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公开(公告)号：US20040179956A1
公开(公告)日：2004-09-16
申请号：US10798015
申请日：2004-03-11
发明人： Takao Tsuda , Motonori Munesue
IPC分类号： F04B039/00
CPC分类号： F04B19/24 , G01N2030/326
摘要： The liquid pump has a pressure vessel with end-openings for hermetically holding liquid therein. The liquid flows from one of the end-openings to the other end-opening by utilizing a difference in a coefficient of thermal expansion of the pressure vessel and the liquid caused by heating or cooling the pressure vessel and the liquid together. The pressure vessel is a tube having an inner diameter of about 0.5 mm or less and a length of about 10 m or more.
摘要翻译： 液体泵具有压力容器，该压力容器具有用于在其中气密保持液体的端部开口。 利用由压力容器和液体加热或冷却而导致的压力容器和液体的热膨胀系数的差异，液体从一个端部开口流到另一个端部开口。 压力容器是具有约0.5mm或更小的内径和约10μm或更大的长度的管。
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公开(公告)号：US20030189001A1
公开(公告)日：2003-10-09
申请号：US10119132
申请日：2002-04-08
发明人： Takao Tsuda , Shinya Kitagawa , Motonori Munesue
IPC分类号： B01D015/08
CPC分类号： B01J20/286 , B01J20/28054 , B01J20/28097 , B01J20/282 , B01J2220/54 , B01J2220/84 , G01N30/52 , G01N30/6078 , G01N2030/525 , G01N2030/567
摘要： In an open capillary column, a stationary phase is formed on the inner wall of a capillary tube. This stationary phase comprises a number of pores on the surface of the capillary tube, and each of pore has an expanded hollow in the stationary phase. A manufacturing method of an open capillary column comprises the steps of giving alkaline treatment to an inner wall of an open capillary tube, applying one of oligo silica, oligo zirconia and oligo titania on the inner wall, filling the open capillary tube with alkaline solution to form one of a silica layer, a zirconia layer and titania layer, discharging the alkaline solution and heat-treating the capillary tube to form a base of a stationary phase. The open capillary column of the present invention comprises a stationary phase having a very large surface area. It is useful for a separation analysis field such as liquid chromatography and electrochromatography.
摘要翻译： 在开放的毛细管柱中，在毛细管的内壁上形成固定相。 该固定相包括毛细管表面上的多个孔，并且每个孔在固定相中具有膨胀的中空。 开放毛细管柱的制造方法包括以下步骤：对开放毛细管的内壁进行碱处理，在内壁上施加低氧二氧化硅，低氧二氧化锆和低氧二氧化钛之一，用碱性溶液填充开放的毛细管， 形成二氧化硅层，氧化锆层和二氧化钛层之一，排出碱溶液并热处理毛细管以形成固定相的碱。 本发明的开放毛细管柱包括具有非常大的表面积的固定相。 它对于分离分析领域如液相色谱和电色谱是有用的。
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公开(公告)号：US20030188575A1
公开(公告)日：2003-10-09
申请号：US10119131
申请日：2002-04-08
发明人： Takao Tsuda , Motonori Munesue
IPC分类号： G01F001/68
CPC分类号： G01N30/32 , G01F1/7084 , G01N2030/324
摘要： A change in physical properties of a fluid within an open tube which is caused by heating an arbitrary portion in the open tube by heating means is detected by using a detector disposed with a predetermined spacing from the arbitrary portion, thereby measuring the flow in the open tube. The present invention provides a method for measuring flow within an open tube, in which a mechanical error and contamination of a passage do not occur, as a method for measuring flow within an open tube having a very small diameter provided for the separation analysis field and chemosynthesis field.
摘要翻译： 通过使用与任意部分隔开预定间隔设置的检测器来检测由加热装置加热开放管中的任意部分而引起的开放管内的流体的物理性质的变化，由此测量开放的流量 管。 本发明提供了一种用于测量开放管内的流动的方法，其中不发生机械误差和通道的污染，作为用于测量具有用于分离分析场的非常小直径的开管内的流动的方法，以及 化学合成领域。
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