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公开(公告)号：US09856355B2
公开(公告)日：2018-01-02
申请号：US11236380
申请日：2005-09-27
IPC分类号： C08J9/00 , C08G18/40 , C08G18/61 , C08G18/65 , C08K5/5419 , C08G101/00
CPC分类号： C08J9/0061 , C08G18/4072 , C08G18/61 , C08G18/657 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J2375/04 , C08J2483/00 , C08K5/5419 , C08L75/04
摘要： Methods for preparing polyurethane flexible foam are described, wherein an organic polyisocyanate is reacted with an active hydrogen-containing component such as an organic polyol, in the presence of a urethane catalyst, a blowing agent, optionally a cell opener, and a siloxane-based surfactant composition as a stabilizer for the foam. The siloxane-based surfactant composition comprises a silanol-functionalized organosiloxane having general formula (I), wherein: the R groups are independently a C1-C3 alkyl, phenyl, or —OSi(R)3; provided that at least one R group is a hydroxyl (—OH) bonded directly to any silicon atom and X is an integer from 0-200.
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公开(公告)号：US09334382B2
公开(公告)日：2016-05-10
申请号：US13178562
申请日：2011-07-08
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译： 公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。 使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的细胞开放助剂 还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。 使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。 此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。
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3.发明授权公开(公告)号：US09145466B2
公开(公告)日：2015-09-29
申请号：US13534239
申请日：2012-06-27
IPC分类号： C08G18/36 , C08G18/30 , C08G18/32 , C08G18/48 , C08G18/66 , C08G18/76 , C08G101/00 , C08K5/00 , C08K5/05 , C08K5/06 , C08K5/20 , C08K5/315 , C08K5/3445 , C08K5/41 , C08K5/45
CPC分类号： C08G18/14 , C08G18/302 , C08G18/3206 , C08G18/343 , C08G18/36 , C08G18/4841 , C08G18/6696 , C08G18/7621 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J2205/06 , C08K5/0008 , C08K5/05 , C08K5/06 , C08K5/20 , C08K5/315 , C08K5/3445 , C08K5/41 , C08K5/45
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译： 公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。 使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的开放助剂 还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。 使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。 此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。
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公开(公告)号：US08552078B2
公开(公告)日：2013-10-08
申请号：US11582178
申请日：2006-10-17
CPC分类号： C08G18/4072 , C08G18/1825 , C08G18/2027 , C08G18/3225 , C08G18/657 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： A composition for making a polyurethane foam includes a non-fugitive tertiary amine urethane catalyst and an alkylated polyamine crosslinking additives. Foams prepared from the reaction of a polyol and an organic isocyanate in the presence of these ingredients show improved resistance to deterioration of physical properties upon humid ageing.
摘要翻译： 用于制备聚氨酯泡沫的组合物包括非逸散性叔胺氨基甲酸酯催化剂和烷基化多胺交联添加剂。 在这些成分的存在下，由多元醇与有机异氰酸酯的反应制备的泡沫显示出改善的抗潮湿老化时的物理性能的劣化。
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公开(公告)号：US08258198B2
公开(公告)日：2012-09-04
申请号：US11131179
申请日：2005-05-18
申请人： Gary Dale Andrew , Mark Leo Listemann , Patrick Gordon Stehley , James Douglas Tobias , John William Miller
发明人： Gary Dale Andrew , Mark Leo Listemann , Patrick Gordon Stehley , James Douglas Tobias , John William Miller
IPC分类号： B01J31/02
CPC分类号： C08G18/7671 , C08G18/092 , C08G18/10 , C08G18/161 , C08G2101/0083 , C08G18/664
摘要： Catalyst compositions for use in forming polyurethane products include a gelling catalyst, a trimerization catalyst, and a cure accelerator. The gelling catalyst is a tertiary amine, mono(tertiary amino) urea, bis(tertiary amino) urea, or a combination of any of these. Any known trimerization catalyst may be used. The cure accelerator may be a diol having at least one primary hydroxyl group, and having from five to 17 chain backbone atoms chosen from carbon, oxygen, or both between the hydroxyl groups, provided that at least five of the backbone atoms are carbon. Alternatively or in addition, the cure accelerator may be a polyol having three or more hydroxyl groups, at least two of which are primary, and having molecular weights between 90 g/mole and 400 g/mole. Delayed initiation of the polyurethane-forming reaction and/or reduced demold time for producing the polyurethane part can be obtained by using these catalyst compositions.
