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公开(公告)号：US5290586A
公开(公告)日：1994-03-01
申请号：US942861
申请日：1992-09-10
CPC分类号： B05D7/546 , B05D3/0254 , G01N21/3563 , G01N21/8422 , H05K1/0266 , H05K3/4644
摘要： Microreflectance infrared (IR) spectroscopy is used to determine the degree of cure of Meta-Paete (pyromellitic dianhydride-oxydianiline ethyl ester) films on metallized substrates. In this method, the infrared bands at 1028 and 1015 cm.sup.-1 are used to indirectly monitor ethanol evolution during Meta-Paete cure. The 1015 cm.sup.-1 band serves as internal reference, while the 1028 cm.sup.-1 band, which corresponds to the C--O stretch in the ethoxy group, is used to monitor imidization through loss of the ethoxy group during cure. Quantification of ethanol evolution is possible, since no apparent distortion is observed in the external reflection spectra at these two frequencies. The method can also be applied to measure the cure uniformity of Meta-Paete films, to provide an estimate of film thickness over metallized substrates, and to monitor temperature uniformity in an oven cavity.
摘要翻译： 使用微反射红外（IR）光谱法测定金属化基底上的Meta-Paete（均苯四酸二酐 - 氧联苯乙烯乙酯）膜的固化程度。 在这种方法中，1028和1015 cm-1的红外波段被用来间接监测Meta-Paete固化过程中的乙醇释放。 1015cm-1带用作内部参考，而对应于乙氧基中的C-O伸展的1028cm-1带用于通过在固化期间失去乙氧基来监测酰亚胺化。 乙醇析出的定量是可能的，因为在这两个频率的外部反射光谱中没有观察到明显的失真。 该方法还可以用于测量Meta-Paete膜的固化均匀性，以提供对金属化基底的膜厚度的估计，并监测烘箱腔中的温度均匀性。
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2.发明授权Base-modified metal oxide catalysts for the conversion of synthesis gas to alcohols 失效用于将合成气转化为醇的碱改性金属氧化物催化剂
公开(公告)号：US4824869A
公开(公告)日：1989-04-25
申请号：US158474
申请日：1988-02-22
IPC分类号： B01J23/887 , C07C29/156 , C07C29/157
CPC分类号： B01J23/8872 , C07C29/156 , C07C29/157
摘要： A method for preparing a mixture of lower aliphatic alcohols from the reaction of carbon monoxide and hydrogen in the presence of an oxide-containing heavy metal catalyst under carbon monoxide-hydrogenation conditions in which said catalyst comprises an alumina support, at least one heavy metal oxide selected from the group of oxides consisting of molybdenum, tungsten, rhenium, optionally, a heavy metal oxide from the group of elements consisting of cobalt, iron and nickel, and an alkali or alkaline earth promotor which has been treated with a nitrogen-containing compound, or a thermally stable derivative thereof is provided.
摘要翻译： 一种在一氧化碳 - 氢化条件下，在含氧化物的重金属催化剂存在下由一氧化碳和氢气反应制备低级脂族醇的混合物的方法，其中所述催化剂包含氧化铝载体，至少一种重金属氧化物 选自由钼，钨，铼组成的氧化物组，任选地，由钴，铁和镍组成的元素组中的重金属氧化物，以及已经用含氮化合物处理的碱金属或碱土金属的促进剂 ，或其热稳定衍生物。
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公开(公告)号：US06437472B1
公开(公告)日：2002-08-20
申请号：US09715620
申请日：2000-11-17
申请人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
发明人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
IPC分类号： H02K1900
CPC分类号： H01F38/18 , Y10S204/07
摘要： A magnetic induction device having at least one secondary induction assembly including a secondary winding is mounted on a rotary element. A magnetic flux is induced the secondary induction assembly, causing an induced secondary alternating current in the secondary winding of the secondary induction assembly. The secondary alternating current is converting to direct current and is stored in an electrical storage device.
摘要翻译： 具有至少一个包括次级绕组的次感应组件的磁感应装置安装在旋转元件上。 引起磁通量的次级感应组件，从而在次级感应组件的次级绕组中产生感应的次级交流电流。 次级交流电转换为直流电并存储在电存储装置中。
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公开(公告)号：US06278210B1
公开(公告)日：2001-08-21
申请号：US09386079
申请日：1999-08-30
申请人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
发明人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
IPC分类号： H02K1900
CPC分类号： H01F38/18 , Y10S204/07
摘要： The method and apparatus for supplying power to a rotary element by magnetic induction. A magnetic induction device having at least one secondary induction assembly including a secondary winding is mounted on the rotary element. A magnetic flux is induced the secondary induction assembly, causing an induced alternating current in the secondary winding of the secondary induction assembly. The secondary alternating current is converting to direct current and is stored in an electrical storage device. A rotary cathode plater is disclosed as a particular application of the apparatus by which power is transferred to a storage battery or high capacity capacitor, without the use of wires.
摘要翻译： 用于通过磁感应向旋转元件供电的方法和装置。 具有至少一个包括次级绕组的次感应组件的磁感应装置安装在旋转元件上。 引起磁通量二次感应组件，从而在次级感应组件的次级绕组中产生感应的交流电流。 次级交流电转换为直流电并存储在电存储装置中。 公开了一种旋转阴极喷涂器作为将电力传送到蓄电池或高容量电容器而不使用电线的装置的具体应用。
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5.发明授权Base-modified zeolite-containing catalysts for the conversion of synthesis gas to alcohols 失效用于将合成气转化为醇的碱改性沸石催化剂
公开(公告)号：US4822825A
公开(公告)日：1989-04-18
申请号：US185575
申请日：1988-04-25
IPC分类号： C07C29/153 , C07C29/156 , C07C27/06
CPC分类号： C07C29/156 , C07C29/153
摘要： A method for preparing a mixture of lower aliphatic alcohols from the reaction of carbon monoxide and hydrogen in the presence of a zeolite-containing heavy metal catalyst under carbon monoxide-hydrogenation conditions in which said catalysts comprises a zeolite support, at least one heavy metal oxide selected from the group of oxides consisting of molybdenum, tungsten, rhenium, optionally, a heavy metal oxide from the group of elements consisting of cobalt, iron and nickel and an alkali or alkaline earth promoter which has been treated with a nitrogen-containing compound, or a thermally stable derivative thereof is provided. A method for preparing zeolite-containing catalysts by treating with volatile metal complexes at high pressure is also provided.
