Hand-held trace vapor/particle sampling system

    公开(公告)号:US20070034024A1

    公开(公告)日:2007-02-15

    申请号:US11202455

    申请日:2005-08-11

    Applicant: Jack Syage

    Inventor: Jack Syage

    CPC classification number: G01N1/22 G01N1/02 G01N1/2205 G01N1/4005 G01N1/405

    Abstract: A sampling system that contains filter components for collecting and concentrating vapor and particles in high-volume flows. The sample is then vaporized and delivered to a detector at a low-volume flow. The invention also has a sampling probe that contains an air-jet to help dislodge particles from surfaces and a heating lamp to help vaporize compounds on surfaces or objects. The sampling system is especially useful for screening for explosives and other illicit chemicals and toxins on people, baggage, cargo, and other objects.

    Interfaces for a photoionization mass spectrometer
    2.
    发明申请
    Interfaces for a photoionization mass spectrometer 审中-公开
    光电离质谱仪的接口

    公开(公告)号:US20070138387A1

    公开(公告)日:2007-06-21

    申请号:US11509479

    申请日:2006-08-23

    CPC classification number: H01J49/162 H01J49/04 H01J49/107

    Abstract: A detector system that contains two inlet port coupled to a photoionization chamber. One inlet port allows for the introduction of a test sample. The test sample may contain contaminants, drugs, explosive, etc. that are to be detected. The other port allows for the simultaneous introduction of a standard sample. The standard sample can be used to calibrate and/or diagnose the detector system. Simultaneous introduction of the standard sample provides for real time calibration/diagnostics of the detector during detection of trace molecules in the test sample. The photoizonizer ionizes the samples which are then directed into a mass detector for detection of trace molecules. The detector system may also include inlet embodiments that allow for vaporization of liquid samples introduced to a low pressure photoionizer.

    Abstract translation: 检测器系统,其包含耦合到光电离室的两个入口端口。 一个入口允许引入测试样品。 试样可能含有要检测的污染物,药物,爆炸物等。 另一个端口允许同时引入标准样品。 标准样品可用于校准和/或诊断检测器系统。 标准样品的同时引入在检测样品中的痕量分子时提供检测器的实时校准/诊断。 光化学剂将样品电离,然后将样品引导到质量检测器中以检测微量分子。 检测器系统还可以包括允许引入低压光离子化器的液体样品蒸发的入口实施方案。

    Glow discharge and photoionization source
    3.
    发明申请
    Glow discharge and photoionization source 有权
    辉光放电和光电离源

    公开(公告)号:US20060284103A1

    公开(公告)日:2006-12-21

    申请号:US11138594

    申请日:2005-05-25

    Applicant: Jack Syage

    Inventor: Jack Syage

    Abstract: A detector that may contain a glow discharge ionizer and a photo-ionizer. The existence of both ionizers may increase the accuracy and number of chemical compounds that can be simultaneously monitored for chemical screening applications. The detector is particularly useful for screening explosives, chemical agents, and other illicit chemicals.

    Abstract translation: 可以包含辉光放电电离器和光电离器的检测器。 两种电离器的存在可能会增加可以同时监测化学筛选应用的化合物的准确性和数量。 检测器特别适用于筛选爆炸物,化学试剂和其他非法化学品。

    Multiple trace portal detection systems
    4.
    发明申请
    Multiple trace portal detection systems 有权
    多路径门户检测系统

    公开(公告)号:US20060196249A1

    公开(公告)日:2006-09-07

    申请号:US11075199

    申请日:2005-03-07

    CPC classification number: G01N27/626

    Abstract: A detector system that can analyze multiple samples with a single detector. The detector may contain a portal with a first opening and a second opening. A first sample is obtained from the first opening and a second sample is obtained from the second opening. The openings are coupled to a single detector that can analyze both samples.

    Abstract translation: 可以用单个检测器分析多个样品的检测器系统。 检测器可以包含具有第一开口和第二开口的入口。 从第一开口获得第一样品,并且从第二开口获得第二样品。 开口耦合到可以分析两个样品的单个检测器。

    Interfaces for a photoionization mass spectrometer
    5.
    发明申请
    Interfaces for a photoionization mass spectrometer 有权
    光电离质谱仪的接口

    公开(公告)号:US20050139764A1

    公开(公告)日:2005-06-30

    申请号:US11004495

    申请日:2004-12-03

    CPC classification number: H01J49/162 H01J49/04 H01J49/107

    Abstract: A detector system that contains two inlet port coupled to a photoionization chamber. One inlet port allows for the introduction of a test sample. The test sample may contain contaminants, drugs, explosive, etc. that are to be detected. The other port allows for the simultaneous introduction of a standard sample. The standard sample can be used to calibrate and/or diagnose the detector system. Simultaneous introduction of the standard sample provides for real time calibration/diagnostics of the detector during detection of trace molecules in the test sample. The photoizonizer ionizes the samples which are then directed into a mass detector for detection of trace molecules. The detector system may also include inlet embodiments that allow for vaporization of liquid samples introduced to a low pressure photoionizer.

