , C23F11/167 , A01N37/16 , A23L3/3463
Abstract: The present invention relates generally to methods for forming peroxyformic acid, comprising contacting formic acid with hydrogen peroxide. The methods for forming peroxyformic acid can include adding formic acid with a relatively lower concentration of hydrogen peroxide, or adding formic acid to a peroxycarboxylic acid composition or forming composition to react with hydrogen peroxide in the compositions. The present invention also relates to peroxyformic acid formed by the above methods. The present invention further relates to the uses of peroxyformic acid for treating a variety of targets, e.g., target water, including target water used in connection with oil- and gas-field operations. The present invention further relates to methods for reducing or removing H2S or iron sulfide in the treated water source, improving clarity of the treated water source, or reducing the total dissolved oxygen or corrosion in the treated water source, using peroxyformic acid, including peroxyformic acid generated in situ.
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公开(公告)号：US10737302B2
公开(公告)日：2020-08-11
申请号：US15381855
申请日：2016-12-16
Applicant: Ecolab USA Inc.
Inventor： Junzhong Li , Cynthia Bunders , Richard Staub , Paul Frazer Schacht , Caleb Power
Abstract: Peroxyformic acid compositions for removal of biofilm growth and mineral deposits on membranes are disclosed. In particular, peroxyformic acid compositions are generated in situ or on site generation for the reduction and prevention, of biofilms and the mitigation of mineral buildup on the membranes. The compositions according to the invention are compatible with the membranes under application of use conditions.
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Patent Agency Ranking
公开(公告)号：US20200157046A1
公开(公告)日：2020-05-21
申请号：US16773288
申请日：2020-01-27
Applicant: ECOLAB USA INC.
Inventor： Ramakrishnan Balasubramanian , Junzhong Li , Richard Staub , Victor Keasler , Brian Bennett , Allison Brewster
IPC: C07C409/24 , C07C407/00 , A23L3/3508 , C23F11/14 , C23F11/10 , C23F11/167 , A01N37/16 , A23L3/3463
Abstract: The present invention relates generally to methods for forming peroxyformic acid, comprising contacting formic acid with hydrogen peroxide. The methods for forming peroxyformic acid can include adding formic acid with a relatively lower concentration of hydrogen peroxide, or adding formic acid to a peroxycarboxylic acid composition or forming composition to react with hydrogen peroxide in the compositions. The present invention also relates to peroxyformic acid formed by the above methods. The present invention further relates to the uses of peroxyformic acid for treating a variety of targets, e.g., target water, including target water used in connection with oil- and gas-field operations. The present invention further relates to methods for reducing or removing H2S or iron sulfide in the treated water source, improving clarity of the treated water source, or reducing the total dissolved oxygen or corrosion in the treated water source, using peroxyformic acid, including peroxyformic acid generated in situ.
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公开(公告)号：US20200029560A1
公开(公告)日：2020-01-30
申请号：US16590478
申请日：2019-10-02
Applicant: ECOLAB USA INC.
Inventor： Junzhong Li , David D. McSherry , Richard Staub
IPC: A01N37/16 , A01N37/12 , C07C409/24
Abstract: The present disclosure is related to percarboxylic acid compositions formed in situ in non-equilibrium reactions. The peroxycarboxylic acid compositions are formed using ester based starting materials. Methods for using the percarboxylic acid compositions are also disclosed.
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公开(公告)号：US10542751B2
公开(公告)日：2020-01-28
申请号：US15967077
申请日：2018-04-30
Applicant: ECOLAB USA INC
Inventor： Junzhong Li , Allison Brewster , Richard Staub , Steven J. Lange , Taz Cheritu , Jonathan P. Fast , Catherine Hanson
IPC: A01N37/16 , C07C407/00 , C11D3/00 , C12P7/40 , C11D3/39 , C11D3/48 , C07C409/24 , A01N37/00 , A61L2/00 , A61L2/16 , A61K8/38 , A61Q17/00
Abstract: The present invention relates generally to peroxyformic acid forming compositions, methods for forming peroxyformic acid, preferably in situ, using the peroxyformic acid forming compositions. The present invention also relates to the peroxyformic acid formed by the above compositions and methods. The present invention further relates to the uses of the peroxyformic acid, preferably in situ, for treating a surface or a target. The present invention further relates to methods for treating a biofilm using peroxyformic acid, including peroxyformic acid generated in situ.
