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    Alkoxylated aminopolyethers, a process for their preparation
    1.
    发明授权
    Alkoxylated aminopolyethers, a process for their preparation 失效
    烷氧基化氨基聚醚，其制备方法

    公开(公告)号：US4739094A

    公开(公告)日：1988-04-19

    申请号：US807388

    申请日：1985-12-10

    Applicant: Jan Mazanek ,  Hanns P. Muller ,  Roland Nast ,  Wolfgang Oberkirch ,  Franz-Moritz Richter ,  Walter Schafer

    Inventor： Jan Mazanek ,  Hanns P. Muller ,  Roland Nast ,  Wolfgang Oberkirch ,  Franz-Moritz Richter ,  Walter Schafer

    IPC: F23K1/02 ,  C08G65/26 ,  C08G65/32 ,  C10L1/32

    CPC classification number: C10L1/326 ,  C08G65/2624

    Abstract: New alkoxylated aminopolyethers of the formula ##STR1## in which Q denotes a polyalkylene oxide radical which has a valency corresponding to n, which has a structure derived from an aminopolyether by removal of the terminal amino groups and which has an average molecular weight of 82 to 30,000,A.sub.1 and A.sub.2 denote identical or different mono- or polyalkylene oxide radicals of the type (RO).sub.y,whereineach radical R represents an alkylene radical with 2 to 40 C atoms andy represents an integer from 1 to 200,B.sub.1 and B.sub.2 denote identical or different mono- or polyalkylene oxide radicals of the type (R'O).sub.z,whereinat least 50% of the R' radicals represent a --CH.sub.2 --CH.sub.2 -- group,the other R' radicals which may be present each represent an alkylene radical with 3 to 40 C atoms andz represents an integer from 1 to 300,Z denotes hydrogen, ##STR2## wherein M.sup..sym. represents one equivalent of a metal ion or represents NH.sub.4.sup..sym. andn denotes an integer from 1 to 30,a process for their preparation and coal/water slurries containing them.

    Abstract translation: 其中Q表示具有对应于n的化合价的聚亚烷基氧基的新的烷氧基化氨基聚醚，其具有通过除去末端氨基而衍生自氨基聚醚的结构，其平均分子量为82〜 30,000，A1和A2表示类型（RO）y相同或不同的单 - 或聚环氧烷基，其中每个基团R表示具有2至40个C原子的亚烷基，y表示1至200的整数，B1和B2 表示类型（R'O）z的相同或不同的单 - 或聚环氧烷基团，其中至少50％的R'基团表示-CH 2 -CH 2 - 基团，可以存在的另一个R'基团表示 具有3至40个C原子的亚烷基，z表示1至300的整数，Z表示氢，其中M（+）表示1当量的金属离子或表示NH 4（+），n表示 1〜30，其制备方法和煤/ 含水的泥浆含有它们。

    Process for the production of polyisocyanates of isocyanurate structure
    3.
    发明授权
    Process for the production of polyisocyanates of isocyanurate structure 失效
    制备异氰脲酸酯结构的多异氰酸酯的方法

    公开(公告)号：US3996223A

    公开(公告)日：1976-12-07

    申请号：US626404

    申请日：1975-10-28

    Applicant: Pramod Gupta ,  Roland Nast ,  Erwin Windemuth

    Inventor： Pramod Gupta ,  Roland Nast ,  Erwin Windemuth

    IPC: C08G18/00 ,  C08G18/02 ,  C07D251/04

    CPC classification number: C08G18/022 ,  Y10S521/902

    Abstract: Soluble polyisocyanates of isocyanurate structure are produced by heating polyisocyanates in the presence of Mannich bases and carbamic acid esters of isocyanates and secondary alcohols. When such a process is used, the polymerization reactions begin without incubation times and the catalysts need not be inactivated by introducing additives because they deactivate themselves at high temperatures.

    Abstract translation: 异氰脲酸酯结构的可溶多异氰酸酯是通过在异氰酸酯和仲醇的曼尼希碱和氨基甲酸酯的存在下加热多异氰酸酯来制备的。 当使用这种方法时，聚合反应开始于没有孵育时间，并且催化剂不需要通过引入添加剂而失活，因为它们在高温下自身失活。

    Process for the production of oligoesters containing hydroxy groups and their use
    5.
    发明授权
    Process for the production of oligoesters containing hydroxy groups and their use 失效
    生产含有羟基的低聚酯及其用途的方法

    公开(公告)号：US4757097A

    公开(公告)日：1988-07-12

    申请号：US65486

    申请日：1987-06-23

    Applicant: Manfred Dietrich ,  Manfred Kapps ,  Klaus Konig ,  Roland Nast

    Inventor： Manfred Dietrich ,  Manfred Kapps ,  Klaus Konig ,  Roland Nast

    IPC: C08G18/42 ,  C07C67/08 ,  C07C69/42 ,  C07C69/657 ,  C08G18/50 ,  C08G63/66 ,  C08G65/32 ,  C08G69/40 ,  C08G18/14

    CPC classification number: C07C69/42 ,  C07C67/08 ,  C07C69/657

    Abstract: Oligoesters having hydroxyl groups and an OH number of from 200 to 600 mg KOH/g are made by reacting a cyclic dicarboxylic acid anhydride in which no halogen is present with a polyfunctional alcohol or dialkanolamine in a molar ratio of from 1:0.5 to 1:1.5 at a temperature of from 50.degree. to 150.degree. C. to form the corresponding dicarboxylic acid semiester and/or semiamide. This semiester and/or semiamide is then alkoxylated with ethylene oxide and/or propylene oxide in the presence of a catalyst at 80.degree. to 150.degree. C. The equivalent ratio of acid groups to alkylene oxide groups is from 1:0.8 to 1:1.7. The catalysts are reaction products of alkoxides with at least 3 C-atoms with ammonia, piperidine, piperazine and/or C.sub.2 -C.sub.6 aliphatic, polyamines, preferably diamines in which all of the NH-functional groups have been alkoxylated. The resultant oligoester may then be reacted with a polyisocyanate optionally in the presence of known additives, such as blowing agents and catalysts.

    Abstract translation: 通过使不存在卤素的环状二羧酸酐与多官能醇或二烷醇胺以摩尔比为1：0.5〜1：1的比例使羟基和OH值为200〜600mg KOH / g的低聚酯制成。 1.5，温度为50-150℃，形成相应的二羧酸半酯和/或半酰胺。 然后将该半酯和/或半酰胺在80-150℃的催化剂存在下，用环氧乙烷和/或环氧丙烷进行烷氧基化。酸基与环氧烷基的当量比为1:0.8至1:1.7 。 催化剂是具有至少3个C原子的烷氧基与氨，哌啶，哌嗪和/或C 2 -C 6脂族多胺，优选其中所有NH官能团已被烷氧基化的二胺的反应产物。 然后可将所得的低聚酯与多异氰酸酯反应，任选地在已知的添加剂如发泡剂和催化剂的存在下进行。

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