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    Preparation of liquid formulations of basic azo dyes
    1.
    发明授权
    Preparation of liquid formulations of basic azo dyes 有权
    碱性偶氮染料液体配方的制备

    公开(公告)号：US06743901B1

    公开(公告)日：2004-06-01

    申请号：US10410397

    申请日：2003-04-10

    申请人： Michael Schmitt ,  Roland Merger ,  Rainer Tresch

    发明人： Michael Schmitt ,  Roland Merger ,  Rainer Tresch

    IPC分类号： C09B3304

    CPC分类号： C09B67/0076 ,  C09B41/001 ,  C09B44/06 ,  C09B69/065

    摘要： A process for preparing liquid formulations of dyes of the general formula I where the variables are as defined in the specification by diazotizing an amine of the formula II and then coupling the diazonium salt onto a compound of the formula III and also optionally adding solubilizing additives, which comprises effecting said diazotizing at a pH set to an acidic value using pure methanesulfonic acid or at least 20 mol % mixtures of methanesulfonic acid in monobasic acids.

    摘要翻译： 制备通式I的染料的液体制剂的方法，其中变量如本说明书中所定义，通过将式II的胺重氮化，然后将重氮盐偶联到式III的化合物上，还任选地加入增溶添加剂，其包括实现 在使用纯甲磺酸或甲磺酸在一元酸中的至少20摩尔％混合物的pH设定为酸值时进行重氮化。

    Azoxy dyes and copper complexes thereof
    3.
    发明授权
    Azoxy dyes and copper complexes thereof 失效
    偶氮染料及其铜络合物

    公开(公告)号：US06903197B2

    公开(公告)日：2005-06-07

    申请号：US10795585

    申请日：2004-03-09

    申请人： Rainer Tresch ,  Karl-Heinz Etzbach ,  Rüdiger Sens ,  Claudia Kräh

    发明人： Rainer Tresch ,  Karl-Heinz Etzbach ,  Rüdiger Sens ,  Claudia Kräh

    IPC分类号： C09B35/039 ,  C09B35/029 ,  C09B43/10 ,  C09B43/44 ,  C09B45/28

    CPC分类号： C09B45/28 ,  C09B43/10 ,  C09B43/44

    摘要： Azoxy dyes of the general formula I in the form of the free acid where n is 0 or 1, each R1 is selected from the group consisting of methoxy, hydroxyl and carboxyl, each R2 is selected from the group consisting of carboxyl, amino, C1-C4-alkylamino, allylamino, benzylamino and methoxycarbonylmethylamino, and the phenyl rings A may additionally be substituted by C1-C8-alkyl, unsubstituted or methyl- or halogen-substituted phenyl, hydroxyl, amino, nitro, halogen, carboxyl, N-benzylcarbamoyl, unsubstituted or nitro-, halogen-, C1-C4-alkoxy- or acetoxy-substituted phenylcarbamoyl and naphthylcarbamoyl or be benzofused, their copper complexes, a process for preparing the copper complex dyes, azoxy dyes of the formula I in their partially or completely deacylated form, their copper complexes, colorants comprising these azoxy dyes and/or their copper complexes and also their use for dyeing and printing natural or synthetic substrates.

    摘要翻译： n为0或1的游离酸形式的通式I的芳氧基染料，每个R 1选自甲氧基，羟基和羧基，每个R 2 选自羧基，氨基，C 1 -C 4 - 烷基氨基，烯丙基氨基，苄基氨基和甲氧基羰基甲基氨基，苯基环A可以另外 被C 1 -C 8 - 烷基取代，未取代的或甲基或卤素取代的苯基，羟基，氨基，硝基，卤素，羧基，N-苄基氨基甲酰基，未取代的 或硝基，卤素，C 1 -C 4 - 烷氧基或乙酰氧基取代的苯基氨基甲酰基和萘基氨基甲酰基或苯并稠合，它们的铜配合物，制备铜的方法 复合染料，它们部分或完全脱酰基形式的式I的偶氮染料，它们的铜络合物，包含这些偶氮染料和/或它们的铜络合物的着色剂，以及它们用于染色和印刷的用途 ral或合成底物。

    Method of producing paper, paperboard and cardboard
    4.
    发明授权
    Method of producing paper, paperboard and cardboard 失效
    生产纸张，纸板和纸板的方法

    公开(公告)号：US06673206B1

    公开(公告)日：2004-01-06

    申请号：US10069719

    申请日：2002-02-28

    申请人： Friedrich Linhart ,  Bernd Dirks ,  Rainer Tresch ,  Bernhard Mohr ,  Dietrich Fehringer

    发明人： Friedrich Linhart ,  Bernd Dirks ,  Rainer Tresch ,  Bernhard Mohr ,  Dietrich Fehringer

    IPC分类号： D21H1755

    CPC分类号： D21H17/22 ,  D21H21/10

    摘要： Paper, board and cardboard are produced by a process in which a paper stock is drained in the presence of condensates of basic amino acids with sheet formation. In particular, homo- and cocondensates of lysine and the crosslinked condensates obtainable therefrom by reaction with crosslinking agents are used in amounts of from 0.01 to 5% by weight, based on dry paper stock, as a means of increasing the dry and wet strength and the absorptivity of paper, for fixing anionic dyes and interfering substances in the paper, for increasing the drainage rate and the retention as well as the efficiency of synthetic anionic and cationic retention aids in the production of paper, board and cardboard by draining a paper stock with sheet formation.

