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公开(公告)号：US08986602B2
公开(公告)日：2015-03-24
申请号：US13220392
申请日：2011-08-29
申请人： Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
发明人： Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
CPC分类号： B22F9/305 , B01J4/002 , B01J19/26 , B01J2219/00006 , B01J2219/00119 , B22F1/0018 , B22F2999/00 , B82Y30/00 , C22B5/20 , C22C19/03 , C22C21/00 , B22F2203/00
摘要： The reactor is used for producing nano-particles of metal from volatile moieties in flow through mode. The reactor comprises at least a first feeder and a second feeder on one end of the vessel. The first feeder feeds the moiety in the form of an educt fluid into the reactor. This fluid is a mixture of metal moieties and a bearer fluid, entering the reactor in a vaporized state, in which the bearer fluid is used as a carrier gas. The second feeder is used as a radiator means to heat up the educt fluid within the reactor. By providing the heating fluid through the second feeder control over some environmental conditions like ambient temperature within the reactor is achieved and dissociation of the metal moieties under such controlled conditions leads to quantitative production of selected nano-particle morphologies.
摘要翻译： 该反应器用于在流动模式下从挥发性部分制备金属的纳米颗粒。 反应器包括至少第一进料器和在容器的一端上的第二进料器。 第一个进料器将部分以喷射流体的形式进料到反应器中。 该流体是金属部分和承载流体的混合物，其以汽化状态进入反应器，其中承载流体用作载气。 第二进料器用作加热反应器内的流出液的散热器装置。 通过在某些环境条件下提供加热流体，例如反应器内的环境温度，并且在这种受控条件下金属部分的解离导致选定的纳米颗粒形态的定量生产。
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2.发明申请Positive active electrode material for lithium secondary battery, process for preparing the same and lithium secondary battery 审中-公开锂二次电池正极活性电极材料及其制备方法以及锂二次电池公开(公告)号：US20120183855A1
公开(公告)日：2012-07-19
申请号：US13498790
申请日：2010-09-27
CPC分类号： H01M4/485 , H01M4/505 , H01M4/525 , H01M10/0525
摘要： Positive active electrode material for lithium secondary batteries comprising a mixed oxide represented by the general formula LivNiwMnxCoyAlzO2 wherein 0.9≦v≦1.2, 0.34≦w≦0.49, 0.34≦x≦0.42, 0.08≦y≦0.20, 0.03≦z≦0.05, 0.8≦w/x≦1.8, −0.08≦w−x≦0.22, 0.12≦y+z≦0.25 and w+x+y+z=1.
摘要翻译： 包含由通式LivNiwMnxCoyAlzO2表示的混合氧化物的锂二次电池的正极活性电极材料，其中0.9和nlE; v和nlE; 1.2,0.34和nlE; w和nlE; 0.49,0.34和n1E; x和nlE; 0.42,0.08和n1E; y和n1E; 0.20,0.03＆ z + nlE; 0.05,0.8＆nlE; w / x和nlE; 1.8,0.08＆nlE; w-x和nlE; 0.22,0.12＆nlE; y + z＆nlE; 0.25和w + x + y + z = 1。
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公开(公告)号：US20090081454A1
公开(公告)日：2009-03-26
申请号：US11922753
申请日：2006-07-07
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C01B2202/06 , C01B2202/36 , Y10T428/2918
摘要： The invention relates to carbon nanoparticles from fibers or tubes or combinations thereof, which have the morphology of macroscopic, spherical and/or spheroid secondary agglomerates, separated from each other. The invention also relates to a method for producing carbon nanoparticles by a CVD method using nanoporous catalyst particles having a spherical and/or spheroid secondary structure and comprising nanoparticulate metals and/or metal oxides or the precursors thereof as the catalytically active components. The inventive carbon nanoparticles are suitable for use in adsorbents, additives or active materials in energy accumulating systems, in supercapacitors, as filtering media, as catalysts or supports for catalysts, as sensors or as substrate for sensors, as additives for polymers, ceramics, metals and metal alloys, glasses, textiles and composite materials.