摘要翻译： 一种一氧化碳氢化条件下，在含有沸石的重金属催化剂存在下，由一氧化碳和氢气反应制备低级脂族醇的混合物的方法，其中所述催化剂包括沸石载体，至少一种重金属氧化物 选自由钼，钨，铼组成的氧化物组，任选地，由钴，铁和镍组成的元素组的重金属氧化物和已经用含氮化合物处理的碱或碱土助催化剂， 或其热稳定衍生物。 还提供了通过用高压挥发性金属络合物处理来制备含沸石催化剂的方法。
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6.发明授权公开(公告)号：US06500316B1
公开(公告)日：2002-12-31
申请号：US09715724
申请日：2000-11-17
申请人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
发明人： Joseph J. Fatula, Jr. , Robert W. Hitzfeld , Richard Contreras , Guillermo Prada-Silva , Andrew Chiu , Rainer Schieferstein
IPC分类号： C25D1700
CPC分类号： H01F38/18 , Y10S204/07
摘要： An apparatus for rotary cathode electroplating having a head assembly, a substrate/thief assembly having a thieving ring which includes a number of individually chargeable segments, and a secondary induction assembly including a secondary core and a secondary winding. A motor drives the substrate/thief assembly to rotate relative to the head assembly. A controller directs electrical charge to each of the individually chargeable segments of the thieving ring. An electrical storage device stores electrical energy which is to be supplied to the controller. A charging apparatus induces a magnetic flux which induces an alternating current in the secondary winding of the secondary induction assembly. A converter converts the induced alternating current to direct current, which is then stored on the electrical storage device.
摘要翻译： 一种用于旋转阴极电镀的装置，其具有头部组件，具有包括多个可单独加载的节段的盗贼环的衬底/小窃贼组件，以及包括次级芯和次级绕组的次级感应组件。 马达驱动基板/窃贼组件相对于头部组件旋转。 控制器将电荷引导到盗窃环的每个可单独计费的段。 电存储装置存储要供给控制器的电能。 充电装置引起在二次感应组件的次级绕组中产生交流电流的磁通量。 A转换器将感应的交流电转换成直流电，然后存储在电存储装置上。
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公开(公告)号：US4886772A
公开(公告)日：1989-12-12
申请号：US208709
申请日：1988-06-20
IPC分类号： C07C29/156
CPC分类号： C07C29/156 , Y02P20/52
摘要： A method for preparing a mixture of lower aliphatic alcohols from the reaction of carbon monoxide and hydrogen in the presence of a sulfide-containing heavy metal catalyst under carbon-monoxide-hydrogenation conditions in which said catalyst comprises at least one sulfided heavy metal element selected from the group consisting of molybdenum, tungsten, rhenium, and an alkali or alkaline earth promoter which has been treated with a nitrogen-containing compound, or a theramlly stable derivative thereof is provided.
摘要翻译： 在一氧化碳 - 氢化条件下，在含硫化物的重金属催化剂的存在下，从一氧化碳和氢气的反应制备低级脂族醇的混合物的方法，其中所述催化剂包含至少一种选自以下的硫化重金属元素： 提供了已经用含氮化合物处理的钼，钨，铼以及碱土或碱土助催化剂或其热稳定的衍生物。
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公开(公告)号：US4774220A
公开(公告)日：1988-09-27
申请号：US20835
申请日：1987-03-02
IPC分类号： B01J23/887 , C07C29/156 , B01J21/04 , B01J23/78 , B01J23/88
CPC分类号： B01J23/8872 , C07C29/156 , Y02P20/52
摘要： A lithium-doped gamma-alumina supported cobalt-molybdenum catalyst and a process for converting synthesis gas to a mixture of lower aliphatic alcohols is provided.
摘要翻译： 提供掺锂的γ-氧化铝负载的钴 - 钼催化剂和将合成气转化为低级脂族醇的混合物的方法。
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公开(公告)号：US4775696A
公开(公告)日：1988-10-04
申请号：US945264
申请日：1986-12-22
IPC分类号： C07C29/156 , C07C27/06
CPC分类号： C07C29/156
摘要： A method for preparing a mixture of lower aliphatic alcohols from the reaction of carbon monoxide and hydrogen in the presence of a sulfide-containing heavy metal catalyst under carbon monoxide-hydrogenation conditions in which said catalyst comprises at least one sulfided heavy metal element selected from the group consisting of molybdenum, tungsten, rhenium, and an alkali or alkaline earth promoter which has been treated with a nitrogen-containing compound, or a thermally stable derivative thereof is provided.
摘要翻译： 在一氧化碳 - 氢化条件下，在含硫化物的重金属催化剂的存在下，由一氧化碳和氢气的反应制备低级脂族醇的混合物的方法，其中所述催化剂包含至少一种选自以下的硫化重金属元素： 提供了已经用含氮化合物处理的钼，钨，铼以及碱土或碱土助催化剂或其热稳定的衍生物组成的组。
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