Method and Apparatus for Producing Purified Methyl Isobutyl Ketone
    1.
    发明申请
    Method and Apparatus for Producing Purified Methyl Isobutyl Ketone 有权
    生产纯化甲基异丁基酮的方法和装置

    公开(公告)号:US20100222612A1

    公开(公告)日:2010-09-02

    申请号:US12086491

    申请日:2006-11-27

    IPC分类号: C07C45/82 B01D3/14

    摘要: This invention relates to a method of producing purified methyl isobutyl ketone (MIBK) comprising subjecting a feed stream containing MIBK and impurities to a first distillation procedure from which acetone is recovered and a bottom product containing MIBK and impurities is withdrawn. This bottom product is fed to a second distillation column, where a vapour overhead product is withdrawn, condensed and fed to an overhead liquid-liquid separator. Part of an organic phase from the overhead liquid-liquid separator is fed to the second distillation column and part is fed to a third distillation column. A vapour overhead product is withdrawn from the third column which is condensed in the same said condensor. The condensed product is fed to the same said overhead liquid-liquid separator, and purified MIBK is withdrawn from the third distillation column. This invention also relates to an apparatus used in such a method.

    摘要翻译: 本发明涉及一种生产纯化甲基异丁基酮(MIBK)的方法,包括使含有MIBK和杂质的进料流经历回收丙酮的第一蒸馏步骤,并且收集含有MIBK和杂质的底部产物。 将该底部产物进料至第二蒸馏塔,蒸馏塔顶产物被抽出,冷凝并送入塔顶液 - 液分离器。 将来自塔顶液 - 液分离器的有机相的一部分进料到第二蒸馏塔,并将一部分进料到第三蒸馏塔。 从第三塔取出蒸气塔顶产物,其在相同的所述冷凝器中冷凝。 将冷凝产物加入到相同的塔顶液 - 液分离器中,从第三蒸馏塔中取出纯化的MIBK。 本发明还涉及在这种方法中使用的装置。

    Method for extracting xenon
    2.
    发明授权
    Method for extracting xenon 失效
    氙气提取方法

    公开(公告)号:US06351970B1

    公开(公告)日:2002-03-05

    申请号:US09701240

    申请日:2001-02-22

    IPC分类号: F25J100

    摘要: The invention relates to a method for extracting xenon and eventually also krypton from a liquid oxygen (LOX) charge, as it accrues in a cryogenic air separation system (LZA) during a rectification of the air, mostly as a bottom product of a low-pressure, column, namely with xenon (Xe), krypton (Kr) and hydrocarbons (CxHy) in a small concentration and approximately 99 mol % oxygen (O2). According to the inventive method, the LOX charge is fed to a first column, the oxygen of the LOX charge is extensively removed by stripping with an inert gas, and is extracted in the top gas, whereas the inert gas is withdrawn in the form of a liquid from the bottom of the first column with little O2 and nearly the total mass of CxHy, Kr, Xe. According to the invention, the liquid discharge is fed to a second column without prior catalytic and/or adsorptive removal of CxHy. A Kr fraction is extracted as top gas of the second column, and an Xe fraction is withdrawn from the bottom of the second column. The method can be used in a device for extracting Xe and/or Kr in an air separation system (LZA). The device can be arranged in a transportable container.

    摘要翻译: 本发明涉及一种用于在空气整流期间在低温空气分离系统(LZA)中产生的从液氧(LOX)装料中提取氙并最终还氪的方法,主要作为低温空气分离系统的底部产物, 压力,柱,即氙(Xe),氪(Kr)和碳氢化合物(CxHy)在小浓度和约99mol%的氧气(O2)。 根据本发明的方法,将LOX装料进料到第一塔中,通过用惰性气体汽提来广泛地除去LOX装料的氧气,并在顶部气体中提取,而惰性气体以 来自第一列底部的液体几乎没有O2,几乎总C 6 H y,Kr,Xe的质量。 根据本发明,将液体排放物进料至第二塔,无需事先催化和/或吸附除去CxHy。 提取Kr馏分作为第二塔的顶部气体,并且从第二塔的底部排出Xe馏分。 该方法可用于在空气分离系统(LZA)中提取Xe和/或Kr的装置。 该装置可以布置在可运输的容器中。

