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    Water- and oil-repellent compositions
    1.
    发明授权
    Water- and oil-repellent compositions 有权
    防水和防油组合物

    公开(公告)号：US06960642B2

    公开(公告)日：2005-11-01

    申请号：US10339418

    申请日：2003-01-09

    申请人： Chetan P. Jariwala ,  Thomas P. Klun ,  Jeffrey G. Linert ,  Richard M. Stern

    发明人： Chetan P. Jariwala ,  Thomas P. Klun ,  Jeffrey G. Linert ,  Richard M. Stern

    IPC分类号： C09K3/18 ,  C03C17/32 ,  C08G63/682 ,  C08G63/688 ,  D06M13/236 ,  D06M13/438 ,  D06M15/507 ,  C08G63/68 ,  C08G63/02 ,  C08G69/00 ,  C08G69/44 ,  C08G75/00

    CPC分类号： C03C17/32 ,  C03C17/324 ,  C08G63/6824 ,  C08G63/6884 ,  D06M13/236 ,  D06M13/438 ,  D06M15/507 ,  D06M15/5075 ,  D06M2200/11 ,  D06M2200/12

    摘要： Fiber, fabric, film, molded or blown article comprising a water- and oil-repellent composition comprising a melt blend of components (a) and (b) in which: (a) comprises a repellency-imparting, fluorochemical composition comprising at least one fluorine-containing aromatic ester oligomer comprising (1) at least two repeat units derived or derivable from the reaction of at least one dicarboxylic acid (or a derivative thereof) and at least one polyol, with the proviso that either the dicarboxylic acid (or derivative) or the polyol (or both) is aromatic or heteroaromatic, and (2) fluorochemical endgroups derived or derivable from the reaction of (i) the dicarboxylic acid (or derivative) and at least one fluorine-containing monoalcohol, or (ii) the polyol and at least one fluorine-containing monocarboxylic acid; and (b) comprises a treatable substrate material; with the proviso that, when the treatable substrate material comprises a mixture of at least two polymers, the mixture is non-stratifying.

    摘要翻译： 1.一种纤维，织物，薄膜，模制或吹塑制品，其包含防水和拒油组合物，其包含组分（a）和（b）的熔融共混物，其中：（a）包含驱斥剂的含氟化合物组合物，其包含至少一种 含氟芳族酯低聚物包含（1）至少两个衍生或衍生自至少一种二羧酸（或其衍生物）和至少一种多元醇的反应的重复单元，条件是二羧酸（或衍生物） ）或多元醇（或两者）是芳香族或杂芳族的，和（2）由（i）二羧酸（或衍生物）和至少一种含氟一元醇的反应衍生或衍生的含氟端基，或（ii） 多元醇和至少一种含氟一元羧酸; 和（b）包括可处理的基材; 条件是当可处理基材材料包含至少两种聚合物的混合物时，该混合物是非分层的。

    Water- and oil-repellent composition
    2.
    发明授权
    Water- and oil-repellent composition 失效
    防水防油组合物

    公开(公告)号：US06586522B1

    公开(公告)日：2003-07-01

    申请号：US09592105

    申请日：2000-06-12

    申请人： Chetan P. Jariwala ,  Thomas P. Klun ,  Jeffrey G. Linert ,  Richard M. Stern

    发明人： Chetan P. Jariwala ,  Thomas P. Klun ,  Jeffrey G. Linert ,  Richard M. Stern

    IPC分类号： C08J300

    CPC分类号： C03C17/32 ,  C03C17/324 ,  C08G63/6824 ,  C08G63/6884 ,  D06M13/236 ,  D06M13/438 ,  D06M15/507 ,  D06M15/5075 ,  D06M2200/11 ,  D06M2200/12

    摘要： A water- and oil-repellent composition comprises (a) a repellency-imparting, fluorochemical composition comprising at least one fluorine-containing aromatic ester oligomer comprising (1) at least two repeat units derived or derivable from the reaction of at least one dicarboxylic acid (or a derivative thereof) and at least one polyol, with the proviso that either the dicarboxylic acid (or derivative) or the polyol (or both) is aromatic or heteroaromatic, and (2) fluorochemical endgroups derived or derivable from the reaction of (i) the dicarboxylic acid (or derivative) and at least one fluorine-containing monoalcohol, or (ii) the polyol and at least one fluorine-containing monocarboxylic acid; and (b) a treatable substrate; with the proviso that, when the treatable substrate comprises a mixture of at least two polymers, the mixture is non-stratifying.

    摘要翻译： 拒水拒油剂组合物包含（a）具有排斥性的氟化合物组合物，其包含至少一种含氟芳族酯低聚物，其包含（1）至少两个衍生或衍生自至少一种二羧酸 （或其衍生物）和至少一种多元醇，条件是二羧酸（或衍生物）或多元醇（或两者）都是芳族或杂芳族的，和（2）衍生或可衍生自（ i）二羧酸（或衍生物）和至少一种含氟一元醇，或（ii）多元醇和至少一种含氟一元羧酸; 和（b）可处理基材; 条件是当可处理基材包含至少两种聚合物的混合物时，该混合物是非分层的。

    Process for the preparation of fluoroaliphatic aminocarboxylate surfactants
    6.
    发明授权
    Process for the preparation of fluoroaliphatic aminocarboxylate surfactants 失效
    制备氟代氨基甲酸酯表面活性剂的方法

