公开(公告)号：US20120040075A1

公开(公告)日：2012-02-16

申请号：US13279407

申请日：2011-10-24

申请人： Shinichiro TAKASHIMA ,  Masaki Iwasaki ,  Kojirou Hashizume ,  Naoki Hosoya ,  Shinji Yamamoto ,  Yoshikazu Ogura ,  Jun Saito ,  Hitoshi Takaya ,  Masami Shimizu ,  Norihiko Satake ,  Eiichi Hoshino ,  Yukiteru Sugiyama

发明人： Shinichiro TAKASHIMA ,  Masaki Iwasaki ,  Kojirou Hashizume ,  Naoki Hosoya ,  Shinji Yamamoto ,  Yoshikazu Ogura ,  Jun Saito ,  Hitoshi Takaya ,  Masami Shimizu ,  Norihiko Satake ,  Eiichi Hoshino ,  Yukiteru Sugiyama

IPC分类号： A23F3/38 ,  A23F3/20 ,  A23F3/16

CPC分类号： C07D311/62 ,  A23F3/163 ,  A23F3/385 ,  A61K31/353

摘要： To provide a packaged high-catechin beverage in which a low-caffeine green tea extract is added.A packaged beverage containing from 0.03 to 1.0 wt % of non-polymer catechins, in which a low-caffeine green tea extract obtained by a method of brining a green tea extract into contact with a 91/9 to 97/3 by weight mixture of an organic solvent and water, activated carbon, and acid clay or activated clay is added.

摘要翻译： 提供其中加入低咖啡因绿茶提取物的包装的高儿茶素饮料。 一种含有0.03〜1.0重量％的非聚合型儿茶素类的包装饮料，其中通过将绿茶提取物与91/9至97/3重量份的混合物接触的方法获得的低咖啡因绿茶提取物 加入有机溶剂和水，活性炭和酸性粘土或活性粘土。

公开(公告)号：US08088429B2

公开(公告)日：2012-01-03

申请号：US10581200

申请日：2004-12-01

申请人： Shinichiro Takashima ,  Masaki Iwasaki ,  Kojirou Hashizume ,  Naoki Hosoya ,  Shinji Yamamoto ,  Yoshikazu Ogura ,  Jun Saito ,  Hitoshi Takaya ,  Masami Shimizu ,  Norihiko Satake ,  Eiichi Hoshino ,  Yukiteru Sugiyama

发明人： Shinichiro Takashima ,  Masaki Iwasaki ,  Kojirou Hashizume ,  Naoki Hosoya ,  Shinji Yamamoto ,  Yoshikazu Ogura ,  Jun Saito ,  Hitoshi Takaya ,  Masami Shimizu ,  Norihiko Satake ,  Eiichi Hoshino ,  Yukiteru Sugiyama

IPC分类号： A23F3/16 ,  A23L2/72 ,  A23L2/80 ,  C12H1/02

CPC分类号： C07D311/62 ,  A23F3/163 ,  A23F3/385 ,  A61K31/353

摘要： To provide a packaged high-catechin beverage in which a low-caffeine green tea extract is added. A packaged beverage containing from 0.03 to 1.0 wt % of non-polymer catechins, in which a low-caffeine green tea extract obtained by a method of brining a green tea extract into contact with a 91/9 to 97/3 by weight mixture of an organic solvent and water, activated carbon, and acid clay or activated clay is added.

摘要翻译： 提供其中加入低咖啡因绿茶提取物的包装的高儿茶素饮料。 一种含有0.03〜1.0重量％的非聚合型儿茶素类的包装饮料，其中通过将绿茶提取物与91/9至97/3重量份的混合物接触的方法获得的低咖啡因绿茶提取物 加入有机溶剂和水，活性炭和酸性粘土或活性粘土。

公开(公告)号：US07098177B1

公开(公告)日：2006-08-29

申请号：US09581594

申请日：1999-10-14

申请人： Teruo Kubota ,  Hitoshi Takaya ,  Hiroyuki Yamashita

发明人： Teruo Kubota ,  Hitoshi Takaya ,  Hiroyuki Yamashita

IPC分类号： C11D11/00

CPC分类号： C11D17/06 ,  C11D11/0082 ,  C11D17/065

摘要： A process for preparing detergent particles containing step (I): mixing a base particle for supporting a surfactant ((a) component), and a surfactant composition ((b) component), under mixing conditions wherein the (a) component does not substantially undergo breakdown, to give a mixture; wherein the base particle is obtained by spray-drying an aqueous slurry, wherein the mixing operation is carried out by using a mixer containing agitation impellers, and where the mixer further contains disintegration impellers, the mixing operation step (I) is carried out without substantially rotating the disintegration impellers; and step (II): mixing the mixture obtained in step (I) with 5 to 100 parts by weight of fine powder, while substantially maintaining the shape of the (a) component containing (b) component, to give detergent particles, having a degree of particle growth of 1.3 or less, and a bulk density of 500 g/L or more.

