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    Low temperature oxyiodination of aromatic compounds
    83.
    发明授权
    Low temperature oxyiodination of aromatic compounds 失效
    芳香族化合物的低温氧碘化

    公开(公告)号：US4778939A

    公开(公告)日：1988-10-18

    申请号：US29896

    申请日：1987-03-25

    Applicant: Gerald C. Tustin ,  Mark Rule

    Inventor： Gerald C. Tustin ,  Mark Rule

    IPC: C07B39/00 ,  C07C17/156 ,  C07C17/15

    CPC classification number: C07B39/00 ,  C07C17/156

    Abstract: The invention relates to a process for iodinating an aromatic compound which comprises reacting iodine and the aromatic compound over a non-acid catalyst, wherein the catalyst has been contacted with an alkali or alkaline earth metal salt, with a source of iodine and a source of molecular oxygen.

    Abstract translation: 本发明涉及一种芳族化合物的碘化方法，其包括在非酸催化剂上使碘和芳族化合物反应，其中催化剂已经与碱金属盐或碱土金属盐接触，得到碘源， 分子氧。

    Method to render surfaces water repellent
    86.
    发明授权
    Method to render surfaces water repellent 有权
    使表面防水的方法

    公开(公告)号：US08221533B2

    公开(公告)日：2012-07-17

    申请号：US13177035

    申请日：2011-07-06

    Applicant: Mark Rule ,  Harry Harshaw

    Inventor： Mark Rule ,  Harry Harshaw

    IPC: C04B41/46 ,  C04B41/47 ,  C04B103/65 ,  C09D5/00 ,  C09K3/18

    CPC classification number: C04B41/46 ,  C04B2111/27 ,  C04B41/502 ,  C04B2103/0094

    Abstract: A method to render stone, ceramic, or cementitious structures water repellent is disclosed. The method includes the step of contacting the stone, ceramic, or cementitious structures with an alkylphosphonic acid. The alkylphosphonic acid can be dispersed in an aqueous medium and can be at least partially neutralized with ammonia, an amine, or a basic alkali salt.

    Abstract translation: 公开了一种提供石材，陶瓷或水泥结构防水剂的方法。 该方法包括使石头，陶瓷或水泥结构与烷基膦酸接触的步骤。 烷基膦酸可以分散在水性介质中，并且可以用氨，胺或碱性碱盐至少部分中和。

    SCAVENGING OXYGEN
    87.
    发明申请
    SCAVENGING OXYGEN 有权

    公开(公告)号：US20120114529A1

    公开(公告)日：2012-05-10

    申请号：US13263803

    申请日：2010-04-08

    Applicant: Adrian John Carmichael ,  Andrew Stuart Ovenrend ,  Mark Rule ,  Ronald James Valus ,  Christine Leeming ,  Steven Burgess Tattum

    Inventor： Adrian John Carmichael ,  Andrew Stuart Ovenrend ,  Mark Rule ,  Ronald James Valus ,  Christine Leeming ,  Steven Burgess Tattum

    IPC: G05B1/00 ,  B23P11/00

    CPC classification number: B65D51/244 ,  A23L2/42 ,  A23L3/3436 ,  A23V2002/00 ,  B65D81/266 ,  Y02E60/36 ,  Y10T29/49826 ,  A23V2200/10 ,  A23V2250/12

    Abstract: A closure (40) includes a body (42) with a screw threaded portion (44) for engaging the closure with a container, for example a bottle. Inwards of portion (44) is a liner (46) comprising a hydrogen generating device, wherein the liner includes one layer (48) which incorporates a hydride dispersed in a polymeric matrix and, on opposite sides of layer (48) are arranged PET layers (50, 52). Layer (50) is arranged to act as a control layer to control the rate of passage of water vapour from the beverage in the container to the hydride containing layer (48) and thereby control generation of hydrogen by the hydrogen generating device. In use, water vapour passes through layer (50) and contacts the hydride associated with layer (48) which results in production of molecular hydrogen which combines with oxygen which may have entered a container with which the closure (40) is associated. Thereafter, a reaction between the hydrogen and oxygen takes place, catalysed by a catalyst associated with the container thereby to scavenge the oxygen.

    Abstract translation: 封闭件（40）包括具有螺纹部分（44）的主体（42），用于将封闭件与容器（例如瓶）接合。 部分（44）的向内是包括氢生成装置的衬套（46），其中衬垫包括一层（48），其包含分散在聚合物基体中的氢化物，并且在层（48）的相对侧上布置有PET层 （50,52）。 层（50）布置成用作控制层，以控制水蒸汽从容器中的饮料到含氢化物层（48）的通过速率，从而通过氢气产生装置控制氢的产生。 在使用中，水蒸汽穿过层（50）并与与层（48）相关联的氢化物接触，导致生成分子氢，其与可能已经进入封闭物（40）的容器进入的氧气结合。 此后，通过与容器相关联的催化剂催化氢和氧之间的反应，从而清除氧气。

