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公开(公告)号：US4816136A
公开(公告)日：1989-03-28
申请号：US15438
申请日：1987-02-17
Applicant: David E. Allan , Don E. Blaser
Inventor： David E. Allan , Don E. Blaser
Abstract: A fluid coking process is provided in which a fresh carbonaceous feed is coked in a transfer line first coking zone positioned in a fluidized bed second coking zone. A heavy oil coker product is recycled to the fluidized bed second coking zone maintained at a lower temperature than the first coking zone. This process permits low severity coking of the fresh carbonceous feed and higher severity coking of the recycle oil, thereby minimizing conversion to coke and gas and increasing yield of normally liquid products.
Abstract translation: 提供了一种流体焦化方法，其中新鲜碳质进料在位于流化床第二焦化区中的输送管线第一焦化区中焦化。 将重油焦化产物再循环至维持在比第一焦化区低的温度的流化床第二焦化区。 该方法允许新鲜碳源进料的低浓度焦化和循环油的较高严重性焦化，从而最小化转化为焦炭和气体并提高常规液体产物的产率。
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公开(公告)号：US4519898A
公开(公告)日：1985-05-28
申请号：US496570
申请日：1983-05-20
Applicant: David E. Allan
Inventor： David E. Allan
CPC classification number: C10B55/00
Abstract: A delayed coking process is conducted at a relatively low temperature with the introduction of a gas into the coking drum to strip volatile matter from the coke product and to form coke containing 6 to 12 weight percent volatile matter. Low temperature delayed coking decreases the amount of coke yield, calculated on a volatile-free basis, and increases liquid yield.
Abstract translation: 在相对较低的温度下进行延迟焦化工艺，其中将气体引入焦化鼓中以从焦炭产物中除去挥发性物质，并形成含有6至12重量％挥发性物质的焦炭。 低温延迟焦化降低焦炭产量，以无挥发为基础计算，并提高液体产率。
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公开(公告)号：US4501654A
公开(公告)日：1985-02-26
申请号：US594851
申请日：1984-03-29
Applicant: David E. Allan
Inventor： David E. Allan
CPC classification number: C10B57/045 , C10G9/005
Abstract: A delayed coking process is provided in which the fresh hydrocarbonaceous oil feed is divided into at least two streams. One stream is introduced directly into the preheating zone of the coking zone and one stream is introduced into the coker product fractionator. The fractionator bottoms fraction is recycled to the preheating zone as a separate stream from the fresh feed stream. The separate preheated fresh feed stream is introduced into the top of the coking zone and the preheated recycled fractionator bottoms fraction is introduced into the bottom of the coking zone. The given fresh feed splitting configuration permits decreasing the recycle rate of the heavy coker product and increasing liquid yield while the top and bottom feeding to the coking zone permit subjecting the given streams to different severity of coking.
Abstract translation: 提供了一种延迟焦化方法，其中新鲜含烃油进料分成至少两股。 将一条流直接引入焦化区的预热区，一条流被引入焦化器产物分馏器。 分馏塔塔底馏分作为与新鲜进料流分离的流循环至预热区。 将单独的预热的新鲜进料流引入焦化区的顶部，并将预热的再循环分馏塔塔底馏分引入焦化区的底部。 给定的新鲜进料分离配置允许降低重焦化产物的再循环速率并提高液体产率，而向焦化区的顶部和底部进料允许使给定流具有不同的焦化严重性。
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公开(公告)号：US4492625A
公开(公告)日：1985-01-08
申请号：US552625
申请日：1983-11-17
Applicant: David E. Allan
Inventor： David E. Allan
CPC classification number: C10B57/045 , C10G9/005
Abstract: A delayed coking process is provided in which the fresh hydrocarbonaceous oil feed is divided into at least two streams. One stream is introduced directly into the preheating zone of the coking zone and one stream is introduced into the coker product fractionator. The fractionator bottoms fraction is recycled to the preheating zone. The given fresh feed splitting configuration permits decreasing the recycle rate of the heavy coker product and increasing liquid yield.