摘要翻译： 一种制备含有步骤（I）的洗涤剂颗粒的方法：在（a）成分基本上不含有（a）成分的混合条件下混合表面活性剂（（a）成分）和表面活性剂组合物（（b）成分） 进行分解，给出混合物; 其特征在于，所述基础颗粒是通过喷雾干燥含水浆料而获得的，其中所述混合操作是通过使用含有搅拌叶轮的混合器进行的，并且其中所述混合器还包含崩解叶轮，所述混合操作步骤（I） 旋转分解叶轮; 和步骤（II）：在基本保持含（b）成分的（a）成分的形状的同时，将步骤（I）中获得的混合物与5至100重量份的细粉末混合，得到具有 粒子生长度为1.3以下，堆积密度为500g / L以上。

公开(公告)号：US06864221B1

公开(公告)日：2005-03-08

申请号：US09762948

申请日：2000-06-14

申请人： Shuji Takana ,  Hitoshi Takaya ,  Hiroki Yamaboshi ,  Yoichi Sugiyama ,  Hiroshi Kitagaito ,  Shu Yamaguchi ,  Hiroyuki Yamashita

发明人： Shuji Takana ,  Hitoshi Takaya ,  Hiroki Yamaboshi ,  Yoichi Sugiyama ,  Hiroshi Kitagaito ,  Shu Yamaguchi ,  Hiroyuki Yamashita

IPC分类号： C11D3/02 ,  C11D3/04 ,  C11D3/10 ,  C11D3/37 ,  C11D11/00 ,  C11D11/02 ,  C11D17/06

CPC分类号： C11D3/046 ,  C11D3/10 ,  C11D3/37 ,  C11D11/0082 ,  C11D11/02 ,  C11D17/065

摘要： The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same. According to the present invention, there can be obtained particles for supporting a surfactant which are excellent in the supporting ability (supporting capacity/supporting strength) for the liquid surfactant composition, and particles for supporting a surfactant which are excellent in the absorption properties (supporting rate) for the liquid surfactant composition, by spray-drying a preparation liquid obtainable by a process comprising the steps of preparing a first preparation liquid comprising a solution or slurry comprising a water-soluble polymer and a water-soluble salt; and subjecting the first preparation liquid to a treatment of increasing a number of water-soluble salt particles, thereby preparing a second preparation liquid having an increased number of water-soluble salt particles, as compared to the number of water-soluble salt particles which are present in the first preparation liquid. Further, since the liquid surfactant composition is supported by the particles for supporting a surfactant, detergent particles which are excellent in detergent performance, quality and the like can be efficiently obtained.

摘要翻译： 本发明涉及用于支撑表面活性剂的颗粒及其制备方法。 此外，本发明涉及使用用于支撑表面活性剂的颗粒的高密度洗涤剂颗粒及其制备方法。 根据本发明，可以获得支撑液体表面活性剂组合物的支持能力（支撑能力/支撑强度）优异的表面活性剂用颗粒和吸收性优异的支撑表面活性剂的颗粒（支撑 速率），通过喷雾干燥可通过包括以下步骤的方法获得的制备液：制备包含水溶性聚合物和水溶性盐的溶液或浆液的第一制备液; 并且对第一制备液进行处理以增加数量的水溶性盐颗粒，从而制备具有增加数量的水溶性盐颗粒的第二制备液，与水溶性盐颗粒的数量相比， 存在于第一准备液中。 此外，由于液体表面活性剂组合物被用于支撑表面活性剂的颗粒负载，所以可以有效地获得洗涤剂性能，质量等方面优异的洗涤剂颗粒。