    SCAVENGING OXYGEN
    88.
    发明申请
    SCAVENGING OXYGEN 有权

    公开(公告)号：US20100028499A1

    公开(公告)日：2010-02-04

    申请号：US12524402

    申请日：2008-01-24

    Applicant: Mark Rule ,  Ronald J. Valus ,  Steven Burgess Tattum

    Inventor： Mark Rule ,  Ronald J. Valus ,  Steven Burgess Tattum

    IPC: B65D85/72 ,  C01B3/02 ,  A23L3/00 ,  B01J19/00

    CPC classification number: B65D81/26 ,  A23L3/3436 ,  B65D51/244 ,  B65D81/266 ,  C01B3/065 ,  C08K3/014 ,  C08K3/10 ,  C08K5/098 ,  Y02E60/362

    Abstract: A container (22) includes a shell (24) made from a polymer, for example PET, and incorporating a catalyst, for example a palladium catalyst. A closure (40) incorporates a plug which includes a source of hydrogen, for example a hydride. In use, with container (22) including a beverage and closure (40) in position, the headspace in the container will be saturated with water vapor. This vapor contacts the hydride associated with plug (42) and as a result the hydride produces molecular hydrogen which migrates into the polymer matrix of shell (24) and combines with oxygen which may have entered the container through its permeable walls. A reaction between the hydrogen and oxygen takes place, catalysed by the catalyst, and water is produced. Thus, oxygen which may ingress the container is scavenged and the contents of the container are protected from oxidation.

    Abstract translation: 容器（22）包括由聚合物例如PET制成的壳体（24），并且加入催化剂，例如钯催化剂。 封闭件（40）包括包括氢源（例如氢化物）的塞子。 在使用时，将包括饮料和封闭物（40）的容器（22）置于适当位置，容器中的顶部空间将被水蒸气饱和。 该蒸汽接触与塞子（42）相关联的氢化物，结果氢化物产生迁移到壳体（24）的聚合物基质中的分子氢并与可能通过其可渗透壁进入容器的氧气结合。 氢和氧之间发生反应，催化剂催化，产生水。 因此，可能进入容器的氧气被清除，容器的内容物被保护免受氧化。

    Metal phosphonates and related nanocomposites
    89.
    发明申请
    Metal phosphonates and related nanocomposites 失效
    金属膦酸盐及相关纳米复合材料

    公开(公告)号：US20050239938A1

    公开(公告)日：2005-10-27

    申请号：US11110269

    申请日：2005-04-20

    Applicant: Mark Rule

    Inventor： Mark Rule

    IPC: C08K3/32 ,  C08K7/00

    CPC classification number: C07F9/3808 ,  C07F9/3834 ,  C07F9/3882 ,  C08K3/32 ,  C08K5/0091 ,  C08K5/101 ,  C08K5/5317 ,  C08K7/00 ,  C08L67/02

    Abstract: Compositions comprising a polymer and an exfoliated metal phosphonate are provided. Processes for making such polymer compositions and articles formed from such polymer compositions are also provided. Compositions according to the invention are useful in polymer applications in which barrier properties are of concern, such as in plastic food and beverage containers.

    Abstract translation: 提供了包含聚合物和剥离的金属膦酸酯的组合物。 还提供了制备由这种聚合物组合物形成的聚合物组合物和制品的方法。 根据本发明的组合物可用于其中涉及阻隔性质的聚合物应用中，例如在塑料食品和饮料容器中。

    Multilayer polymeric/inorganic oxide structure with top coat for enhanced gas or vapor barrier and method for making same
    90.
    发明授权
    Multilayer polymeric/inorganic oxide structure with top coat for enhanced gas or vapor barrier and method for making same 失效
    多层聚合物/无机氧化物结构，具有用于增强气体或蒸汽阻挡层的顶涂层及其制造方法

    公开(公告)号：US06808753B2

    公开(公告)日：2004-10-26

    申请号：US10664292

    申请日：2003-09-17

    Applicant: Mark Rule ,  Yu Shi ,  Thomas Gebele ,  Helmut Grimm ,  Elisabeth Budke

    Inventor： Mark Rule ,  Yu Shi ,  Thomas Gebele ,  Helmut Grimm ,  Elisabeth Budke

    IPC: B05D136

    CPC classification number: C08J7/045 ,  B65D1/0215 ,  Y10T428/1352 ,  Y10T428/1379 ,  Y10T428/1383 ,  Y10T428/139 ,  Y10T428/1393

    Abstract: The coated multilayer structure comprising a polymeric base layer, an inorganic oxide gas barrier layer on a surface of the polymeric base layer, and a top coat on the inorganic oxide gas barrier layer, the top coat comprising a soluble compound capable of reducing the permeability of the multilayer structure to gas or vapor. A method for enhancing the gas or vapor barrier properties of a multilayer polymeric/inorganic oxide structure is also disclosed. According to one embodiment, SiOx coated polyethylene terephthalate containers are coated with a gas or vapor barrier enhancing top coat.

    Abstract translation: 该涂覆的多层结构包括聚合物基层，聚合物基层的表面上的无机氧化物气体阻隔层和无机氧化物气体阻隔层上的顶涂层，该顶涂层包含能够降低渗透性的可溶性化合物 多层结构为气体或蒸汽。 还公开了一种用于增强多层聚合物/无机氧化物结构的气体或蒸气阻隔性能的方法。 根据一个实施方案，SiO x涂覆的聚对苯二甲酸乙二醇酯容器涂覆有气体或蒸气阻隔增强顶涂层。

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