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公开(公告)号：US4793850A
公开(公告)日：1988-12-27
申请号：US798210
申请日：1985-11-14
申请人： Josef Koester , Karl Schmid , Konrad Albrecht , Paul Bittner , Fritz Keim
发明人： Josef Koester , Karl Schmid , Konrad Albrecht , Paul Bittner , Fritz Keim
摘要： An evaporation inhibitor composition which consists essentially of:A. from about 15 to about 50% by weight of a wax mixture containing at least about 5% by weight, based on the wax mixture, of a wax component having an acid number of from about 10 to about 95 mg KOH/g wax;B. from about 4 to about 20% by weight of at least one nonionic and/or anionic emulsifier;C. from about 19.5 to about 81% by weight of water and/or at least one organic solvent selected from the group consisting of hydrocarbons, esters, and ketones having a boiling point of from about 70.degree. to about 280.degree. C.
摘要翻译： 一种蒸发抑制剂组合物，其基本上由以下组成：A.约15至约50重量％的蜡混合物，其基于蜡混合物含有至少约5重量％的蜡组分，所述蜡组分的酸值为约 10至约95mg KOH / g蜡; B.约4至约20重量％的至少一种非离子和/或阴离子乳化剂; C.约19.5至约81重量％的水和/或至少一种选自沸点为约70至约280℃的烃，酯和酮的有机溶剂。
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62.发明授权Process for the preparation of fatty acid alkyl esters having improved processing properties 失效具有改进加工性能的脂肪酸烷基酯的制备方法
公开(公告)号：US4650611A
公开(公告)日：1987-03-17
申请号：US749056
申请日：1985-06-26
申请人： Karl Schmid , Horst Baumann
发明人： Karl Schmid , Horst Baumann
摘要： Lower alkyl esters of higher fatty acids with improved processing properties, particularly sulfonation, are obtained by subjecting lower alkyl esters of higher fatty acids of plant and/or animal origin, or said fatty acids per se, in the presence of esterification catalysts and/or carboxylic acid anhydrides, to a brief temperature treatment above 150.degree. C., and separating simultaneously and/or subsequently, preferably by distillation, the purified lower alkyl esters of higher fatty acids or the purified higher fatty acids from the treated material and the purified higher fatty acids are then esterified with lower alkanols.
摘要翻译： 具有改进的加工性能，特别是磺化的高级脂肪酸的低级烷基酯是通过在酯化催化剂存在下使植物和/或动物来源的高级脂肪酸的低级烷基酯或所述脂肪酸本身进行的，和/或 羧酸酐在150℃以上进行短暂温度处理，并同时和/或随后优选通过蒸馏分离纯化的高级脂肪酸低级烷基酯或经处理物质的纯化高级脂肪酸和纯化的较高级 脂肪酸然后用低级链烷醇酯化。
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63.发明授权
公开(公告)号：US4552702A
公开(公告)日：1985-11-12
申请号：US397095
申请日：1982-07-12
申请人： Karl Schmid , Horst Baumann
发明人： Karl Schmid , Horst Baumann
摘要： Lower alkyl esters of higher fatty acids with improved processing properties, particularly sulfonation, are obtained by subjecting lower alkyl esters of higher fatty acids of plant and/or animal origin, or said fatty acids per se, in the presence of esterification catalysts and/or carboxylic acid anhydrides, to a brief temperature treatment above 150.degree. C., and separating simultaneously and/or subsequently, preferably by distillation, the purified lower alkyl esters of higher fatty acids or the purified higher fatty acids from the treated material and the purified higher fatty acids are then esterified with lower alkanols.