Abstract translation: 提供了一种延迟焦化方法，其中新鲜含烃油进料分成至少两股。 将一条流直接引入焦化区的预热区，一条流被引入焦化器产物分馏器。 分馏塔塔底馏分再循环到预热区。 给定的新鲜进料分离配置允许降低重型焦化产物的再循环速率并提高液体产率。
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公开(公告)号：US4096199A
公开(公告)日：1978-06-20
申请号：US772636
申请日：1977-02-28
Applicant: Donald L. Green , William C. Behrmann , David E. Allan
Inventor： Donald L. Green , William C. Behrmann , David E. Allan
CPC classification number: C07C2/62 , C07C2527/03 , Y02P20/584
Abstract: A process for regenerating an alkylation catalyst comprising fluorosulfuric acid, said catalyst being at least partially deactivated, which comprises:(1) contacting at least a portion of the fluorosulfuric acid with water to form an acid-water mixture, thereby converting at least a portion of the fluorosulfuric acid therein to hydrogen fluoride and sulfuric acid;(2) removing at least a portion of the hydrogen fluoride from said acid-water mixture formed in step (1) by contacting same with a stripping agent to form a gaseous phase containing hydrogen fluoride and said stripping agent and a liquid phase containing sulfuric acid and sludge;(3) cooling the gas phase formed in step (2) to a temperature sufficient to form a mixed phase comprising at least a liquid phase containing hydrogen fluoride; and(4) treating the mixed phase formed in step (3) with sulfur trioxide under substantially liquid phase conditions so as to regenerate the fluorosulfuric acid. In a preferred embodiment, at least a portion of the regenerated fluorosulfuric acid is recycled to the alkylation zone for use as an alkylation catalyst therein.
Abstract translation: 一种用于再生包含氟代硫酸的烷基化催化剂的方法，所述催化剂至少部分失活，其包括：
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Patent Agency Ranking
公开(公告)号：US4151070A
公开(公告)日：1979-04-24
申请号：US862341
申请日：1977-12-20
Applicant: David E. Allan , William E. Lewis
Inventor： David E. Allan , William E. Lewis
Abstract: A staged hydrocarbon hydroconversion process is provided in which a portion of the product boiling up to an atmospheric pressure distillation cut point of about 1050.degree. F. is removed between the stages and in which the first stage is operated at lower severity than the second stage.
Abstract translation: 提供了分阶段的烃加氢转化方法，其中沸腾至大约1050°F的大气压蒸馏馏分的产物的一部分在阶段之间被除去，其中第一阶段以比第二阶段更低的严重程度运行。
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公开(公告)号：US4137149A
公开(公告)日：1979-01-30
申请号：US810913
申请日：1977-06-29
Applicant: David E. Allan , William E. Lewis , William J. Metrailer
Inventor： David E. Allan , William E. Lewis , William J. Metrailer
Abstract: The liquid product of a slurry hydrogen treating zone is separated into fractions in the same separation zone used to obtain the heavy hydrocarbonaceous oil fraction used as feed for the hydrogen treating zone. A separate portion of coarser solids is withdrawn from the hydrogen treating zone.
Abstract translation: 将浆液氢处理区的液体产物在用于获得用作氢处理区的进料的重质烃油馏分的相同分离区中分离成馏分。 从氢处理区抽出较粗的固体的单独部分。
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8.发明授权Feed injection method to prevent coking on the walls of transfer line reactors 失效进料注射方法，以防止转运线反应器壁上的焦化
公开(公告)号：US4534851A
公开(公告)日：1985-08-13
申请号：US500408
申请日：1983-06-02
Applicant: David E. Allan , Charles H. Martinez
Inventor： David E. Allan , Charles H. Martinez
CPC classification number: C10G9/32 , B01J19/0026 , C10G11/18
Abstract: A hydrocarbon feed injection method is provided in which concentric inlet conduits carry hydrocarbon liquid and steam. Small nozzles located on the outer steam-carrying conduit discharge steam in the direction of the inner wall of the transfer line reactor to protect the inner wall from carbonaceous deposits. The hydrocarbon feed nozzles are staged along a line parallel to the longitudinal axis of the transfer line.
