公开(公告)号：US10144662B2

公开(公告)日：2018-12-04

申请号：US14951117

申请日：2015-11-24

申请人： Evonik Degussa GmbH

发明人： Manfred Kreczinski ,  Robert Jansen ,  Matthias Woyciechowski

IPC分类号： C02F1/72 ,  C02F1/76 ,  C02F1/04 ,  C02F1/66 ,  C02F1/78 ,  C02F101/38 ,  C02F103/36 ,  C02F101/34

摘要： Contaminated wastewater from the preparation of isophorone, isophoronenitrile and isophoronediamine is treated by A) 1. treating the wastewater from the preparation of isophoronenitrile from the reaction of isophorone with hydrogen cyanide by alkaline hydrolysis of isophoronenitrile to isophorone, and the salts of hydrogen cyanide within a pH range of 12.0 to 13.7 and at temperatures of 60 to 200° C., and 2. processing the wastewater from A) 1. by an oxidation, or B) treating the wastewater from the preparation of isophoronenitrile from the reaction of isophorone with hydrogen cyanide by an oxidation, or C) processing the wastewater from A) 1. and the wastewater from the preparation of isophorone and/or the wastewater from the preparation of isophoronediamine by an oxidation.

公开(公告)号：US10131628B2

公开(公告)日：2018-11-20

申请号：US15507970

申请日：2015-07-23

申请人： Katrin Marie Dyballa ,  Robert Franke ,  Dirk Fridag ,  Siegfried R. Waldvogel ,  Bernd Elsler ,  Mathias Enders

发明人： Katrin Marie Dyballa ,  Robert Franke ,  Dirk Fridag ,  Siegfried R. Waldvogel ,  Bernd Elsler ,  Mathias Enders

IPC分类号： C25B3/10 ,  C07C311/21 ,  C07C233/25 ,  C07C233/43 ,  C07C217/84 ,  C25B11/12

摘要： An electrochemical treatment of differently protected aniline or napthylamine results in the preparation of unsymmetrical 2, 2′-diaminebiaryls provided with different protecting groups. The treatment involves the protecting groups prior to the C, C coupling step. The co-reactants generally have different oxidation potentials which results from the selection of the protecting groups. The treatment also enables controlled access to the individual amino functions of the 2, 2′-diaminobiaryls by subsequent selective deprotection.

公开(公告)号：US20180327432A1

公开(公告)日：2018-11-15

申请号：US15771227

申请日：2016-10-11

申请人： EVONIK DEGUSSA GMBH

发明人： Emmanouil Spyrou ,  Manfred Kreczinski ,  Tobias Unkelhaeusser ,  Sabine Naumann ,  Holger Loesch ,  Marion Ewald ,  Thomas Weihrauch

IPC分类号： C07F7/18 ,  C07C271/66 ,  C09D175/04 ,  C09J175/04

CPC分类号： C07F7/1804 ,  C07C271/66 ,  C08F20/00 ,  C08G18/6225 ,  C08G18/718 ,  C08G18/7837 ,  C09D133/066 ,  C09D175/04 ,  C09J175/04

摘要： A monoallophanate can be used in paint or adhesive compositions. The monoallophanate has the formula 1: where R, R1-R6 are each independently identical or different hydrocarbyl radicals having 1-8 carbon atoms, which may be branched or cyclic, or else may be integrated together to form a cyclic system, and m and n are each independently 0-2.

