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    Microwave-assisted chromatography preparation
    3.
    发明授权
    Microwave-assisted chromatography preparation 有权
    微波辅助色谱法制备

    公开(公告)号：US07939785B2

    公开(公告)日：2011-05-10

    申请号：US12020711

    申请日：2008-01-28

    Applicant: Michael Collins, Sr. ,  Wyatt P. Hargett, Jr. ,  James Edward Thomas ,  E. Keller Barnhardt ,  Michael Collins, Jr.

    Inventor： Michael Collins, Sr. ,  Wyatt P. Hargett, Jr. ,  James Edward Thomas ,  E. Keller Barnhardt ,  Michael Collins, Jr.

    IPC: H05B6/64

    CPC classification number: H05B6/806 ,  F26B3/347 ,  F26B5/048 ,  F26B9/003 ,  F26B21/14 ,  G01N1/44 ,  G01N30/06 ,  G01N2030/567

    Abstract: An instrument and associated method are disclosed for preparing samples for column chromatography. The method includes the steps of applying microwave energy to a sample composition containing at least one solvent to encourage a chemical reaction and generate desired products, thereafter mixing an absorbent media with the sample to absorb the solvent, the media being compatible with liquid chromatography that will separate the expected products, being chemically inert to the expected products, and being added in an amount sufficient to provide a substantially dry mixture of the media and the sample, but less than an amount that overly broadens the resolution of the sample during liquid chromatography, thereafter applying microwave energy to the dry mixture of the media and the sample to thereby encourage the solvent to evaporate under the influence of the microwave energy, and thereafter adding the dry mixture of the media and the remaining sample to a liquid chromatography column and separating the components of the remaining sample for identification and purification purposes.

    Abstract translation: 公开了用于制备用于柱色谱法的样品的仪器和相关方法。 该方法包括以下步骤：向含有至少一种溶剂的样品组合物施加微波能量以促进化学反应并产生所需产物，然后将吸收介质与样品混合以吸收溶剂，该介质与液相色谱相容， 将期望的产品分离，对预期产品具有化学惰性，并且以足以提供介质和样品的基本上干燥的混合物的量加入，但小于在液相色谱法过度扩大样品分辨率的量， 然后将微波能量施加到介质和样品的干燥混合物中，从而促使溶剂在微波能量的影响下蒸发，然后将介质和剩余样品的干混合物加入液相色谱柱中， 剩余样品的组分用于鉴定和纯化目的。

    MICROWAVE-ASSISTED CHROMATOGRAPHY PREPARATION
    4.
    发明申请
    MICROWAVE-ASSISTED CHROMATOGRAPHY PREPARATION 有权
    微波辅助色谱准备

    公开(公告)号：US20080116363A1

    公开(公告)日：2008-05-22

    申请号：US12020711

    申请日：2008-01-28

    Applicant: MICHAEL COLLINS ,  WYATT HARGETT ,  JAMES THOMAS ,  MICHAEL COLLINS ,  E. BARNHARDT

    Inventor： MICHAEL COLLINS ,  WYATT HARGETT ,  JAMES THOMAS ,  MICHAEL COLLINS ,  E. BARNHARDT

    IPC: H05H3/02

    CPC classification number: H05B6/806 ,  F26B3/347 ,  F26B5/048 ,  F26B9/003 ,  F26B21/14 ,  G01N1/44 ,  G01N30/06 ,  G01N2030/567

    Abstract: An instrument and associated method are disclosed for preparing samples for column chromatography. The method includes the steps of applying microwave energy to a sample composition containing at least one solvent to encourage a chemical reaction and generate desired products, thereafter mixing an absorbent media with the sample to absorb the solvent, the media being compatible with liquid chromatography that will separate the expected products, being chemically inert to the expected products, and being added in an amount sufficient to provide a substantially dry mixture of the media and the sample, but less than an amount that overly broadens the resolution of the sample during liquid chromatography, thereafter applying microwave energy to the dry mixture of the media and the sample to thereby encourage the solvent to evaporate under the influence of the microwave energy, and thereafter adding the dry mixture of the media and the remaining sample to a liquid chromatography column and separating the components of the remaining sample for identification and purification purposes.