Abstract translation: 提供了一种烃进料注入方法，其中同心入口导管携带烃液体和蒸汽。 位于外部蒸汽输送管道上的小喷嘴沿着输送管线反应器的内壁方向排放蒸汽，以保护内壁免受含碳沉积物的侵害。 碳氢化合物进料喷嘴沿着平行于输送管线纵轴的直线分段。
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9.发明授权
公开(公告)号：US4501820A
公开(公告)日：1985-02-26
申请号：US518026
申请日：1983-07-28
Applicant: David E. Allan , Byron V. Molstedt , Raam R. Mohan
Inventor： David E. Allan , Byron V. Molstedt , Raam R. Mohan
CPC classification number: C10G11/04 , B01J23/92 , Y10S502/516
Abstract: A tungsten-containing catalyst associated with coke containing vanadium and nickel is recovered by a method which includes steam gasification, low temperature burning to remove at least a portion of the coke and selective extraction of the nickel and vanadium.
Abstract translation: 通过包括蒸汽气化，低温燃烧以除去至少一部分焦炭并选择性提取镍和钒的方法回收与含有钒和镍的焦炭相关的含钨催化剂。
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公开(公告)号：US4075258A
公开(公告)日：1978-02-21
申请号：US708058
申请日：1976-07-23
Applicant: Robert H. Caulk , David E. Allan
Inventor： Robert H. Caulk , David E. Allan
CPC classification number: B01F7/00466 , B01J19/0066 , C07C2/60 , C07C2/62 , C07C2527/054 , C07C2527/1206 , C07C2527/1213 , C07C2527/126 , Y10S585/922 , Y10S585/955
Abstract: An improved process for the production of higher octane number products by the high intensity mixing of alkylation media, or media wherein olefins are alkylated by the addition thereto of isobutane. The alkylation reaction is conducted by contact between the reactants, which constitute a hydrocarbon phase, and an acid catalyst which constitutes an aqueous phase, the reactants being dispersed as an emulsion. It is found that when stirring an alkylation medium at above a certain threshold fluid mixing intensity, a C.sub.6 + Motor Octane Number (MON) improvement ranging from about 0.5, and generally from about 0.5 to about 3.3, can be obtained by alkylating olefins with isobutane at high acid concentration while maintaining an acid soluble oil content ranging to about 3 percent, preferably from about 0.1 to about 3 percent, and more preferably from about 0.5 to about 2.5 percent, based on the weight of the reaction mixture, exclusive of the hydrocarbon phase. The alkylation is suitably conducted at acid strengths ranging from about 98 to about 88 percent, preferably from about 98 to about 94, based on the weight of the aqueous phase.
Abstract translation: 通过烷基化介质的高强度混合生产高辛烷值产物的改进方法，或其中通过加入异丁烷将烯烃烷基化的介质。 烷基化反应通过构成烃相的反应物和构成水相的酸催化剂之间的接触进行，反应物作为乳液分散。 发现当烷基化介质在高于某一阈值流体混合强度下搅拌时，C6 +马达辛烷值（MON）的改进范围为约0.5，通常为约0.5至约3.3，可以通过用异丁烷将烯烃烷基化 高酸浓度，同时保持基于反应混合物重量的约3％，优选约0.1％至约3％，更优选约0.5至约2.5％的酸溶性油含量，不包括烃相 。 基于水相的重量，烷基化适合在约98至约88％，优选约98至约94的酸强度下进行。
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