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公开(公告)号：US10017403B2
公开(公告)日：2018-07-10
申请号：US13798311
申请日：2013-03-13
Applicant: ECOLAB USA INC.
Inventor： Victor Keasler , Renato De Paula , Junzhong Li , David D. McSherry , Brandon Herdt , Richard Staub
IPC: A01N25/22 , A01N25/32 , A01N37/16 , C02F1/50 , C02F1/70 , C02F1/72 , C02F3/34 , C09K8/60 , C09K8/66 , E21B21/06 , E21B43/00 , C02F1/76 , C02F103/08 , C02F103/10 , C02F103/36
CPC classification number: C02F1/70 , A01N25/22 , A01N25/32 , A01N37/16 , C02F1/50 , C02F1/722 , C02F1/76 , C02F3/342 , C02F2103/08 , C02F2103/10 , C02F2103/365 , C02F2303/04 , C02F2303/08 , C02F2303/18 , C02F2303/20 , C02F2305/02 , C09K8/605 , C09K8/66 , C09K2208/28 , C09K2208/32 , E21B21/068 , E21B43/00 , Y02W10/37 , A01N59/00
Abstract: Compositions and methods for the use of peracid compositions having low to substantially no hydrogen peroxide for various water treatments, including oil- and gas-field operations, and/or other aseptic treatments are disclosed. In numerous aspects, peracetic acid is the preferred peracid and is treated with a peroxide-reducing agent to substantially reduce the hydrogen peroxide content. Methods for using the treated peracid compositions for treatment of drilling fluids, frac fluids, flow back waters and disposal waters are also disclosed for improving water condition, reducing oxidizing damage associated with hydrogen peroxide and/or reducing bacteria infestation.
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公开(公告)号：US10010075B2
公开(公告)日：2018-07-03
申请号：US14562960
申请日：2014-12-08
Applicant: Ecolab USA Inc.
Inventor： Brandon Herdt , Richard Staub , Thomas C. Rustad , Junzhong Li , David D. McSherry , Paul R. Kraus , Richard Walsh
IPC: B05C3/00 , B08B3/04 , A01N37/16 , C02F1/50 , C07C407/00 , A01N59/00 , B01J19/00 , B01J4/00 , A61L2/24 , C07C409/24 , A61L2/18 , B01J19/24 , B01J14/00 , C02F1/72 , C02F103/08
CPC classification number: A01N37/16 , A01N37/02 , A01N59/00 , A61L2/18 , A61L2/186 , A61L2/24 , A61L2202/14 , B01J4/001 , B01J4/008 , B01J14/00 , B01J19/0006 , B01J19/0013 , B01J19/24 , B01J2219/00049 , B01J2219/00121 , B01J2219/00159 , B01J2219/24 , C02F1/50 , C02F1/722 , C02F2103/08 , C07C407/00 , C07C409/24 , A01N2300/00
Abstract: Methods and systems for temperature-controlled, on-site generation of peracids, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions are disclosed. In particular, methods for using an adjustable biocide formulator or generator system overcome the limitations of temperature on the kinetics of the peracid generation and/or peracid decomposition inside an adjustable biocide formulator or generator system. The methods include the controlling of the temperature of at least one raw starting material, namely water, to improve upon methods of on-site generation of peracids. The methods allow for the generation of user-selected chemistry without regard to the ambient temperatures of the raw starting materials and/or the biocide formulator or generator system.
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