公开(公告)号：US10125108B2

公开(公告)日：2018-11-13

申请号：US15570167

申请日：2016-04-19

申请人： Robert Jahn ,  Wolfgang Wöll ,  Bernd Jaeger ,  Matthias Pascaly

发明人： Robert Jahn ,  Wolfgang Wöll ,  Bernd Jaeger ,  Matthias Pascaly

IPC分类号： C07D301/12 ,  C07D303/04 ,  B01D3/34 ,  B01D3/42 ,  B01D19/04 ,  B01J29/89 ,  C07D301/36

摘要： In a process for the epoxidation of propene, comprising the steps: reacting propene with hydrogen peroxide in the presence of a titanium silicalite catalyst and a methanol solvent; separating non-reacted propene and propene oxide from the resulting reaction mixture to provide a solvent mixture comprising methanol and water in a combined amount of at least 90% by weight; and feeding this solvent mixture as a feed stream to a continuously operated methanol distillation column at a feed point in the middle section of said column to provide an overhead product comprising at least 90% by weight methanol and a bottoms product comprising at least 90% by weight water; the addition of a liquid defoamer, having a solubility in the feed stream of less than 10 mg/kg at 25° C. and a surface tension at the liquid air interface of less than 22 mN/m at 20° C., at or above the feed point in an amount exceeding the solubility of the liquid defoamer in the feed stream suppresses foam formation in the methanol distillation column.

公开(公告)号：US10119002B2

公开(公告)日：2018-11-06

申请号：US13178558

申请日：2011-07-08

申请人： Juan Jesus Burdeniuc ,  James Douglas Tobias ,  Renee Jo Keller ,  You-Moon Jeon

发明人： Juan Jesus Burdeniuc ,  James Douglas Tobias ,  Renee Jo Keller ,  You-Moon Jeon

IPC分类号： C08J9/00 ,  C08G18/18 ,  C08G18/32 ,  C08G18/38 ,  C08G18/48 ,  C08G18/66 ,  C08G18/67 ,  C08K5/31 ,  C08G101/00

摘要： Polyurethane foam compositions and processes to make flexible polyurethane foams are disclosed. Polyurethane foam is produced in the presence of additives comprising guanidine derivatives. Improvements in physical properties such as air flow, dimensional stability, tensile, tear, elongation and foam hardness is observed when these additives are present in polyurethane formulations. In addition, these additives can minimize polymer degradation under humid ageing conditions resulting in foam products with better mechanical properties.

公开(公告)号：US10113671B2

公开(公告)日：2018-10-30

申请号：US14224807

申请日：2014-03-25

申请人： Juergen Franosch ,  Jan Berger ,  Andreas Dowe ,  Marco Gensheimer ,  Uwe Kannengiesser

发明人： Juergen Franosch ,  Jan Berger ,  Andreas Dowe ,  Marco Gensheimer ,  Uwe Kannengiesser

IPC分类号： F16L9/00 ,  F16L57/00 ,  F16L58/00 ,  B29C63/00 ,  F16L9/14 ,  B29C63/34 ,  F16L9/19 ,  F16L57/06 ,  F16L58/10 ,  F16L9/147 ,  E21B17/00

摘要： A process for the production of a pipe comprising: an interior surface having a shape; and a thermoplastic inliner is provided. The process comprises: introducing the thermoplastic inliner into the interior of the pipe; heating the pipe from the outside to a temperature higher than a crystallite melting point (Tm) of a molding composition of an exterior surface of the inliner; expanding the inliner radially in the pipe so that an exterior surface of the inliner assumes the shape of the interior surface of the pipe; and cooling the inliner; wherein a cross section of the inliner is optionally reduced through exposure to an exterior force prior to being introduced into the pipe. Relative movements between carrier pipe and inliner are thus prevented; the risk of collapse of the inliner is moreover low. The pipe is used for the production of a laid pipeline.