摘要翻译： 用于形成聚氨酯产品的催化剂组合物包括胶凝催化剂，三聚催化剂和固化促进剂。 胶凝催化剂是叔胺，单（叔氨基）脲，双（叔氨基）脲或这些中的任何一种的组合。 可以使用任何已知的三聚催化剂。 固化促进剂可以是具有至少一个伯羟基的二醇，并且在羟基之间具有5至17个选自碳，氧或两者的链骨架原子，条件是至少五个骨架原子是碳。 或者或另外，固化促进剂可以是具有三个或更多个羟基的多元醇，其中至少两个是伯的，分子量在90g / mol至400g / mol之间。 通过使用这些催化剂组合物可以获得聚氨酯形成反应的延迟起始和/或用于制备聚氨酯部分的脱模时间的减少。
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公开(公告)号：US20120178839A1
公开(公告)日：2012-07-12
申请号：US13178562
申请日：2011-07-08
CPC分类号： C08J9/0028 , C08G18/0838 , C08G18/16 , C08G18/185 , C08G18/4072 , C08G18/6552 , C08G2101/00 , C08G2101/0008 , C08J9/0033 , C08J9/0042 , C08J2205/05 , C08J2375/04 , C08J2375/08
摘要： A composition and process useful to make flexible polyurethane foams and in particular flexible molded polyurethane foams is disclosed. The usage of dipolar aprotic liquids such as DMSO, DMI, sulfolane, N-methyl-acetoacetamide, N,N-dimethylacetoacetamide as well as glycols containing hydroxyl numbers OH#≦1100 as cell opening aides for 2-cyanoacetamide or other similar molecules containing active methylene or methine groups to make a polyurethane foam is also disclosed. The advantage of using cell opener aids results in a) no foam shrinkage; b) lower use levels of cell opener; c) foam performance reproducibility d) optimum physical properties. In addition, combining the acid blocked amine catalyst together with the cell opener and the cell opener aid results in a less corrosive mixture as well as provides a method that does not require mechanical crushing for cell opening.
摘要翻译： 公开了用于制备柔性聚氨酯泡沫，特别是柔性模塑聚氨酯泡沫的组合物和方法。 使用偶极非质子液体如DMSO，DMI，环丁砜，N-甲基 - 乙酰乙酰胺，N，N-二甲基乙酰乙酰胺以及含有羟基数OH＃＆amp; 1100的二醇作为2-氰基乙酰胺或其它类似分子的细胞开放助剂 还公开了制备聚氨酯泡沫的活性亚甲基或次甲基。 使用细胞开放助剂的优点导致a）没有泡沫收缩; b）细胞开放剂的使用水平较低; c）泡沫性能重现性d）最佳物理性能。 此外，将酸封闭的胺催化剂与开孔剂和开孔剂组合在一起导致较少的腐蚀性混合物，并且提供了不需要机械破碎以进行开孔的方法。
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7.发明授权Dimensional stabilizing, cell opening additives for polyurethane flexible and rigid foams 失效尺寸稳定，聚氨酯柔性和刚性泡沫的开孔添加剂
公开(公告)号：US6046249A
公开(公告)日：2000-04-04
申请号：US338105
申请日：1999-06-23
申请人： James Douglas Tobias , Julia Renae Bennett , Gary Dale Andrew , John Elton Dewhurst , Robert G. Petrella
发明人： James Douglas Tobias , Julia Renae Bennett , Gary Dale Andrew , John Elton Dewhurst , Robert G. Petrella
IPC分类号： C08G18/00 , C08G18/18 , C08G18/34 , C08G18/40 , C08G18/42 , C08G18/48 , C08G18/65 , C08G18/66
CPC分类号： C08G18/341 , C08G18/6552 , C08G2101/0008 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： A method for preparing a polyurethane flexible or rigid foam by reacting an organic polyisocyanate with a polyol in the presence of urethane catalyst, water as a blowing agent, optionally a silicone surfactant, and a cell opener characterized in that the cell opener comprises the reaction product of a C1-C20 hydrocarbyl group-containing organic acid anhydride and a substituted phenol which may be alkoxylated or an alkoxylated primary alcohol, optionally reacted in the presence of a tertiary amine urethane catalyst.
