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    Process for preparing 3-(1-hydroxyphenyl-1-alkoximinomethyl) dioxazines
    1.
    发明授权
    Process for preparing 3-(1-hydroxyphenyl-1-alkoximinomethyl) dioxazines 有权
    制备3-（1-羟基苯基-1-肟基甲基）二恶嗪的方法

    公开(公告)号：US6093837A

    公开(公告)日：2000-07-25

    申请号：US186708

    申请日：1998-11-05

    Applicant: Bernd Gallenkamp ,  Lothar Rohe ,  Herbert Gayer ,  Peter Gerdes

    Inventor： Bernd Gallenkamp ,  Lothar Rohe ,  Herbert Gayer ,  Peter Gerdes

    IPC: C07D273/00 ,  C07D273/01 ,  C07D307/82

    CPC classification number: C07D273/00 ,  C07D307/82

    Abstract: The present invention relates to a novel process for preparing 3-(1-hydroxyphenyl-1-alkoximinomethyl)dioxazines which are known as intermediates for preparing compounds having fungicidal properties (WO 95-04728). Furthermore, the invention relates to novel 3-(1-hydroxyphenyl-1-alkoximinomethyl)dioxazines, to novel intermediates for their preparation and to a plurality of processes for preparing the novel intermediates.

    Abstract translation: 本发明涉及一种制备作为制备具有杀真菌性的化合物的中间体的3-（1-羟基苯基-1-肟基甲基）二恶嗪的新方法（WO 95-04728）。 此外，本发明涉及新的3-（1-羟基苯基-1-肟基甲基）二恶嗪，用于制备新的中间体和多种制备新型中间体的方法。

    Process for preparing 3,5-dimethylisoxazole-4-sulphonyl chloride
    2.
    发明授权
    Process for preparing 3,5-dimethylisoxazole-4-sulphonyl chloride 失效
    制备3,5-二甲基异恶唑-4-磺酰氯的方法

    公开(公告)号：US5959119A

    公开(公告)日：1999-09-28

    申请号：US175817

    申请日：1998-10-20

    Applicant: Bernd Gallenkamp ,  Lothar Rohe

    Inventor： Bernd Gallenkamp ,  Lothar Rohe

    IPC: C07D261/10

    CPC classification number: C07D261/10

    Abstract: By a novel process, 3,5-dimethylisoxazole-4-sulphonyl chloride is prepared by reacting 3,5-dimethylisoxazole initially with chlorosulphonic acid and then additionally with thionyl chloride at a temperature between 60.degree. C. and 110.degree. C.

    Abstract translation: 通过新方法，通过使3,5-二甲基异恶唑最初与氯磺酸反应，然后另外与亚硫酰氯在60℃至110℃的温度下反应制备3,5-二甲基异恶唑-4-磺酰氯。

    1,3-dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride
    3.
    发明授权
    1,3-dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride 失效
    1,3-二甲基-5-氟 - 吡唑-4-碳酰氟

    公开(公告)号：US5750721A

    公开(公告)日：1998-05-12

    申请号：US838660

    申请日：1997-04-09

    Applicant: Bernd Gallenkamp ,  Lothar Rohe ,  Albrecht Marhold

    Inventor： Bernd Gallenkamp ,  Lothar Rohe ,  Albrecht Marhold

    IPC: C07D231/16 ,  A01N43/56 ,  C07D231/14

    CPC classification number: C07D231/14

    Abstract: A new process for the preparation of a known 1,3-dimethyl-5-fluoro-pyrazole-4-carboxanilide of the formula ##STR1## in which Ar represents optionally substituted phenyl, which process comprises a) reacting in a first stage, 1,3-dimethyl-5-chloro-pyrazole-4-carbonyl chloride with a fluoride, if appropriate in the presence of a diluent, andb) reacting in a second stage, the 1,3-dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride obtained in this reaction with an aniline of the formula H.sub.2 N--Ar in which Ar has the abovementioned meaning, if appropriate in the presence of an acid acceptor and if appropriate in the presence of a diluent. 1,3-Dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride as a new compound.