公开(公告)号：US10113025B2

公开(公告)日：2018-10-30

申请号：US15089745

申请日：2016-04-04

申请人： Evonik Degussa GmbH

发明人： Christoph Juergen Duerr ,  Bettina Burian ,  Daniel Engelke ,  Michael Ewald ,  Tanja Joerres ,  Erika Retzlaff

IPC分类号： C08G6/02 ,  C09D161/02 ,  C08G18/54 ,  C09D5/02 ,  C09D17/00 ,  C08G12/06 ,  C09B67/46 ,  C08G18/75 ,  C09D175/04 ,  C08G4/00 ,  C08G16/02 ,  C09D159/00 ,  C09D161/00 ,  C09D161/22

摘要： A functionalized ketone-aldehyde condensation resin is produced by condensing a ketone and an aldehyde in the presence of at least one alcohol or alkoxylate thereof, wherein the alcohol comprises amino alcohols and derivatives thereof, hydroxybutyl vinyl ether, OH-functional acrylates, OH-functional terpenes, OH-functional halogen compounds, hydroxycarboxylic acids, sulphur-containing alcohols, hydroxyl-containing urea derivatives, carbohydrates, siloxanes, OH-functional phosphorus compounds or unsaturated alcohols.

公开(公告)号：US10106497B2

公开(公告)日：2018-10-23

申请号：US15157934

申请日：2016-05-18

申请人： EVONIK DEGUSSA GMBH

发明人： Katrin Marie Dyballa ,  Robert Franke ,  Siegfried R Waldvogel ,  Thomas Quell ,  Michael Mirion

IPC分类号： C07C391/02

摘要： The present invention relates to a method for coupling two arenes with selenium dioxide to give a selenobiaryl ether. The method of the present invention includes: adding a first arene to the reaction mixture, adding a second arene to the reaction mixture, adding selenium dioxide to the reaction mixture, adding an acid having a pKa in the range from 0 to 5 to the reaction mixture, and adjusting the reaction temperature of the reaction mixture such that the first arene and the second arene are converted to a selenobiaryl ether. The present invention also relates to novel selenobiaryl ethers.

公开(公告)号：US10105644B2

公开(公告)日：2018-10-23

申请号：US15619584

申请日：2017-06-12

申请人： Evonik Degussa GmbH

发明人： Olivier Zehnacker ,  Benjamin Willy

IPC分类号： B01D53/26 ,  B01D53/77 ,  B01D53/78 ,  C07C9/02 ,  C07D233/56 ,  C07F9/09 ,  C07F9/11 ,  C01D5/00

摘要： The invention relates to a process for dehumidifying a moist gas mixture in which the moist gas mixtures are brought into contact with an absorbent comprising dialkylimidazolium salts and trialkyl phosphate. In addition, the invention also relates to an absorption heat pump comprising the absorbent according to the invention and to the absorbent according to the invention itself.

公开(公告)号：US10103384B2

公开(公告)日：2018-10-16

申请号：US14903864

申请日：2013-07-09

申请人： EVONIK DEGUSSA GmbH

发明人： Bernhard Haeupler ,  Ulrich Schubert

IPC分类号： H01M4/60 ,  H01M4/62 ,  H01M4/86 ,  H01M4/90 ,  C08F112/14 ,  C08F226/10 ,  H01G11/30 ,  H01G9/042

摘要： Disclosed is an oligomeric or polymeric compound comprising at least two structural units of formula (I) wherein Ar is a carbocyclic aromatic radical or a heterocyclic aromatic radical with the two carbonyl carbon atoms being attached to two ring carbon atoms of the Ar group forming together with the imide-nitrogen atom a five-membered or a six-membered ring X is a divalent group selected from —CR1R2—, —CO—, —SiR3R4—, —P(O)R5—, —P(O)(OR6)—, —PR7—, —P(OR8)—, —S(O)— or —S(O)2—. R1 to R8 independently of one another are hydrogen, alkyl, cycloalkyl, aryl or heteroaryl groups, R9 is a divalent hydrocarbon group or a covalent bond, and R10, R11 and R12 independently of one another are hydrogen or C1-C6 alkyl or R10 and R11 or R10 and R12 together with the carbon atoms to which they are attached form a cycloaliphatic ring or a bicyclic aliphatic system The oligomeric or polymeric compound comprising units of formula (I) of the invention can be used as redox-active material in storage means for electric energy, for example in batteries, redox-flow cells, fuel cells or capacitors.