摘要翻译： 本发明涉及具有彼此分离的宏观，球形和/或球状二次附聚物形态的来自纤维或管的碳纳米颗粒或其组合。 本发明还涉及通过使用具有球形和/或球体二级结构并包含纳米颗粒金属和/或金属氧化物的纳米多孔催化剂颗粒或其前体作为催化活性组分的CVD方法制备碳纳米颗粒的方法。 本发明的碳纳米颗粒适用于能量积聚系统中的吸附剂，添加剂或活性材料，超级电容器，过滤介质，催化剂催化剂或载体，传感器或传感器基质，聚合物，陶瓷，金属添加剂 和金属合金，玻璃，纺织品和复合材料。
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4.发明授权Nickel mixed hydroxide, method for the producing the same, and the use thereof as a cathode material in alkaline batteries 失效镍混合氢氧化物，其制造方法及其在碱性电池中作为阴极材料的用途公开(公告)号：US06849208B1
公开(公告)日：2005-02-01
申请号：US09868995
申请日：1999-12-14
申请人： Viktor Stoller , Armin Olbrich , Juliane Meese-Marktscheffel , Margret Wohlfahrt-Mehrens , Peter Axmann , Herbert Dittrich , Sandra Ströbele
发明人： Viktor Stoller , Armin Olbrich , Juliane Meese-Marktscheffel , Margret Wohlfahrt-Mehrens , Peter Axmann , Herbert Dittrich , Sandra Ströbele
CPC分类号： C01G53/006 , C01G53/04 , C01P2002/52 , C01P2002/72 , C01P2004/03 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/40 , C01P2006/80 , H01M4/32 , H01M4/38 , H01M10/30
摘要： The invention relates to a nickel mixed hydroxide with Ni as the main element and with a layer structure, comprising at least one element Ma from the group comprising Fe, Cr, Co, Ti, Zr and Cu which is present in two different oxidation states which differ by one electron in terms of the number of outer electrons; at least one element Mb from the group comprising B, Al, Ga, In and RE (rare earth metals) present in the trivalent oxidation state; optionally at least one element Mc from the group comprising Mg, Ca, Sr, Ba and Zn present in the divalent oxidation state; apart from the hydroxide, at least one additional anion from the group comprising halides, carbonate, sulfate, oxalate, acetate, borate and phosphate in a quantity sufficient to preserve the electroneutrality of the mixed hydroxide; and water of hydration in a quantity which stabilizes the relevant structure of the mixed hydroxide.
摘要翻译： 本发明涉及以Ni为主要元素并具有层结构的镍混合氢氧化物，其包含至少一种元素Ma，所述组分包含Fe，Cr，Co，Ti，Zr和Cu，其以两种不同的氧化态存在， 在外电子数方面相差一电子; 来自包含以三价氧化态存在的B，Al，Ga，In和RE（稀土金属）的组中的至少一种元素Mb; 任选地，存在二价氧化态的包含Mg，Ca，Sr，Ba和Zn的组中的至少一种元素Mc; 除了氢氧化物外，还含有足以保持混合氢氧化物的电中性的量的卤代烃，碳酸盐，硫酸盐，草酸盐，乙酸盐，硼酸盐和磷酸盐的至少一种另外的阴离子; 和水合水，其量稳定了混合氢氧化物的相关结构。
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公开(公告)号：US20120048064A1
公开(公告)日：2012-03-01
申请号：US13220494
申请日：2011-08-29
申请人： Michael Kasper , Emilie Bekaert , Chistian Dreer , Peter Axmann
发明人： Michael Kasper , Emilie Bekaert , Chistian Dreer , Peter Axmann
CPC分类号： B22F9/305 , B01J23/745 , B01J23/75 , B01J23/755 , B01J35/0013 , B01J37/086 , B22F1/0018 , B22F1/02 , B82Y30/00 , C22B5/20
摘要： A production complex is used for producing nano-particles of metal from volatile moieties like metal carbonyls in a flow through reactor. The carbonyls are fed into the reactor through a first feeder, which is a moiety feeder. The moiety, a mixture of metal carbonyl and a bearer fluid, is entering the reactor in a vaporized state. Decomposition of carbonyls is carried out by controlled ambient temperature within the reactor, which is provided by means of a heated inert gas through a heating feed line of the production complex into a second feeder of the reactor, when the production complex is in an operational state. Gases like nitrogen are heated up in units of the production complex as heating feed. The gas supply unit in pre-operational state is used to provide inert gas for cleaning a carbonyl feed line in order to improve the quality of nano-particles of metal produced.
摘要翻译： 生产复合物用于从流动反应器中的挥发性部分如金属羰基化物制备金属纳米颗粒。 羰基通过作为部分进料器的第一进料器进料至反应器中。 该部分是金属羰基和承载流体的混合物，在蒸发状态下进入反应器。 羰基化合物的分解是通过在反应器内的受控环境温度进行的，当生产复合物处于操作状态时，其通过加热的惰性气体通过生产复合物的加热供料管线提供给反应器的第二进料器 。 像氮气这样的气体以加热饲料为单位被加热。 在操作状态下的气体供应单元用于提供用于清洁羰基进料管线的惰性气体，以提高生产的金属的纳米颗粒的质量。
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6.发明申请公开(公告)号：US20120055285A1
公开(公告)日：2012-03-08
申请号：US13220392
申请日：2011-08-29
申请人： Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
发明人： Robert Mercuri , Michael Kasper , Emilie Bekaert , Peter Axmann
CPC分类号： B22F9/305 , B01J4/002 , B01J19/26 , B01J2219/00006 , B01J2219/00119 , B22F1/0018 , B22F2999/00 , B82Y30/00 , C22B5/20 , C22C19/03 , C22C21/00 , B22F2203/00
摘要： The reactor is used for producing nano-particles of metal from volatile moieties in flow through mode. The reactor comprises at least a first feeder and a second feeder on one end of the vessel. The first feeder feeds the moiety in the form of an educt fluid into the reactor. This fluid is a mixture of metal moieties and a bearer fluid, entering the reactor in a vaporized state, in which the bearer fluid is used as a carrier gas. The second feeder is used as a radiator means to heat up the educt fluid within the reactor. By providing the heating fluid through the second feeder control over some environmental conditions like ambient temperature within the reactor is achieved and dissociation of the metal moieties under such controlled conditions leads to quantitative production of selected nano-particle morphologies.
