摘要:
A process for producing polyacrylonitrile-base precursor fibers for production of carbon fibers, which comprises spinning a spinning dope containing 10 to 25 wt % of a polyacrylonitrile-base polymer having an intrinsic viscosity of 2.0 to 10.0 by extruding the spinning dope from a spinneret by a wet spinning or a dry wet spinning method, drying and heat-treating fibers obtained by the spinning, and then steam drawing the resulting fibers, wherein the linear extrusion rate of the polyacrylonitrile-base polymer from the spinneret is 2 to 15 m/min. Carbon fibers which are produced by stabilizing-carbonizing treatment of the polyacrylonitrile-base precursor fibers and which have a strand tensile modulus of 320 to 380 GPa and a conduction electron density of 3.0×1019 to 7.0×1019 spins/g as determined by electron spin resonance.
摘要翻译:一种制造用于生产碳纤维的聚丙烯腈基前体纤维的方法,其包括通过将纺丝原液从喷丝头挤出而纺丝纺丝原液,该纺丝原液含有10-25重量%的特性粘度为2.0至10.0的聚丙烯腈基聚合物 湿式纺丝或干式湿式纺丝方法,通过纺丝得到的纤维的干燥和热处理,然后对所得纤维进行蒸汽拉伸,其中来自喷丝板的聚丙烯腈基聚合物的线性挤出速率为2〜15m / min 。 通过使聚丙烯腈类前体纤维进行稳定碳化处理而得到的碳纤维,其股线拉伸模量为320〜380GPa,导电电子密度为3.0×1019〜7.0×1019,通过电子自旋测定 谐振。
摘要:
A method of manufacturing a polyacrylonitrile fiber includes a spinning process in which a spinning dope including polyacrylonitrile is spun; a first drawing process; a drying process; and a second hot drawing process in this order.
摘要:
A process for producing polyacrylonitrile-base precursor fibers for production of carbon fibers, which comprises spinning a spinning dope containing 10 to 25 wt % of a polyacrylonitrile-base polymer having an intrinsic viscosity of 2.0 to 10.0 by extruding the spinning dope from a spinneret by a wet spinning or a dry wet spinning method, drying and heat-treating fibers obtained by the spinning, and then steam drawing the resulting fibers, wherein the linear extrusion rate of the polyacrylonitrile-base polymer from the spinneret is 2 to 15 m/min. Carbon fibers which are produced by stabilizing-carbonizing treatment of the polyacrylonitrile-base precursor fibers and which have a strand tensile modulus of 320 to 380 GPa and a conduction electron density of 3.0×1019 to 7.0×1019 spins/g as determined by electron spin resonance.
摘要翻译:一种制造用于生产碳纤维的聚丙烯腈基前体纤维的方法,其包括通过将纺丝原液从喷丝头挤出而纺丝纺丝原液,该纺丝原液含有10-25重量%的特性粘度为2.0至10.0的聚丙烯腈基聚合物 湿式纺丝或干式湿式纺丝方法,通过纺丝得到的纤维的干燥和热处理,然后对所得纤维进行蒸汽拉伸,其中来自喷丝板的聚丙烯腈基聚合物的线性挤出速率为2〜15m / min 。 通过使聚丙烯腈类前体纤维进行稳定碳化处理而得到的碳纤维,其股线拉伸模量为320〜380GPa,导电电子密度为3.0×1019〜7.0×1019,通过电子自旋测定 谐振。
摘要:
A method for calculating area values of a pattern written by using a charged particle beam, includes virtually dividing a pattern into a plurality of mesh-like first square regions surrounded by first grids defined at intervals of a predetermined size, virtually dividing the pattern into a plurality of mesh-like second square regions surrounded by second grids defined at intervals of the predetermined size, wherein the second grids being positionally deviated from the first grids by a half of the predetermined size, distributing an area value of a sub-pattern in each of the second square regions to a plurality of apexes of each of the second square regions such that a center-of-gravity position of the sub-pattern does not change, wherein the sub-pattern being a part of the pattern, and outputting the distributed area values as area values, for correcting a proximity effect, defined at the center position of each of the first square regions.
摘要:
A method of manufacturing a polyacrylonitrile fiber includes a spinning process in which a spinning dope including polyacrylonitrile is spun; a first drawing process; a drying process; and a second hot drawing process in this order.
摘要:
A process for producing polyacrylonitrile-base precursor fibers for production of carbon fibers, which comprises spinning a spinning dope containing 10 to 25 wt % of a polyacrylonitrile-base polymer having an intrinsic viscosity of 2.0 to 10.0 by extruding the spinning dope from a spinneret by a wet spinning or a dry wet spinning method, drying and heat-treating fibers obtained by the spinning, and then steam drawing the resulting fibers, wherein the linear extrusion rate of the polyacrylonitrile-base polymer from the spinneret is 2 to 15 m/min.
摘要翻译:一种制造用于生产碳纤维的聚丙烯腈基前体纤维的方法,其包括通过将纺丝原液从喷丝头挤出而纺丝纺丝原液,该纺丝原液含有10-25重量%的特性粘度为2.0至10.0的聚丙烯腈基聚合物 湿式纺丝或干式湿式纺丝方法,通过纺丝得到的纤维的干燥和热处理,然后对所得纤维进行蒸汽拉伸,其中来自喷丝板的聚丙烯腈基聚合物的线性挤出速率为2〜15m / min 。
摘要:
A method for calculating area values of a pattern written by using a charged particle beam, includes virtually dividing a pattern into a plurality of mesh-like first square regions surrounded by first grids defined at intervals of a predetermined size, virtually dividing the pattern into a plurality of mesh-like second square regions surrounded by second grids defined at intervals of the predetermined size, wherein the second grids being positionally deviated from the first grids by a half of the predetermined size, distributing an area value of a sub-pattern in each of the second square regions to a plurality of apexes of each of the second square regions such that a center-of-gravity position of the sub-pattern does not change, wherein the sub-pattern being a part of the pattern, and outputting the distributed area values as area values, for correcting a proximity effect, defined at the center position of each of the first square regions.