    摘要翻译： 纸，纸板和纸板通过在存在碱性氨基酸与片材形成的冷凝物的情况下排干纸浆的方法来生产。 特别地，通过与交联剂反应可得到的赖氨酸和交联缩合物的均聚物和共缩合物的用量为干浆料的0.01至5重量％，作为提高干湿强度的方法，以及 纸张的吸收性，用于固定纸中的阴离子染料和干扰物质，用于增加排水速率和保留率以及合成阴离子和阳离子助留剂在通过排出纸料的纸张，纸板和纸板的生产中的效率 与片形成。

    Azoxy dyes and their Cu complexes
    9.
    发明授权
    Azoxy dyes and their Cu complexes 失效
    偶氮染料及其Cu配合物

    公开(公告)号：US06727351B1

    公开(公告)日：2004-04-27

    申请号：US09936432

    申请日：2001-09-13

    申请人： Rainer Tresch ,  Karl-Heinz Etzbach ,  Rüdiger Sens ,  Claudia Kräh

    发明人： Rainer Tresch ,  Karl-Heinz Etzbach ,  Rüdiger Sens ,  Claudia Kräh

    IPC分类号： C09B4310

    CPC分类号： C09B45/28 ,  C09B43/10 ,  C09B43/44

    摘要： Azoxy dyes of the general formula I in the form of the free acid where n is 0 or 1, each R1 is selected from the group consisting of methoxy, hydroxyl and carboxyl, each R2 is selected from the group consisting of carboxyl, amino, C1-C4-alkylamino, allylamino, benzylamino and methoxycarbonylmethylamino, and the phenyl rings A may additionally be substituted by C1-C8-alkyl, unsubstituted or methyl- or halogen-substituted phenyl, hydroxyl, amino, nitro, halogen, carboxyl, N-benzylcarbamoyl, unsubstituted or nitro-, halogen-, C1-C4-alkoxy- or acetoxy-substituted phenylcarbamoyl and naphthylcarbamoyl or be benzofused, their copper complexes, a process for preparing the copper complex dyes, azoxy dyes of the formula I in their partially or completely deacylated form, their copper complexes, colorants comprising these azoxy dyes and/or their copper complexes and also their use for dyeing and printing natural or synthetic substrates.

    摘要翻译： 游离酸式的通式I的偶氮染料为0或1，每个R 1选自甲氧基，羟基和羧基，每个R 2选自羧基，氨基 ，C 1 -C 4 - 烷基氨基，烯丙基氨基，苄基氨基和甲氧基羰基甲基氨基，并且苯环A可另外被C 1 -C 8 - 烷基，未取代的或甲基或卤素取代的苯基，羟基，氨基，硝基，卤素，羧基，N - 苄基氨基甲酰基，未取代的或硝基 - ，卤素 - ，C 1 -C 4 - 烷氧基 - 或乙酰氧基取代的苯基氨基甲酰基和萘基氨基甲酰基或被苯并稠合，它们的铜络合物，制备铜络合物染料的方法，式I的氧化偶氮染料在其部分 或完全脱酰基形式，它们的铜络合物，包含这些偶氮染料和/或其铜络合物的着色剂，以及它们用于染色和印刷天然或合成底物的用途。

    Cationic azo-dyes
    10.
    发明授权
    Cationic azo-dyes 失效
    阳离子偶氮染料

    公开(公告)号：US06346609B1

    公开(公告)日：2002-02-12

    申请号：US09807999

    申请日：2001-05-04

    申请人： Karl-Heinz Etzbach ,  Torsten Freund ,  Rainer Tresch

    发明人： Karl-Heinz Etzbach ,  Torsten Freund ,  Rainer Tresch

    IPC分类号： C09B35023

    CPC分类号： C09B44/02 ,  C09B67/0046 ,  Y10S534/03

    摘要： Cationic azo dyes of the general formula I where R1, R2, R3, A1, A2, B1, B2, An⊖, n and K have the meaning given in the specification are prepared and used for the dyeing and printing of natural or synthetic substrates and mixtures thereof.

    摘要翻译： 具有通式I的阳离子偶氮染料，其中R1，R2，R3，A1，A2，B1，B2，An⊖，n和K具有本说明书中给出的含义，并用于天然或合成底物的染色和印刷， 其混合物。