    Abstract translation: 用于制备式IMAMA的已知1,3-二甲基-5-氟 - 吡唑-4-甲酰苯胺的新方法，其中Ar表示任选取代的苯基，该方法包括：a）在第一阶段中反应1 如果合适的话，在稀释剂的存在下，使用3-氟-2-甲基-3-二甲基-5-氯 - 吡唑-4-碳酰氯，和b）在第二阶段中使1,3-二甲基-5-氟 - 在该反应中获得的式IV-羰基氟与式H2N-阿林的苯胺反应，其中Ar具有上述含义，如果合适，在酸受体的存在下和在稀释剂存在下适当的话。 1,3-二甲基-5-氟 - 吡唑-4-羰基氟化物。

    4-Amino-5-thione-1,2,4-triazines
    4.
    发明授权
    4-Amino-5-thione-1,2,4-triazines 失效
    4-氨基-5-硫酮-1,2,4-三嗪

    公开(公告)号：US4058525A

    公开(公告)日：1977-11-15

    申请号：US670911

    申请日：1976-03-26

    Applicant: Wolfgang Hofer ,  Fritz Maurer ,  Hans-Jochem Riebel ,  Lothar Rohe ,  Ludwig Eue ,  Robert R. Schmidt

    Inventor： Wolfgang Hofer ,  Fritz Maurer ,  Hans-Jochem Riebel ,  Lothar Rohe ,  Ludwig Eue ,  Robert R. Schmidt

    IPC: C07D253/06 ,  A01N43/707 ,  C07D253/075 ,  C07D295/13

    CPC classification number: C07D253/075 ,  A01N43/707 ,  C07D295/13

    Abstract: The invention provides new 4-amino-5-thione-1,2,4-triazine (4,5-H) of the formula ##STR1## in which R is alkyl of up to 8 carbon atoms, cycloalkyl of from 5 to 7 carbon atoms, cycloalkenyl of from 5 to 7 carbon atoms, phenyl, which can optionally be mono-substituted or polysubstituted by halogen, or alkoxyalkyl of from 1 to 4 carbon atoms per alkyl and alkoxy moiety, andR' is hydrogen or alkyl of up to 4 carbon atoms;Which are outstandingly effective as herbicides, particularly as selective herbicides.

    Abstract translation: 本发明提供了新颖的式（IMAGE）的4-氨基-5-硫酮-1,2,4-三嗪（4,5-H），其中R是至多8个碳原子的烷基，5至7个的环烷基 碳原子，5至7个碳原子的环烯基，苯基，其可以任选被卤素单取代或多取代，或每个烷基和烷氧基部分具有1至4个碳原子的烷氧基烷基，R'是氢或烷基 至4个碳原子; 作为除草剂特别有效，特别是选择性除草剂。

    Process for the preparation of 1,3-dimethyl-5-fluoro-pyrazole-4-carboxanilides
    7.
    发明授权
    Process for the preparation of 1,3-dimethyl-5-fluoro-pyrazole-4-carboxanilides 失效
    制备1,3-二甲基-5-氟 - 吡唑-4-甲酰苯胺的方法

    公开(公告)号：US5675016A

    公开(公告)日：1997-10-07

    申请号：US755678

    申请日：1996-11-25

    Applicant: Bernd Gallenkamp ,  Lothar Rohe ,  Albrecht Marhold

    Inventor： Bernd Gallenkamp ,  Lothar Rohe ,  Albrecht Marhold

    IPC: C07D231/16 ,  A01N43/56 ,  C07D231/14

    CPC classification number: C07D231/14

    Abstract: A new process for the preparation of a known 1,3-dimethyl-5-fluoro-pyrazole-4-carboxanilide of the formula ##STR1## in which Ar represents optionally substituted phenyl, which process comprises a) reacting in a first stage, 1,3-dimethyl-5-chloro-pyrazole-4-carbonyl chloride with a fluoride, if appropriate in the presence of a diluent, andb) reacting in a second stage, the 1,3-dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride obtained in this reaction with an aniline of the formula H.sub.2 N--Ar in which Ar has the abovementioned meaning, if appropriate in the presence of an acid acceptor and if appropriate in the presence of a diluent. 1,3-Dimethyl-5-fluoro-pyrazole-4-carbonyl fluoride as a new compound.