公开(公告)号：US06831056B1

公开(公告)日：2004-12-14

申请号：US09868897

申请日：2001-07-06

申请人： Kazuo Oki ,  Hiroji Hosokawa ,  Mikio Sakaguchi ,  Hiroshi Kitagaito ,  Kazuo Taguchi ,  Hitoshi Takaya

发明人： Kazuo Oki ,  Hiroji Hosokawa ,  Mikio Sakaguchi ,  Hiroshi Kitagaito ,  Kazuo Taguchi ,  Hitoshi Takaya

IPC分类号： C11D714

CPC分类号： C01B39/14 ,  C01B39/02 ,  C11D3/128

摘要： A process for efficiently preparing fine zeolite particles comprising synthesizing zeolite in the presence of an alkaline earth metal-containing compound and/or with controlling the preparation process of zeolite, thereby giving fine zeolite particles being composed of crystalline aluminosilicate, the fine zeolite particles having a fine average primary particle size, being excellent in the cationic exchange properties and the oil-absorbing ability, having a fine average aggregate particle size, and being excellent in the dispersibility; fine zeolite particles obtainable by the above process; and a detergent composition comprising the fine zeolite particles, the detergent composition being excellent in the detergency.

摘要翻译： 包括在含碱土金属的化合物的存在下合成沸石和/或控制沸石的制备方法的精细沸石颗粒的方法，从而得到由结晶硅铝酸盐构成的细沸石颗粒，所述细沸石颗粒具有 平均一次粒径优异，阳离子交换性和油吸收性优异，平均聚集体粒径均匀，分散性优异; 通过上述方法获得的细沸石颗粒; 以及包含细小沸石颗粒的洗涤剂组合物，洗涤剂组合物的去污力优异。

公开(公告)号：US06602846B1

公开(公告)日：2003-08-05

申请号：US09762934

申请日：2001-02-14

申请人： Teruo Kubota ,  Hitoshi Takaya ,  Motomitsu Hasumi ,  Hiroyuki Yamashita

发明人： Teruo Kubota ,  Hitoshi Takaya ,  Motomitsu Hasumi ,  Hiroyuki Yamashita

IPC分类号： C11D1100

CPC分类号： C11D17/065 ,  C11D11/0082

摘要： The present invention relates to a process for preparing uni-core detergent particles having a degree of particle growth of 1.5 or less and a bulk density of 500 g/L or more, comprising the steps of (A-I) mixing base particles for supporting a surfactant which have an average particle size of from 150 to 500 &mgr;m and a bulk density of 400 g/L or more [Component (a)] with a surfactant composition [Component (c)]; (A-II) mixing a mixture obtained in Step (A-I) with a powdery builder [Component (b)] of which primary average particle size is from 3 to 30 &mgr;m; and (A-III) mixing a mixture obtained in Step (A-II) with a fine powder [Component (d)] of which primary average particle size is smaller than that of Component (b). By using the process of the present invention, the uni-core detergent particles which are excellent in the dissolubility and the flowability properties can be prepared.

摘要翻译： 本发明涉及一种制备颗粒生长度为1.5以下，体积密度为500g / L以上的单核洗涤剂粒子的方法，其特征在于，包括（A1）混合用于担载表面活性剂的基础粒子 具有表面活性剂组合物[组分（c）]的平均粒度为150至500μm，堆积密度为400g / L或更高[组分（a）]]。 （A-II）将步骤（A-I）中获得的混合物与一次平均粒径为3-30μm的粉末助洗剂[组分（b）]混合; 和（A-III）将步骤（A-II）中获得的混合物与一次平均粒径小于组分（b）的细粉末[组分（d）]混合。 通过使用本发明的方法，可以制备溶解性和流动性优异的单核洗涤剂颗粒。

公开(公告)号：US20050079994A1

公开(公告)日：2005-04-14

申请号：US10954087

申请日：2004-09-30

申请人： Kazuo Oki ,  Hiroji Hosokawa ,  Mikio Sakaguchi ,  Hiroshi Kitagaito ,  Kazuo Taguchi ,  Hitoshi Takaya

发明人： Kazuo Oki ,  Hiroji Hosokawa ,  Mikio Sakaguchi ,  Hiroshi Kitagaito ,  Kazuo Taguchi ,  Hitoshi Takaya

IPC分类号： C01B39/02 ,  C01B39/14 ,  C11D3/12 ,  C11D17/00

CPC分类号： C01B39/14 ,  C01B39/02 ,  C11D3/128

摘要： A process for efficiently preparing fine zeolite particles comprising synthesizing zeolite in the presence of an alkaline earth metal-containing compound and/or with controlling the preparation process of zeolite, thereby giving fine zeolite particles being composed of crystalline aluminosilicate, the fine zeolite particles having a fine average primary particle size, being excellent in the cationic exchange properties and the oil-absorbing ability, having a fine average aggregate particle size, and being excellent in the dispersibility; fine zeolite particles obtainable by the above process; and a detergent composition comprising the fine zeolite particles, the detergent composition being excellent in the detergency.