    Abstract translation: 检测器系统,其包含耦合到光电离室的两个入口端口。 一个入口允许引入测试样品。 测试样品可能含有要检测的污染物,药物,爆炸物等。 另一个端口允许同时引入标准样品。 标准样品可用于校准和/或诊断检测器系统。 标准样品的同时引入在检测样品中的痕量分子时提供检测器的实时校准/诊断。 光化学剂将样品电离,然后将样品引导到质量检测器中以检测微量分子。 检测器系统还可以包括允许引入低压光离子化器的液体样品蒸发的入口实施方案。

    Real-time multispecies monitoring by photoionization mass spectrometry
    6.
    发明授权
    Real-time multispecies monitoring by photoionization mass spectrometry 失效
    通过光电离质谱法进行实时多物种监测

    公开(公告)号:US5808299A

    公开(公告)日:1998-09-15

    申请号:US802004

    申请日:1997-02-18

    Applicant: Jack Syage

    Inventor: Jack Syage

    CPC classification number: H01J49/162 H01J49/0422 H01J49/40 H01J49/424

    Abstract: A monitor that photo-ionizes trace constituents within a quadrupole ion trap (QIT). The QIT may have a valve that discharges a gas specimen into a trap chamber or a gas line that continuously discharges a gas specimen into the QIT. The trap chamber is surrounded by a ring, and an extractor plate that has an orifice. The trace molecules within the air may be ionized at the nozzle of the valve by a photo-ionizer. Photo-ionizing at the valve nozzle provides a relatively high density of ionized molecules. The photo-ionizer may be either a pulsed light source or a continuous wave light source. The trace molecules are preferably ionized with energy between 8.0 and 11.0 electron volts (eV). The energy is selected to ionize the trace molecules without fragmenting the trace constituents. A radio frequency or other oscillating frequency voltage potential is applied to the ring to trap the ionized trace molecules within the trap chamber. A voltage pulse is applied to the extractor plate to pull the ionized molecules out of the chamber and through the orifice. The extracted ionized molecules are then accelerated to a detector. The monitor has a time of flight analyzer to measure the mass of the trace constituents in the specimen.

    Abstract translation: 在四极离子阱(QIT)内对痕量成分进行光电离的监测仪。 QIT可以具有将气体样本排放到陷阱室或将气体样本连续排放到QIT中的气体管线的阀。 捕集室被环包围,并且具有孔的抽出板。 空气中的痕量分子可以通过光电离器在阀的喷嘴处离子化。 在阀喷嘴处的光电离提供了相对较高密度的电离分子。 光电离器可以是脉冲光源或连续波光源。 微量分子优选以8.0和11.0电子伏(eV)之间的能量电离。 选择能量来电离微量分子,而不会使微量成分碎裂。 将射频或其他振荡频率电压电位施加到环上以将电离的微量分子捕获在捕获室内。 电压脉冲施加到提取器板以将离子化的分子拉出腔室并通过孔口。 然后将提取的离子化分子加速至检测器。 显示器有一个飞行时间分析仪来测量样品中微量成分的质量。

    High speed, multiple mass spectrometry for ion sequencing
    7.
    发明申请
    High speed, multiple mass spectrometry for ion sequencing 失效
    用于离子测序的高速多重质谱

    公开(公告)号:US20050242278A1

    公开(公告)日:2005-11-03

    申请号:US11051427

    申请日:2005-02-03

    CPC classification number: H01J49/0045 H01J49/40 H01J49/42 H01J49/424

    Abstract: A detector system for detecting trace molecules. The detector includes an ion trap that is coupled to an ionizer and a detector. The system also includes a controller that can generate voltage potentials within the ion trap. The controller can generate a voltage waveform to isolate one or more ions within the ion trap. The controller can then generate a voltage to dissociate the isolated ion(s). The controller can vary the dissociating voltage to dissociate and detect different ions. For example, the controller may vary the amplitude of the voltage to dissociate a target ion. Other techniques are described which generally improve the speed of detecting different target ions.

    Abstract translation: 用于检测痕量分子的检测器系统。 检测器包括耦合到离子发生器和检测器的离子阱。 该系统还包括可在离子阱内产生电压电位的控制器。 控制器可以产生电压波形以隔离离子阱内的一个或多个离子。 然后,控制器可产生电压以离解分离的离子。 控制器可以改变解离电压以离解和检测不同的离子。 例如,控制器可以改变电压的幅度以解离目标离子。 描述了通常提高检测不同目标离子的速度的其它技术。

Patent Agency Ranking