    Method and apparatus for producing purified methyl isobutyl ketone
    3.
    发明授权
    Method and apparatus for producing purified methyl isobutyl ketone 有权
    生产纯化甲基异丁基酮的方法和设备

    公开(公告)号:US07671239B2

    公开(公告)日:2010-03-02

    申请号:US12085990

    申请日:2006-11-27

    IPC分类号: C07C45/82 C07C45/84

    摘要: This invention relates to a method of producing purified methyl isobutyl ketone (MIBK) comprising subjecting a feed stream containing MIBK and impurities to a first distillation procedure from which acetone is recovered. The bottom product of the first distillation procedure is fed to a liquid-liquid separator and an organic phase from the said liquid-liquid separator is fed to the top region of a second distillation column to produce an overhead product. The said overhead product is condensed and fed to the said liquid-liquid separator. A bottom product containing MIBK is withdrawn from the second distillation column. This bottom product is fed to a third distillation column, high boiling impurities are withdrawn as a bottom product, and purified MIBK is also withdrawn. The invention also relates to an apparatus used in such a method.

    摘要翻译: 本发明涉及一种生产纯化的甲基异丁基酮(MIBK)的方法,包括使含有MIBK和杂质的进料流经历回收丙酮的第一蒸馏步骤。 将第一蒸馏程序的底部产物进料至液 - 液分离器,并将来自所述液 - 液分离器的有机相进料至第二蒸馏塔的顶部区域以产生塔顶产物。 所述塔顶产物被冷凝并进料至所述液 - 液分离器。 含有MIBK的底部产物从第二蒸馏塔排出。 将该底部产物进料至第三蒸馏塔,将高沸点杂质作为底部产物取出,还提取纯化的MIBK。 本发明还涉及在这种方法中使用的装置。

    Method and apparatus for producing purified methyl isobutyl ketone
    4.
    发明授权
    Method and apparatus for producing purified methyl isobutyl ketone 有权
    生产纯化甲基异丁基酮的方法和设备

    公开(公告)号:US08242314B2

    公开(公告)日:2012-08-14

    申请号:US12086491

    申请日:2006-11-27

    IPC分类号: C07C45/82 C07C45/84

    摘要: This invention relates to a method of producing purified methyl isobutyl ketone (MIBK) comprising subjecting a feed stream containing MIBK and impurities to a first distillation procedure from which acetone is recovered and a bottom product containing MIBK and impurities is withdrawn. This bottom product is fed to a second distillation column, where a vapor overhead product is withdrawn, condensed and fed to an overhead liquid-liquid separator. Part of an organic phase from the overhead liquid-liquid separator is fed to the second distillation column and part is fed to a third distillation column. A vapor overhead product is withdrawn from the third column which is condensed in the same said condenser. The condensed product is fed to the same said overhead liquid-liquid separator, and purified MIBK is withdrawn from the third distillation column. This invention also relates to an apparatus used in such a method.

    摘要翻译: 本发明涉及一种生产纯化甲基异丁基酮(MIBK)的方法,包括使含有MIBK和杂质的进料流经历回收丙酮的第一蒸馏步骤,并且收集含有MIBK和杂质的底部产物。 将该底部产物进料至第二蒸馏塔,蒸馏塔顶产物被抽出,冷凝并送入塔顶液 - 液分离器。 将来自塔顶液 - 液分离器的有机相的一部分进料到第二蒸馏塔,并将一部分进料到第三蒸馏塔。 将蒸气塔顶产物从第三塔取出,该第三塔在相同的冷凝器中冷凝。 将冷凝产物加入到相同的塔顶液 - 液分离器中,从第三蒸馏塔中取出纯化的MIBK。 本发明还涉及在这种方法中使用的装置。

    Method and Apparatus for Producing Purified Methyl Isobutyl Ketone
    5.
    发明申请
    Method and Apparatus for Producing Purified Methyl Isobutyl Ketone 有权
    生产纯化甲基异丁基酮的方法和装置

    公开(公告)号:US20090253940A1

    公开(公告)日:2009-10-08

    申请号:US12085990

    申请日:2006-11-27

    IPC分类号: C07C45/82 B01J8/00 C07C49/04

    摘要: This invention relates to a method of producing purified methyl isobutyl ketone (MIBK) comprising subjecting a feed stream containing MIBK and impurities to a first distillation procedure from which acetone is recovered. The bottom product of the first distillation procedure is fed to a liquid-liquid separator and an organic phase from the said liquid-liquid separator is fed to the top region of a second distillation column to produce an overhead product. The said overhead product is condensed and fed to the said liquid-liquid separator. A bottom product containing MIBK is withdrawn from the second distillation column. This bottom product is fed to a third distillation column, high boiling impurities are withdrawn as a bottom product, and purified MIBK is also withdrawn. The invention also relates to an apparatus used in such a method.