摘要翻译： 包括在含碱土金属的化合物的存在下合成沸石和/或控制沸石的制备方法的精细沸石颗粒的方法，从而得到由结晶硅铝酸盐构成的细沸石颗粒，所述细沸石颗粒具有 平均一次粒径优异，阳离子交换性和油吸收性优异，平均聚集体粒径均匀，分散性优异; 通过上述方法获得的细沸石颗粒; 以及包含细小沸石颗粒的洗涤剂组合物，洗涤剂组合物的去污力优异。

公开(公告)号：US06734156B1

公开(公告)日：2004-05-11

申请号：US09762948

申请日：2001-02-14

申请人： Shuji Takana ,  Hitoshi Takaya ,  Hiroki Yamaboshi ,  Yoichi Sugiyama ,  Hiroshi Kitagaito ,  Shu Yamaguchi ,  Hiroyuki Yamashita

发明人： Shuji Takana ,  Hitoshi Takaya ,  Hiroki Yamaboshi ,  Yoichi Sugiyama ,  Hiroshi Kitagaito ,  Shu Yamaguchi ,  Hiroyuki Yamashita

IPC分类号： C11D1100

CPC分类号： C11D3/046 ,  C11D3/10 ,  C11D3/37 ,  C11D11/0082 ,  C11D11/02 ,  C11D17/065

摘要： The present invention relates to particles for supporting a surfactant and a process for preparing the same. Further, the present invention relates to high-density detergent particles using the particles for supporting a surfactant, and a process for preparing the same. According to the present invention, there can be obtained particles for supporting a surfactant which are excellent in the supporting ability (supporting capacity/supporting strength) for the liquid surfactant composition, and particles for supporting a surfactant which are excellent in the absorption properties (supporting rate) for the liquid surfactant composition, by spray-drying a preparation liquid obtainable by a process comprising the steps of preparing a first preparation liquid comprising a solution or slurry comprising a water-soluble polymer and a water-soluble salt; and subjecting the first preparation liquid to a treatment of increasing a number of water-soluble salt particles, thereby preparing a second preparation liquid having an increased number of water-soluble salt particles, as compared to the number of water-soluble salt particles which are present in the first preparation liquid. Further, since the liquid surfactant composition is supported by the particles for supporting a surfactant, detergent particles which are excellent in detergent performance, quality and the like can be efficiently obtained.

摘要翻译： 本发明涉及用于支持表面活性剂的颗粒及其制备方法。 此外，本发明涉及使用用于支撑表面活性剂的颗粒的高密度洗涤剂颗粒及其制备方法。 根据本发明，可以获得支撑液体表面活性剂组合物的支持能力（支撑能力/支撑强度）优异的表面活性剂用颗粒和吸收性优异的支撑表面活性剂的颗粒（支撑 速率），通过喷雾干燥可通过包括以下步骤的方法获得的制备液：制备包含水溶性聚合物和水溶性盐的溶液或浆液的第一制备液; 并且对第一制备液进行处理以增加数量的水溶性盐颗粒，从而制备具有增加数量的水溶性盐颗粒的第二制备液，与水溶性盐颗粒的数量相比， 存在于第一准备液中。 此外，由于液体表面活性剂组合物被用于支撑表面活性剂的颗粒负载，所以可以有效地获得洗涤剂性能，质量等方面优异的洗涤剂颗粒。

公开(公告)号：US06645931B1

公开(公告)日：2003-11-11

申请号：US09594025

申请日：2000-06-15

申请人： Yuhki Yanagisawa ,  Nobuyoshi Yamaguchi ,  Shu Yamaguchi ,  Hitoshi Takaya ,  Hiroyuki Yamashita

发明人： Yuhki Yanagisawa ,  Nobuyoshi Yamaguchi ,  Shu Yamaguchi ,  Hitoshi Takaya ,  Hiroyuki Yamashita

