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    Methods and systems for the selective formation of thiourethane bonds and compounds formed therefrom
    1.
    发明申请
    Methods and systems for the selective formation of thiourethane bonds and compounds formed therefrom 审中-公开
    用于选择性形成硫代氨基甲酸酯键的方法和系统及由其形成的化合物

    公开(公告)号：US20090124762A1

    公开(公告)日：2009-05-14

    申请号：US11983388

    申请日：2007-11-08

    Applicant: Chad W. Brown ,  Mitchell D. Refvik ,  Jim D. Byers ,  Roger A. Patton

    Inventor： Chad W. Brown ,  Mitchell D. Refvik ,  Jim D. Byers ,  Roger A. Patton

    IPC: C08G18/28

    CPC classification number: C08G18/71 ,  C08G18/18 ,  C08G18/3876

    Abstract: The present techniques relate to thiourethane compositions formed by reacting a reactive composition containing active molecules having an average of at least one thiol group per active molecule and an average of at least one hydroxyl group per active molecule with a monomer composition containing monomer molecules having an average of at least two isocyanate groups per monomer molecule. The reactions are performed in the presence of an amine catalyst, which may preferentially react thiol groups over hydroxyl groups, thus forming a thiourethane composition having, on average, more hydroxyl groups than thiol groups and more thiourethane groups than urethane groups, on a normalized basis.

    Abstract translation: 本技术涉及硫代氨基甲酸酯组合物，其通过使含有活性分子的活性组分含有每个活性分子平均至少一个硫醇基并且每个活性分子至少一个羟基的平均值与含有具有平均值的单体分子的单体组合物反应而形成 每个单体分子具有至少两个异氰酸酯基团。 反应在胺催化剂的存在下进行，胺催化剂可以优先反应羟基上的硫醇基团，从而形成硫代氨基甲酸酯组合物，其平均比巯基更多的羟基和比氨基甲酸酯基团更多的硫代氨基甲酸酯基团 。

    Process and catalyst for synthesis of mercaptans and sulfides from alcohols
    2.
    发明授权
    Process and catalyst for synthesis of mercaptans and sulfides from alcohols 有权
    从醇合成硫醇和硫化物的方法和催化剂

    公开(公告)号：US07399893B2

    公开(公告)日：2008-07-15

    申请号：US11302038

    申请日：2005-12-13

    Applicant: Daniel M. Hasenberg ,  Mitchell D. Refvik

    Inventor： Daniel M. Hasenberg ,  Mitchell D. Refvik

    IPC: C07C921/00

    CPC classification number: C07C319/08 ,  C07C319/14 ,  C07C321/04 ,  C07C321/22

    Abstract: A process and catalyst blend for selectively producing mercaptans and sulfides from alcohols. The alcohol is reacted with hydrogen sulfide, in the presence of a catalyst blend containing a hydrotreating catalyst and a dehydration catalyst to convert the alcohol to mercaptan or sulfide in one-pass. The alcohols can include primary and secondary alcohols. The mercaptan or sulfide having less than about 30% unreacted alcohol contained therein.

    Abstract translation: 用于从醇选择性地制备硫醇和硫化物的方法和催化剂共混物。 在含有加氢处理催化剂和脱水催化剂的催化剂共混物存在下，使醇与硫化氢反应，将醇转化成硫醇或硫化物。 醇可以包括伯醇和仲醇。 其中含有少于约30％未反应的醇的硫醇或硫化物。

    Polythiourethane compositions and processes for making and using same
    4.
    发明授权
    Polythiourethane compositions and processes for making and using same 有权
    聚硫氨酯组合物及其制备和使用方法

    公开(公告)号：US08003748B2

    公开(公告)日：2011-08-23

    申请号：US11204728

    申请日：2005-08-16

    Applicant: Jim D. Byers ,  Mitchell D. Refvik ,  Chad W. Brown ,  Michael S. Matson ,  Michael S. Hankinson

    Inventor： Jim D. Byers ,  Mitchell D. Refvik ,  Chad W. Brown ,  Michael S. Matson ,  Michael S. Hankinson

    IPC: C08G18/00

    CPC classification number: C08G18/3876

    Abstract: Polythiourethane polymer compositions, methods of making the polythiourethane polymer compositions, and methods of using the polythiourethane polymer compositions are provided. The polythiourethane can be produced by contacting a thiol ester composition and an isocyanate to produce a mixture and then heating the mixture to produce the polythiourethane polymer. In some embodiments, the thiol ester compositions include thiol esters, hydroxy thiol esters, and cross-linked thiol esters.

    Abstract translation: 提供聚硫氨酯聚合物组合物，制备聚硫氨酯聚合物组合物的方法，以及使用聚硫氨酯聚合物组合物的方法。 聚硫氨酯可以通过使硫羟酸酯组合物和异氰酸酯接触以制备混合物，然后加热混合物以制备聚硫氨酯聚合物来制备。 在一些实施方案中，硫羟酸酯组合物包括硫醇酯，羟基硫羟酸酯和交联的硫醇酯。

    Thiol ester compositions and processes for making and using same
    5.
    发明授权
    Thiol ester compositions and processes for making and using same 有权
    硫醇酯组合物及其制备和使用方法

    公开(公告)号：US07781484B2

    公开(公告)日：2010-08-24

    申请号：US11059792

    申请日：2005-02-17

    Applicant: Jim D. Byers ,  Mitchell D. Refvik ,  Chad W. Brown

    Inventor： Jim D. Byers ,  Mitchell D. Refvik ,  Chad W. Brown

    IPC: A61K31/21 ,  C07C327/08

    CPC classification number: C05C9/00 ,  C05G3/0023 ,  C05G3/0029 ,  C07C327/22 ,  C08G75/00 ,  C08G75/04 ,  C08G75/26 ,  C11C3/00 ,  C05G3/0035

    Abstract: Thiol ester compositions, methods of making the thiol ester compositions, and methods of using the thiol ester compositions are provided. In some embodiments, the thiol ester compositions include thiol esters, hydroxy thiol esters and cross-linked thiol esters. The thiol ester composition can be used to produce cross-linked thiol esters, sulfonic acid-containing esters, sulfonate containing esters and thioacrylate containing esters. The thiol ester compositions can be used to produce polythiourethanes. The polythiourethanes can be used in fertilizers and fertilizer coatings.