    摘要翻译: 本发明涉及一种生产纯化的甲基异丁基酮(MIBK)的方法,包括使含有MIBK和杂质的进料流经历回收丙酮的第一蒸馏步骤。 将第一蒸馏程序的底部产物进料到液 - 液分离器,并将来自所述液 - 液分离器的有机相进料到第二蒸馏塔的顶部区域以产生塔顶产物。 所述塔顶产物被冷凝并进料至所述液 - 液分离器。 含有MIBK的底部产物从第二蒸馏塔排出。 将该底部产物进料至第三蒸馏塔,将高沸点杂质作为底部产物取出,还提取纯化的MIBK。 本发明还涉及在这种方法中使用的装置。

    Device for document filming
    6.
    发明授权
    Device for document filming 失效
    用于文件填充的装置

    公开(公告)号:US3947112A

    公开(公告)日:1976-03-30

    申请号:US482095

    申请日:1974-06-24

    IPC分类号: G01J1/42 G03B27/74 G03B27/76

    CPC分类号: G01J1/4223

    摘要: A document photographing device has a surface for supporting a document to be photographed, a camera positioned about the surface, to receive light reflected from and transmitted by a document supported on the surface, and separate means for illuminating the document from above and below respectively. An exposure meter receives light reflected from or transmitted through the document and indicates when correct exposure conditions have been set. The exposure meter includes correction means for correcting the reading of the exposure meter to take account of the different spectral radiation characteristics of the illuminating means.

    Microbiocidal compositions
    7.
    发明申请
    Microbiocidal compositions 审中-公开
    杀微生物剂

    公开(公告)号:US20090123397A1

    公开(公告)日:2009-05-14

    申请号:US11988670

    申请日:2006-07-11

    CPC分类号: A61Q17/005 A61K8/345 A61K8/49

    摘要: A microbiocidal composition comprising: a non-halogenated 2-alkyl-3-isothiazolone, and chlorphenesin and/or an alkane diol, wherein the alkyl group in the non-halogenated 2-alkyl-3-isothiazolone comprises 1 to 4 carbon atoms, the alkane diol comprises from 5 to 12 carbon atoms, and the hydroxyl groups of the alkane diol are vicinally substituted.

    摘要翻译: 一种杀微生物组合物,其包含:非卤代2-烷基-3-异噻唑酮和氯苯醚和/或烷二醇,其中非卤代2-烷基-3-异噻唑酮中的烷基包含1至4个碳原子, 烷二醇包含5至12个碳原子,链烷二醇的羟基被相邻取代。

    Device to cover the sight on hunting and sports bows
    8.
    发明授权
    Device to cover the sight on hunting and sports bows 失效
    覆盖狩猎和运动弓的视线的装置

    公开(公告)号:US06453898B1

    公开(公告)日:2002-09-24

    申请号:US09494426

    申请日:2000-01-31

    IPC分类号: F41G1467

    CPC分类号: F41G1/467 F41B5/14

    摘要: A cover is provided to protect the sight of an archery bow from distortion caused by falling precipitation, regardless of the horizontal position of the bow. The bow is provided with a sight having a lens; the sight is attached to the bow by a bracket. A cover is pivotally attached to the bracket, and includes an upper protective hood over the sight, and a lower counterweight. The counterweight is of sufficient weight so that the cover will pivot about the bracket as the bow is pivoted about a horizontal axis, or laid down, so the hood will maintain its protective position above the sight.

    摘要翻译: 提供了一个盖子,以保护射箭弓的视线免受由降水引起的变形,不管弓的水平位置如何。 弓提供有一个镜头的视线; 视线通过支架附着在弓上。 盖子可枢转地附接到支架上,并且包括在视线上的上保护罩和下配重。 配重具有足够的重量,使得当弓围绕水平轴线枢转或者放下时,盖将围绕支架枢转,因此罩将保持其在视线上方的保护位置。