IPC分类号： C11D1700

CPC分类号： C11D3/0052 ,  C11D17/0047 ,  C11D17/065

摘要： A solid-shaped detergent comprising particles for detergent, wherein the particles have a dissolution rate of 90% or more, under conditions where the particles are supplied in water at 5° C.; stirred for 60 seconds under the stirring conditions that 1 g of the particles are supplied to a 1-L beaker having an inner diameter of 105 mm which is charged with 1 L of hard, water having 71.2 mg CaCO3/L, wherein a molar ratio of Ca/Mg is 7/3, and stirred with a stirring bar of 35 mm in length and 8 mm in diameter at a rotational speed of 800 rpm; and filtered with a standard sieve having a sieve-opening of 74 &mgr;m as defined by JIS Z 8801, wherein the dissolution rate of the particles is calculated by the Equation (1): Dissolution Rate (%)=[1−(T/S)]×100 (1), wherein S is a weight (g) of the particles supplied; and T is a dry weight (g) of insoluble remnants of the particles remaining on the sieve when an aqueous solution prepared under the above stirring conditions is filtered with the sieve.

摘要翻译： 一种固体形洗涤剂，其包含用于洗涤剂的颗粒，其中颗粒在5℃的水中供应的条件下，其溶解速率为90％以上。 在搅拌条件下搅拌60秒，将1g的颗粒供给到内径为105mm的1L的烧杯中，该烧杯装入1L的具有71.2mg CaCO 3 / L的硬水，其中摩尔比 的Ca / Mg为7/3，并以800rpm的转速与长35mm，直径8mm的搅拌棒一起搅拌， 用JIS Z 8801定义的筛孔为74μm的标准筛过滤，其中通过式（1）计算颗粒的溶解速率：溶解速率（％）= [1-（T / S ）]×100（1），其中S是供给的颗粒的重量（g） 当用筛子过滤在上述搅拌条件下制备的水溶液时，T是残留在筛上的颗粒的不溶性残留物的干重（g）。

公开(公告)号：US06534474B1

公开(公告)日：2003-03-18

申请号：US09701781

申请日：2000-12-04

申请人： Kyoko Okada ,  Teruo Kubota ,  Hitoshi Takaya ,  Shu Yamaguchi ,  Hiroyuki Yamashita

发明人： Kyoko Okada ,  Teruo Kubota ,  Hitoshi Takaya ,  Shu Yamaguchi ,  Hiroyuki Yamashita

IPC分类号： C11D183

CPC分类号： C11D17/06 ,  C11D1/83 ,  C11D3/3707 ,  C11D10/045

摘要： The surfactant composition of the present invention is a surfactant composition which is capable of being formulated for use in a non-liquid detergent composition, the surfactant composition comprising a) a nonionic surfactant having a melting point of 30° C. or less; b) an anionic surfactant having sulfonate group; and c) an immobilization agent for a) component, wherein b) component is formulated in an amount of from 0 to 300 parts by weight, based on 100 parts by weight of a) component, and wherein c) component is formulated in an amount of from 1 to 100 parts by weight, based on 100 parts by weight of a) component, and wherein the surfactant composition has (1) a temperature range that a viscosity of the composition is 10 Pa·s or less at a temperature equal to or higher than a pour point of the surfactant composition; and (2) a temperature range that a penetrating hardness of the composition is 100 g/cm2 or more in a temperature range between a temperature lower than the pour point of the surfactant composition and a temperature higher than the melting point of a) component.

摘要翻译： 本发明的表面活性剂组合物是能够配制用于非液体洗涤剂组合物的表面活性剂组合物，所述表面活性剂组合物包含a）熔点为30℃以下的非离子表面活性剂; b）具有磺酸盐基团的阴离子表面活性剂; 和c）a）组分的固定剂，其中b）组分的配制量为0至300重量份，基于100重量份的a）组分，并且其中c）组分配制成一定量 1至100重量份，基于100重量份的a）组分，并且其中表面活性剂组合物具有（1）组合物的粘度在等于或等于10℃的温度下为10Pa·s以下的温度范围 或高于表面活性剂组合物的倾点; 和（2）在比表面活性剂组合物的倾点低的温度和高于a）成分的熔点的温度的温度范围内组合物的穿透硬度为100g / cm 2以上的温度范围。