    公开(公告)号：US5144069A

    公开(公告)日：1992-09-01

    申请号：US626739

    申请日：1990-12-13

    申请人： Richard M. Stern ,  Richard A. Guenthner ,  Roger R. Alm ,  Thomas K. Wilkinson

    发明人： Richard M. Stern ,  Richard A. Guenthner ,  Roger R. Alm ,  Thomas K. Wilkinson

    IPC分类号： C07C303/40 ,  C07C311/09

    CPC分类号： C07C311/09

    摘要： A process for the synthesis of the fluorochemical compound having formulaR.sub.f SO.sub.2 N(CHR.sup.2 --CHR.sup.2 COO.sup.-) R.sup.1 N.sup.+ (R).sub.2 Hwherein R.sub.f is a fluoraliphatic radical containing at least 3 carbon atoms. The synthesis involves reaction of compounds of formula R.sub.f SO.sub.2 N(H)R.sup.1 N(R).sub.2 and CHR.sup.2 .dbd.CH.sup.2 COOH in solution at elevated temperatures. The process can be used to synthesize the fluoroaliphatic amphoteric amino carboxylate surfactant having the formula:C.sub.6 F.sub.13 SO.sub.2 N(C.sub.2 H.sub.4 COO.sup.-) C.sub.3 H.sub.6 N.sup.+ (CH.sub.3).sub.2 Hwhich compound is useful in aqueous film-forming foamable concentrates for extinguishing flammable liquid fires.

    摘要翻译： 合成具有式RfSO 2 N（CHR 2 -CH 2 COO-）R 1 N +（R）2H的含氟化合物的方法，其中Rf是含有至少3个碳原子的氟脂肪基。 该合成包括式R f SO 2 N（H）R 1 N（R）2和CHR 2 = CH 2 COOH的化合物在升高的温度下在溶液中的反应。 该方法可用于合成具有下列通式的氟代脂族两性氨基羧酸盐表面活性剂：C6F13SO2N（C2H4COO-）C3H6N +（CH3）2H）该化合物可用于水性成膜可发泡浓缩物，用于扑灭易燃液体火焰。

    Intermediates for the preparation of 8,9-dihalobenzo[ij]quinolizine carboxylic acids
    7.
    发明授权
    Intermediates for the preparation of 8,9-dihalobenzo[ij]quinolizine carboxylic acids 失效
    用于制备8,9-二卤苯并[i]喹嗪化羧酸的中间体

    公开(公告)号：US4691016A

    公开(公告)日：1987-09-01

    申请号：US768127

    申请日：1985-08-22

    申请人： Richard M. Stern

    发明人： Richard M. Stern

    IPC分类号： C07D455/04 ,  C07D471/04

    CPC分类号： C07D455/04

    摘要： The compounds 8-bromo-6,7-dihydro-9-fluoro-5-methyl-1-oxo-1H,5H-benzo[ij]quinolizine-2-carboxylic acid and 8-chloro-6,7-dihydro-9-fluoro-5-methyl-1-oxo-1H,5H-benzo[ij]quinolizine-2-carboxylic acid are disclosed as potent antimicrobials. Pharmaceutically-acceptable carboxylate salts, acyl chlorides, esters and alkylaminoalkyl ester salts of the acids are also disclosed.

    摘要翻译： 化合物8-溴-6,7-二氢-9-氟-5-甲基-1-氧代-1H，5H-苯并[i]喹嗪-2-羧酸和8-氯-6,7-二氢-9 - 氟-5-甲基-1-氧代-1H，5H-苯并[i]喹啉盐e-2-羧酸被公开为有效的抗微生物剂。 还公开了酸的药学上可接受的羧酸盐，酰氯，酯和烷基氨基烷基酯盐。

    Antimicrobial 8-substituted benzo [IJ]quinolizines
    8.
    发明授权
    Antimicrobial 8-substituted benzo [IJ]quinolizines 失效
    抗菌8-取代苯并[I]喹啉

    公开(公告)号：US4404207A

    公开(公告)日：1983-09-13

    申请号：US318929

    申请日：1981-11-06

    申请人： Richard M. Stern

    发明人： Richard M. Stern

    IPC分类号： C07D215/18 ,  C07D215/38 ,  C07D455/04 ,  A01N43/42 ,  A61K31/47

    CPC分类号： C07D455/04 ,  C07D215/18 ,  C07D215/38

    摘要： Antimicrobial compounds of the following formula are disclosed: ##STR1## wherein Het is selected from the goup consisting of pyrryl, pyrrolidyl, tetrazolyl of the formula ##STR2## wherein R.sup.1 is lower alkyl or benzyl and oxadiazolyl of the formula ##STR3## wherein R.sup.2 is lower alkyl, trifluoromethyl or --NH.phi.--; X is hydrogen and when Het is pyrryl or pyrrolidyl, X may be fluorine. Pharmaceutically acceptable carboxylate salts and esters of the acids are also disclosed.

    摘要翻译： 公开了下式的抗微生物化合物：其中Het选自由下式的吡咯，吡咯烷基，吡唑基，四唑基，其中R 1是下式的低级烷基或苄基和恶二唑基，其中R 2是 低级烷基，三氟甲基或-NH。 X是氢，当Het是吡咯基或吡咯烷基时，X可以是氟。 还公开了药学上可接受的羧酸盐和酸的酯。