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公开(公告)号：US4520578A
公开(公告)日：1985-06-04
申请号：US492432
申请日：1983-05-06
申请人： Christian Schiel , Georg Zurn , Karl Schmid
发明人： Christian Schiel , Georg Zurn , Karl Schmid
摘要： A drying cylinder adapted to receive steam therein includes a cylindrical cylinder jacket and two end covers. There is a flange connection between the jacket and the covers. The jacket has a rectangular cross-section flange. The covers have an L-shaped flange which receives the end flange of the cover. The covers are concave to the outside of the cylinder. The point of intersection of a curved line through the cover and of the axial center line of the axial arm of the cover flange lies at a distance from the outer face of the flange of the end cover that is at most about 60% of the axial length of the axial arm of that flange. There is thermal insulation on the axially exterior side of each cover.
摘要翻译： 适于在其中接受蒸汽的干燥筒包括圆柱形圆筒套和两个端盖。 护套和盖子之间有法兰连接。 护套具有矩形横截面法兰。 盖子有一个L形的凸缘，它接收盖的端部凸缘。 盖子对缸体的外侧是凹的。 通过盖子的曲线和盖凸缘的轴向臂的轴线中心线的交点与端盖的凸缘的外表面的距离至多为轴向的约60％ 该法兰的轴向臂的长度。 每个盖子的轴向外侧都有保温。
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公开(公告)号：US4418217A
公开(公告)日：1983-11-29
申请号：US257632
申请日：1981-04-27
IPC分类号： C07C43/164 , B01F17/42 , B01J27/00 , B01J27/02 , B01J27/16 , B01J29/00 , B01J29/04 , B01J31/00 , B01J31/02 , B01J31/08 , C07C41/00 , C07C41/48 , C07C43/11 , C07C43/30 , C07C43/315 , C07C67/00 , C08G4/00 , C08G65/00 , C08G65/32 , C08G65/331 , C08G65/34 , C11D1/72 , C07C41/14
CPC分类号： C08G65/331 , C07C43/30 , C08G4/00 , C08G65/34 , C11D1/721 , Y10S516/01
摘要： A process for the production of a mixed formal of polyglycol ethers having formulae selected from the group consisting of ##STR1## wherein R.sup.1 is a straight or branched chain alkyl having from 1 to 18 carbon atoms, and R.sup.2 is selected from the group consisting of hydrogen and straight or branched chain alkyl having from 1 to 17 carbon atoms, where the sum of the carbon atoms in R.sup.1 plus R.sup.2 is from 6 to 18, R.sup.3 is a member selected from the group consisting of monoalkylphenyl having from 14 to 26 carbon atoms, dialkylphenyl having from 14 to 26 carbon atoms, trialkylphenyl having from 14 to 26 carbon atoms, a straight or branched chain alkyl having from 8 to 22 carbon atoms, a straight or branched chain alkenyl having from 8 to 22 carbon atoms, and a radical having the formula ##STR2## wherein R.sup.1 and R.sup.2 have the above assigned values, and R.sup.5 is selected from the group consisting of a straight or branched chain alkyl having from 1 to 5 carbon atoms, phenyl and alkylphenyl having from 7 to 9 carbon atoms, R.sup.4 is a straight or branched chain alkyl having from 1 to 5 carbon atoms, A and B are selected from the group consisting of ethylene and isopropylene, m and n are integers from 0 to 50, p is an integer from 2 to 50, and q is an integer from 0 to 3, where the sum of m plus n is from 2 to 50, consisting essentially of the steps of(1) reacting a polyglycol ether having the formulae selected from the group consisting of ##STR3## wherein R.sup.1, R.sup.2, R.sup.3, A, m, n and p have the above-assigned meanings, with a diformal having the formulaR.sup.4 --O--(B--O).sub.q --CH.sub.2 --(O--B).sub.q --O--R.sup.4wherein R.sup.4, B and q have the above-assigned meanings, at a temperature of from 60.degree. to 150.degree. C. in the presence of a strong acid, while employing from 2 to 10 mols of said diformal per mol of hydroxyl groups in said polyglycol ether.(2) distilling off the alcohol formed having the formulaR.sup.4 --O--(B--O).sub.q --H(3) neutralizing,(4) distilling of unreacted diformal, and(5) recovering said mixed formal of polyglycol ethers; as well as novel mixed formals of polyglycol ethers produced by the process.
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