    Abstract translation: 用于制备式IMAMA的已知1,3-二甲基-5-氟 - 吡唑-4-甲酰苯胺的新方法，其中Ar表示任选取代的苯基，该方法包括：a）在第一阶段中反应1 如果合适的话，在稀释剂的存在下，使用3-氟-2-甲基-3-二甲基-5-氯 - 吡唑-4-碳酰氯，和b）在第二阶段中使1,3-二甲基-5-氟 - 在该反应中获得的式IV-羰基氟与式H2N-阿林的苯胺反应，其中Ar具有上述含义，如果合适，在酸受体的存在下和在稀释剂存在下适当的话。 1,3-二甲基-5-氟 - 吡唑-4-羰基氟化物。

    O-�1-substituted-6-pyridazinon(3)yl!-thionoalkanephosphonic acid esters for combating insects and acarids
    8.
    发明授权
    O-�1-substituted-6-pyridazinon(3)yl!-thionoalkanephosphonic acid esters for combating insects and acarids 失效
    O- {8 1-取代-6-哒嗪酮（3）（用于防治昆虫和螨类的9-硫代烷基膦酸酯

    公开(公告)号：US4097592A

    公开(公告)日：1978-06-27

    申请号：US708669

    申请日：1976-07-26

    Applicant: Wolfgang Hofer ,  Fritz Maurer ,  Hans-Jochem Riebel ,  Lothar Rohe ,  Rolf Schroder ,  Ingeborg Hammann ,  Wolfgang Behrenz ,  Bernhard Homeyer

    Inventor： Wolfgang Hofer ,  Fritz Maurer ,  Hans-Jochem Riebel ,  Lothar Rohe ,  Rolf Schroder ,  Ingeborg Hammann ,  Wolfgang Behrenz ,  Bernhard Homeyer

    IPC: A01N57/24 ,  A01P7/02 ,  A01P7/04 ,  C07F9/6509 ,  C07F9/65 ,  A01N9/36

    CPC classification number: C07F9/650929 ,  A01N57/24

    Abstract: O-�1-substituted-6-pyridazinon(3)yl!-thionoalkanephosphonic acid esters of the formula ##STR1## in which R.sub.1 and R.sub.2 each independently is alkyl with 1 to 7 carbon atoms, R.sub.3 is alkyl, cyanoalkyl, alkylcarbonylalkyl, carbalkoxyalkyl, hydroxyalkyl, alkylthioalkyl or halogenalkyl with 1 to 4 carbon atoms per alkyl radical, alkenyl or alkynyl with 3 to 5 carbon atoms, benzyl, benzyl carrying at least one substituent selected from halogen and alkyl with 1 to 3 carbon atoms, phenyl, phenyl carrying at least one substituent selected from nitro, halogen, alkyl with 1 to 3 carbon atoms and carbalkoxy with 1 to 4 carbon atoms, morpholinomethyl or piperidinomethyl,R.sub.4 and R.sub.5 each independently is hydrogen or alkyl with 1 to 3 carbon atoms, and X and Y each independently is oxygen or sulfur, Which possess insecticidal and acaricidal properties.

    Abstract translation: 具有式“IMAGE”的O- [1-取代-6-哒嗪酮（3）基] - 硫代烷基膦酸酯，其中R 1和R 2各自独立地为具有1至7个碳原子的烷基，R 3为烷基，氰基烷基，烷基羰基烷基， ，每个烷基具有1至4个碳原子的羟基烷基，烷硫基烷基或卤代烷基，具有3至5个碳原子的烯基或炔基，苄基，带有至少一个选自卤素和具有1至3个碳原子的烷基的取代基的苄基，苯基， 选自硝基，卤素，具有1至3个碳原子的烷基和具有1至4个碳原子的烷氧基的至少一个取代基，吗啉代甲基或哌啶子基，R 4和R 5各自独立地是氢或具有1至3个碳原子的烷基，X和Y 各自独立地是氧或硫，具有无毒的杀虫剂和杀虫剂性质。

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