摘要翻译： 该反应器用于在流动模式下从挥发性部分制备金属的纳米颗粒。 反应器包括至少第一进料器和在容器的一端上的第二进料器。 第一个进料器将部分以喷射流体的形式进料到反应器中。 该流体是金属部分和承载流体的混合物，其以汽化状态进入反应器，其中承载流体用作载气。 第二进料器用作加热反应器内的流出液的散热器装置。 通过在某些环境条件下提供加热流体，例如反应器内的环境温度，并且在这种受控条件下金属部分的解离导致选定的纳米颗粒形态的定量生产。
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7.发明申请MIXED OXIDE CONTAINING A LITHIUM MANGANESE SPINEL AND PROCESS FOR ITS PREPARATION 有权含有锰锰矿的混合氧化物及其制备方法公开(公告)号：US20110287319A1
公开(公告)日：2011-11-24
申请号：US12999376
申请日：2009-06-23
IPC分类号： H01M4/505
CPC分类号： H01M4/505 , C01B35/128 , C01G45/1242 , C01G51/54 , C01P2002/32 , C01P2002/52 , C01P2002/72 , C01P2004/03 , C01P2004/51 , C01P2004/52 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/13 , C01P2006/40 , C30B1/10 , C30B29/22 , H01M4/131 , H01M4/62 , H01M10/052 , H01M10/0525 , H01M2004/021 , H01M2004/028 , Y02E60/122
摘要： A mixed oxide containing a) a mixed-substituted lithium manganese spinel in which some of the manganese lattice sites are occupied by lithium ions and b) a boron-oxygen compound. Furthermore, a process for its preparation and the use of the mixed oxide as electrode material for lithium ion batteries.
摘要翻译： 一种混合氧化物，其包含a）混合取代的锂锰尖晶石，其中一些锰晶格点由锂离子占据，b）硼 - 氧化合物。 此外，其制备方法和使用混合氧化物作为锂离子电池的电极材料。
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公开(公告)号：US5670271A
公开(公告)日：1997-09-23
申请号：US551451
申请日：1995-11-01
申请人： Peter Axmann
发明人： Peter Axmann
摘要： The present invention relates to manganese-containing nickel(II) hydroxide powders, wherein at least 50 mole % of the manganese are present in the trivalent oxidation state, a process for the preparation of such powders and battery electrodes and batteries made therefrom.
摘要翻译： 本发明涉及含锰的镍（II）氢氧化物粉末，其中至少50摩尔％的锰以三价氧化态存在，制备这种粉末的方法和由其制成的电池电极和电池。
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9.发明授权Mixed oxide containing a lithium manganese spinel and process for its preparation 有权含有锂锰尖晶石的混合氧化物及其制备方法公开(公告)号：US09281522B2
公开(公告)日：2016-03-08
申请号：US12999376
申请日：2009-06-23
CPC分类号： H01M4/505 , C01B35/128 , C01G45/1242 , C01G51/54 , C01P2002/32 , C01P2002/52 , C01P2002/72 , C01P2004/03 , C01P2004/51 , C01P2004/52 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/13 , C01P2006/40 , C30B1/10 , C30B29/22 , H01M4/131 , H01M4/62 , H01M10/052 , H01M10/0525 , H01M2004/021 , H01M2004/028 , Y02E60/122
摘要： A mixed oxide containing a) a mixed-substituted lithium manganese spinel in which some of the manganese lattice sites are occupied by lithium ions and b) a boron-oxygen compound. Furthermore, a process for its preparation and the use of the mixed oxide as electrode material for lithium ion batteries.
摘要翻译： 一种混合氧化物，其包含a）混合取代的锂锰尖晶石，其中一些锰晶格点由锂离子占据，b）硼 - 氧化合物。 此外，其制备方法和使用混合氧化物作为锂离子电池的电极材料。
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10.发明授权
公开(公告)号：US5599436A
公开(公告)日：1997-02-04
申请号：US547802
申请日：1995-10-25
申请人： Peter Axmann
发明人： Peter Axmann
CPC分类号： C01G53/00 , H01M4/50 , H01M4/52 , C01P2006/40
摘要： The present invention relates to a process for the preparation of manganese(III)-containing nickel(II) hydroxide powders, more than 50 mole % of the manganese being present in the trivalent oxidation state, by co-precipitation of nickel(II) and manganese salt solutions with alkali liquors.
摘要翻译： 本发明涉及一种制备含有锰（III）的氢氧化镍（II）粉末的方法，其中超过50摩尔％的锰以三价氧化态存在，通过共沉淀镍（II）和 锰盐溶液与碱液。
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