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公开(公告)号:US20120048064A1
公开(公告)日:2012-03-01
申请号:US13220494
申请日:2011-08-29
申请人: Michael Kasper , Emilie Bekaert , Chistian Dreer , Peter Axmann
发明人: Michael Kasper , Emilie Bekaert , Chistian Dreer , Peter Axmann
CPC分类号: B22F9/305 , B01J23/745 , B01J23/75 , B01J23/755 , B01J35/0013 , B01J37/086 , B22F1/0018 , B22F1/02 , B82Y30/00 , C22B5/20
摘要: A production complex is used for producing nano-particles of metal from volatile moieties like metal carbonyls in a flow through reactor. The carbonyls are fed into the reactor through a first feeder, which is a moiety feeder. The moiety, a mixture of metal carbonyl and a bearer fluid, is entering the reactor in a vaporized state. Decomposition of carbonyls is carried out by controlled ambient temperature within the reactor, which is provided by means of a heated inert gas through a heating feed line of the production complex into a second feeder of the reactor, when the production complex is in an operational state. Gases like nitrogen are heated up in units of the production complex as heating feed. The gas supply unit in pre-operational state is used to provide inert gas for cleaning a carbonyl feed line in order to improve the quality of nano-particles of metal produced.
摘要翻译: 生产复合物用于从流动反应器中的挥发性部分如金属羰基化物制备金属纳米颗粒。 羰基通过作为部分进料器的第一进料器进料至反应器中。 该部分是金属羰基和承载流体的混合物,在蒸发状态下进入反应器。 羰基化合物的分解是通过在反应器内的受控环境温度进行的,当生产复合物处于操作状态时,其通过加热的惰性气体通过生产复合物的加热供料管线提供给反应器的第二进料器 。 像氮气这样的气体以加热饲料为单位被加热。 在操作状态下的气体供应单元用于提供用于清洁羰基进料管线的惰性气体,以提高生产的金属的纳米颗粒的质量。
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2.
公开(公告)号:US08986602B2
公开(公告)日:2015-03-24
申请号:US13220392
申请日:2011-08-29
申请人: Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
发明人: Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
CPC分类号: B22F9/305 , B01J4/002 , B01J19/26 , B01J2219/00006 , B01J2219/00119 , B22F1/0018 , B22F2999/00 , B82Y30/00 , C22B5/20 , C22C19/03 , C22C21/00 , B22F2203/00
摘要: The reactor is used for producing nano-particles of metal from volatile moieties in flow through mode. The reactor comprises at least a first feeder and a second feeder on one end of the vessel. The first feeder feeds the moiety in the form of an educt fluid into the reactor. This fluid is a mixture of metal moieties and a bearer fluid, entering the reactor in a vaporized state, in which the bearer fluid is used as a carrier gas. The second feeder is used as a radiator means to heat up the educt fluid within the reactor. By providing the heating fluid through the second feeder control over some environmental conditions like ambient temperature within the reactor is achieved and dissociation of the metal moieties under such controlled conditions leads to quantitative production of selected nano-particle morphologies.
摘要翻译: 该反应器用于在流动模式下从挥发性部分制备金属的纳米颗粒。 反应器包括至少第一进料器和在容器的一端上的第二进料器。 第一个进料器将部分以喷射流体的形式进料到反应器中。 该流体是金属部分和承载流体的混合物,其以汽化状态进入反应器,其中承载流体用作载气。 第二进料器用作加热反应器内的流出液的散热器装置。 通过在某些环境条件下提供加热流体,例如反应器内的环境温度,并且在这种受控条件下金属部分的解离导致选定的纳米颗粒形态的定量生产。
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3.
公开(公告)号:US20120055285A1
公开(公告)日:2012-03-08
申请号:US13220392
申请日:2011-08-29
申请人: Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
发明人: Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
CPC分类号: B22F9/305 , B01J4/002 , B01J19/26 , B01J2219/00006 , B01J2219/00119 , B22F1/0018 , B22F2999/00 , B82Y30/00 , C22B5/20 , C22C19/03 , C22C21/00 , B22F2203/00
摘要: The reactor is used for producing nano-particles of metal from volatile moieties in flow through mode. The reactor comprises at least a first feeder and a second feeder on one end of the vessel. The first feeder feeds the moiety in the form of an educt fluid into the reactor. This fluid is a mixture of metal moieties and a bearer fluid, entering the reactor in a vaporized state, in which the bearer fluid is used as a carrier gas. The second feeder is used as a radiator means to heat up the educt fluid within the reactor. By providing the heating fluid through the second feeder control over some environmental conditions like ambient temperature within the reactor is achieved and dissociation of the metal moieties under such controlled conditions leads to quantitative production of selected nano-particle morphologies.
摘要翻译: 该反应器用于在流动模式下从挥发性部分制备金属的纳米颗粒。 反应器包括至少第一进料器和在容器的一端上的第二进料器。 第一个进料器将部分以喷射流体的形式进料到反应器中。 该流体是金属部分和承载流体的混合物,其以汽化状态进入反应器,其中承载流体用作载气。 第二进料器用作加热反应器内的流出液的散热器装置。 通过在某些环境条件下提供加热流体,例如反应器内的环境温度,并且在这种受控条件下金属部分的解离导致选定的纳米颗粒形态的定量生产。
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