    Abstract translation: 公开了用于制备用于柱色谱法的样品的仪器和相关方法。 该方法包括以下步骤：向含有至少一种溶剂的样品组合物施加微波能量以促进化学反应并产生所需产物，然后将吸收介质与样品混合以吸收溶剂，该介质与液相色谱相容， 将期望的产品分离，对预期产品具有化学惰性，并且以足以提供介质和样品的基本上干燥的混合物的量加入，但小于在液相色谱法过度扩大样品分辨率的量， 然后将微波能量施加到介质和样品的干燥混合物中，从而促使溶剂在微波能量的影响下蒸发，然后将介质和剩余样品的干混合物加入液相色谱柱中， 剩余样品的组分用于鉴定和纯化目的。

    Microwave-Assisted Chromatography Preparation
    5.
    发明申请
    Microwave-Assisted Chromatography Preparation 有权
    微波辅助色谱法制备

    公开(公告)号：US20060261058A1

    公开(公告)日：2006-11-23

    申请号：US11456997

    申请日：2006-07-12

    Applicant: Michael Collins ,  Wyatt Hargett ,  James Thomas ,  Michael Collins ,  E. Barnhardt

    Inventor： Michael Collins ,  Wyatt Hargett ,  James Thomas ,  Michael Collins ,  E. Barnhardt

    IPC: B01L9/00

    CPC classification number: H05B6/806 ,  F26B3/347 ,  F26B5/048 ,  F26B9/003 ,  F26B21/14 ,  G01N1/44 ,  G01N30/06 ,  G01N2030/567

    Abstract: An instrument and associated method are disclosed for preparing samples for column chromatography. The method includes the steps of applying microwave energy to a sample composition containing at least one solvent to encourage a chemical reaction and generate desired products, thereafter mixing an absorbent media with the sample to absorb the solvent, the media being compatible with liquid chromatography that will separate the expected products, being chemically inert to the expected products, and being added in an amount sufficient to provide a substantially dry mixture of the media and the sample, but less than an amount that overly broadens the resolution of the sample during liquid chromatography, thereafter applying microwave energy to the dry mixture of the media and the sample to thereby encourage the solvent to evaporate under the influence of the microwave energy, and thereafter adding the dry mixture of the media and the remaining sample to a liquid chromatography column and separating the components of the remaining sample for identification and purification purposes.

    Abstract translation: 公开了用于制备用于柱色谱法的样品的仪器和相关方法。 该方法包括以下步骤：向含有至少一种溶剂的样品组合物施加微波能量以促进化学反应并产生所需产物，然后将吸收介质与样品混合以吸收溶剂，该介质与液相色谱相容， 将期望的产品分离，对预期产品具有化学惰性，并且以足以提供介质和样品的基本上干燥的混合物的量加入，但小于在液相色谱法过度扩大样品分辨率的量， 然后将微波能量施加到介质和样品的干燥混合物中，从而促使溶剂在微波能量的影响下蒸发，然后将介质和剩余样品的干混合物加入液相色谱柱中， 剩余样品的组分用于鉴定和纯化目的。

    Microwave-assisted chromatography preparation
    6.
    发明申请
    Microwave-assisted chromatography preparation 有权
    微波辅助色谱法制备

    公开(公告)号：US20060038118A1

    公开(公告)日：2006-02-23

    申请号：US10923243

    申请日：2004-08-20

    Applicant: Michael Collins ,  Wyatt Hargett ,  James Thomas ,  Michael Collins ,  E. Barnhardt

    Inventor： Michael Collins ,  Wyatt Hargett ,  James Thomas ,  Michael Collins ,  E. Barnhardt

    IPC: H05H3/02

    CPC classification number: H05B6/806 ,  F26B3/347 ,  F26B5/048 ,  F26B9/003 ,  F26B21/14 ,  G01N1/44 ,  G01N30/06 ,  G01N2030/567

    Abstract: An instrument and associated method are disclosed for preparing samples for column chromatography. The method includes the steps of applying microwave energy to a sample composition containing at least one solvent to encourage a chemical reaction and generate desired products, thereafter mixing an absorbent media with the sample to absorb the solvent, the media being compatible with liquid chromatography that will separate the expected products, being chemically inert to the expected products, and being added in an amount sufficient to provide a substantially dry mixture of the media and the sample, but less than an amount that overly broadens the resolution of the sample during liquid chromatography, thereafter applying microwave energy to the dry mixture of the media and the sample to thereby encourage the solvent to evaporate under the influence of the microwave energy, and thereafter adding the dry mixture of the media and the remaining sample to a liquid chromatography column and separating the components of the remaining sample for identification and purification purposes.

    Abstract translation: 公开了用于制备用于柱色谱法的样品的仪器和相关方法。 该方法包括以下步骤：向含有至少一种溶剂的样品组合物施加微波能量以促进化学反应并产生所需产物，然后将吸收介质与样品混合以吸收溶剂，该介质与液相色谱相容， 将期望的产品分离，对预期产品具有化学惰性，并且以足以提供介质和样品的基本上干燥的混合物的量加入，但小于在液相色谱法过度扩大样品分辨率的量， 然后将微波能量施加到介质和样品的干燥混合物中，从而促使溶剂在微波能量的影响下蒸发，然后将介质和剩余样品的干混合物加入液相色谱柱中， 剩余样品的组分用于鉴定和纯化目的。

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