摘要翻译： 一种通过有机多异氰酸酯与聚氨酯催化剂，水作为发泡剂，任选的硅氧烷表面活性剂的存在下反应制备聚氨酯软质或刚性泡沫的方法，以及开孔剂，其特征在于开孔剂包括反应产物 含有C1-C20烃基的有机酸酐和可以被烷氧基化的取代苯酚或烷氧基化伯醇，任选在叔胺氨基甲酸酯催化剂存在下反应。
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8.发明授权公开(公告)号：US09447223B2
公开(公告)日：2016-09-20
申请号：US13534171
申请日：2012-06-27
CPC分类号： C08G18/6696 , C08G18/3838 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J9/0028 , C08J2205/06 , C08J2375/04 , C08K5/31 , C08K5/3155 , C08L75/04
摘要： Polyurethane foam compositions and processes to make flexible polyurethane foams are disclosed. Polyurethane foam is produced in the presence of additives comprising guanidine derivatives. Improvements in physical properties such as air flow, dimensional stability, tensile, tear, elongation and foam hardness is observed when these additives are present in polyurethane formulations. In addition, these additives can minimize polymer degradation under humid ageing conditions resulting in foam products with better mechanical properties.
摘要翻译： 公开了聚氨酯泡沫组合物和制备柔性聚氨酯泡沫体的方法。 在包含胍衍生物的添加剂的存在下生产聚氨酯泡沫。 当这些添加剂存在于聚氨酯配方中时，观察到物理性能如气流，尺寸稳定性，拉伸，撕裂，伸长率和泡沫硬度的改善。 此外，这些添加剂可以在潮湿老化条件下使聚合物降解最小化，从而产生具有更好机械性能的泡沫产品。
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9.发明申请公开(公告)号：US20130065978A1
公开(公告)日：2013-03-14
申请号：US13534171
申请日：2012-06-27
CPC分类号： C08G18/6696 , C08G18/3838 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08J9/0028 , C08J2205/06 , C08J2375/04 , C08K5/31 , C08K5/3155 , C08L75/04
摘要： Polyurethane foam compositions and processes to make flexible polyurethane foams are disclosed. Polyurethane foam is produced in the presence of additives comprising guanidine derivatives. Improvements in physical properties such as air flow, dimensional stability, tensile, tear, elongation and foam hardness is observed when these additives are present in polyurethane formulations. In addition, these additives can minimize polymer degradation under humid ageing conditions resulting in foam products with better mechanical properties.
摘要翻译： 公开了聚氨酯泡沫组合物和制备柔性聚氨酯泡沫体的方法。 在包含胍衍生物的添加剂的存在下生产聚氨酯泡沫。 当这些添加剂存在于聚氨酯配方中时，观察到物理性能如气流，尺寸稳定性，拉伸，撕裂，伸长率和泡沫硬度的改善。 此外，这些添加剂可以在潮湿老化条件下使聚合物降解最小化，从而产生具有更好机械性能的泡沫产品。
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公开(公告)号：US10106638B2
公开(公告)日：2018-10-23
申请号：US13556334
申请日：2012-07-24
IPC分类号： C08G18/18 , C08G18/48 , C08G18/76 , C08G101/00
摘要： This disclosure is directed to make low density and low amine emissions water blown polyurethane foams using a reactive catalyst composition. The method is particularly useful in the preparation of full water blown, low density polyurethane foams having a density in the range of about 6 to about 16 kg/m3. A catalyst composition comprising at least one non-emissive amine catalyst and tetraalkyl guanidine, the method of employing the catalyst composition and a formulation comprising the catalyst composition are disclosed.
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