    Abstract translation: 提供硫醇酯组合物，制备硫羟酸酯组合物的方法，以及使用硫羟酸酯组合物的方法。 在一些实施方案中，硫羟酸酯组合物包括硫醇酯，羟基硫羟酸酯和交联的硫羟酸酯。 硫醇酯组合物可用于制备交联硫醇酯，含磺酸酯，含磺酸酯和含硫丙烯酸酯的酯。 硫醇酯组合物可用于制备聚氨基甲酸乙酯。 聚硫氨酯可用于肥料和肥料涂料。

    Process to isomerize 1-butene to 2-butene
    7.
    发明授权
    Process to isomerize 1-butene to 2-butene 失效
    将1-丁烯异构化为2-丁烯的方法

    公开(公告)号：US06852901B2

    公开(公告)日：2005-02-08

    申请号：US10156582

    申请日：2002-05-28

    Applicant: Dan M. Hasenberg ,  Mitchell D. Refvik ,  Michael S. Matson

    Inventor： Dan M. Hasenberg ,  Mitchell D. Refvik ,  Michael S. Matson

    IPC: C07C5/25

    CPC classification number: C07C5/2506 ,  Y10S585/906 ,  C07C11/08

    Abstract: A process is provided to produce a 2-alkene product from a 1-alkene-containing feed stream. The process comprises contacting the 1-alkene-containing feed stream in a reactor zone to isomerize the 1-alkene-containing feed stream to produce the 2-alkene product. More specifically, a process is provided to produce a 2-butene product from a 1-butene containing feed stream.

    Abstract translation: 提供了从含1-烯烃的进料流产生2-烯烃产物的方法。 该方法包括在反应器区中使含1-烯烃的进料流接触异构化含1-烯烃的进料流以产生2-烯烃产物。 更具体地，提供了从含1-丁烯的进料流产生2-丁烯产物的方法。

    Graded catalyst bed for methyl mercaptan synthesis
    9.
    发明授权
    Graded catalyst bed for methyl mercaptan synthesis 有权
    分级催化剂床用于甲硫醇合成

    公开(公告)号：US07645906B2

    公开(公告)日：2010-01-12

    申请号：US11691615

    申请日：2007-03-27

    Applicant: Daniel M Hasenberg ,  Mitchell D Refvik

    Inventor： Daniel M Hasenberg ,  Mitchell D Refvik

    IPC: C07C319/00

    CPC classification number: B01J35/0006 ,  B01J23/882 ,  B01J23/883 ,  B01J35/0026 ,  B01J2208/00805 ,  C07C319/08 ,  C07C321/04

    Abstract: A process and graded catalyst bed for selectively producing methyl mercaptan from methanol. The methanol is reacted with hydrogen sulfide, in the presence of a graded catalyst bed containing at least three types of nickel or cobalt molybdenum alumina catalysts to convert the methanol to methyl mercaptan in one-pass. At least one of the hydrotreating catalysts can contain aluminium phosphate. Use of the graded catalyst bed prevents the formation of a hot spot within the graded catalyst bed. The methyl mercaptan having less than about 30 wt. % unreacted methanol contained therein.

    Abstract translation: 一种用于从甲醇中选择性生产甲硫醇的工艺和分级催化剂床。 在含有至少三种类型的镍或钴钼氧化铝催化剂的分级催化剂床的存在下，使甲醇与硫化氢反应，以一次通过将甲醇转化成甲硫醇。 至少一种加氢处理催化剂可以含有磷酸铝。 使用分级催化剂床防止在分级催化剂床内形成热点。 甲硫醇的含量小于约30wt。 ％未反应的甲醇。

    Method of making 2-thiols
    10.
    发明授权
    Method of making 2-thiols 有权
    制备2-硫醇的方法

    公开(公告)号：US07217843B2

    公开(公告)日：2007-05-15

    申请号：US11115775

    申请日：2005-04-27

    Applicant: Daniel M. Hasenberg ,  Mitchell D. Refvik

    Inventor： Daniel M. Hasenberg ,  Mitchell D. Refvik

    IPC: C07C319/00

    CPC classification number: C07C319/04

    Abstract: A process for selectively making 2-thiols from alpha olefins is described. The process includes contacting a linear or branched alpha olefin having with H2S in the presence of a catalyst and recovering the 2-thiol from a product mixture. The catalyst includes a support and at least one metal selected from Group IIIA-VIIIA and the branched olefin is branched at the 3-position or higher with respect to the olefin double bond. Compositions wherein the 2-thiols are substantially free of 1-thiol and 3-thiol isomers are also described.

    Abstract translation: 描述了从α-烯烃选择性制备2-硫醇的方法。 该方法包括在催化剂存在下使具有H 2 S的直链或支链α-烯烃接触并从产物混合物中回收2-硫醇。 催化剂包括载体和选自IIIA-VIIIA族的至少一种金属，支化烯烃相对于烯烃双键在3位或更高分支。 还描述了其中2-硫醇基本上不含1-硫醇和3-硫醇异构体的组合物。

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