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公开(公告)号：US20070049509A1
公开(公告)日：2007-03-01
申请号：US11511351
申请日：2006-08-29
申请人： Akira Yamamoto , Shoji Ichinohe
发明人： Akira Yamamoto , Shoji Ichinohe
IPC分类号： C11D1/66
摘要： A highly volatile electrical/electronic parts surfactant containing a polyether-modified silicone having one polyether chain in the molecule, wherein the surface tension at 25° C. of a 0.01 mass % aqueous solution thereof is 25 mN/m or less, the aforesaid silicone is expressed by the following average structural formula (1), and when heated from room temperature to 200° C. at a rate of 5° C./minute to 200° C. and maintained at a temperature of 200° C. for 100 minutes, the polyether-modified silicone completely volatilizes without leaving any remainder, and a method of manufacturing this highly volatile polyether-modified silicone are disclosed. AMe2SiO(MeASiO)nSiMe2A (1) In formula (1), any one of A is a substituent group expressed by the following general formula (2), the remaining A are methyl groups and n is an integer from 0-2. —CaH2aO(C2H4O)bR (2) In formula (2), a is 3-4, b is an integer from 1-7 and R is a methyl group or an ethyl group.
摘要翻译： 含有分子中具有一个聚醚链的聚醚改性硅酮的高挥发性电气/电子部件表面活性剂，其中0.01质量％水溶液在25℃下的表面张力为25mN / m以下，上述硅氧烷 由以下平均结构式（1）表示，当以5℃/分钟至200℃的温度从室温加热至200℃并保持在200℃的温度下保持100 分钟，聚醚改性硅氧烷完全挥发而不留下任何剩余部分，并且公开了制造这种高挥发性聚醚改性硅氧烷的方法。 <？in-line-formula description =“In-line Formulas”end =“lead”？>第二个二氧化硅（MeASiO）N 2 SiMe 2 在式（1）中，A中的任何一个是由以下通式（2）表示的取代基，其中，A是（1）<αin-line-formula description =“In-line Formulas”end =“tail” ），其余的A为甲基，n为0-2的整数。 <？in-line-formula description =“In-line Formulas”end =“lead”？ - - - - - - - - - - - - - - - - - - - - （2） R（2）<βin-line-formula description =“In-line Formulas”end =“tail”？>在式（ 2）中，a为3-4，b为1-7的整数，R为甲基或乙基。
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公开(公告)号：US20070015884A1
公开(公告)日：2007-01-18
申请号：US11483587
申请日：2006-07-11
申请人： Akira Yamamoto , Shoji Ichinohe , Eiichi Tabei
发明人： Akira Yamamoto , Shoji Ichinohe , Eiichi Tabei
CPC分类号： C08L63/00 , C07F7/0838 , C08G59/306 , C08K5/54 , C08L83/00
摘要： Epoxy-modified low molecular weight silicones are added to epoxy resins for reducing surface tension and improving fluidity.
摘要翻译： 将环氧改性的低分子量硅氧烷加入到环氧树脂中以降低表面张力并提高流动性。
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公开(公告)号：US06495651B1
公开(公告)日：2002-12-17
申请号：US09608004
申请日：2000-06-30
IPC分类号： C08G1822
CPC分类号： C08G18/8175 , C08G18/2063 , C08G18/222 , C08G18/672 , C08G18/61
摘要： A process for preparing an urethane compound for medical instruments, characterized by reacting a hydroxyl compound (A) with an isocyanate compound (B) in the absence of a catalyst or in the presence of a reaction catalyst other than an organic tin compound to give an urethane compound (I). According to the process, the urethane compound showing high safety can be easily prepared, in particular, while molecular weight of the compound is controlled.
摘要翻译： 一种用于医疗器械的氨基甲酸酯化合物的制备方法，其特征在于在不存在催化剂的情况下或在除有机锡化合物以外的反应催化剂存在下使羟基化合物（A）与异氰酸酯化合物（B）反应，得到 氨基甲酸酯化合物（I）。 根据该方法，可以容易地制备显示高安全性的氨基甲酸酯化合物，特别是在控制化合物的分子量时。
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公开(公告)号：US6015870A
公开(公告)日：2000-01-18
申请号：US161290
申请日：1998-09-28
CPC分类号： C07F7/1892
摘要： Polysulfide silanes: (RO).sub.3 SiC.sub.3 H.sub.6 S.sub.x C.sub.3 H.sub.6 Si(OR).sub.3 are reacted with an anhydrous sulfur compound: M.sup.1.sub.2 S or M.sup.2 S and a halogenoalkoxysilane: XC.sub.3 H.sub.6 Si(OR).sub.3 to form polysulfide silanes: (RO).sub.3 SiC.sub.3 H.sub.6 S.sub.y C.sub.3 H.sub.6 Si(OR).sub.3 wherein R is methyl or ethyl, x is a positive number of 3 to 6 on the average, M.sup.1 is an alkali metal or ammonium, M.sup.2 is an alkaline earth metal or zinc, X is a halogen, and y is a positive number less than x on the average. Short chain polysulfide silanes can be prepared with the industrial advantages of safety, high yields and low cost.
摘要翻译： 将多硫化硅烷：（RO）3SiC 3 H 6 S x C 3 H 6 Si（OR）3与无水硫化合物：M12S或M2S和卤代烷氧基硅烷：XC3H6Si（OR）3反应形成多硫化硅烷：（RO）3SiC 3 H 6 S 3 C 6 H 6 Si（OR）3，其中R为甲基或乙基 x是平均为3〜6的正数，M1为碱金属或铵，M2为碱土金属或锌，X为卤素，y为平均小于x的正数。 短链多硫硅烷可以安全，高产率，低成本的工业优点制备。
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公开(公告)号：US5739369A
公开(公告)日：1998-04-14
申请号：US634829
申请日：1996-04-19
申请人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
发明人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
IPC分类号： C09D183/08 , C03C17/30 , C09D183/04 , C09K3/18 , C07F7/10
摘要： A surface treating agent comprising a reaction product of (A) a fluoroalkyl group-containing alkoxysilane with (B) an amino group-containing alkoxysilane and optionally further with (C) an alkyl group-containing alkoxysilane is water soluble. The agent is diluted with water to form a solution for treating glass and other substrates to impart durable water repellency and other improved properties to the substrates.
摘要翻译： 包含（A）含氟烷基的烷氧基硅烷与（B）含氨基的烷氧基硅烷和任选地还含有（C）含烷基的烷氧基硅烷的反应产物的表面处理剂是水溶性的。 用水稀释试剂以形成用于处理玻璃和其它基材的溶液，以赋予基材持久的拒水性和其它改进的性能。
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公开(公告)号：US5519070A
公开(公告)日：1996-05-21
申请号：US350025
申请日：1994-11-29
IPC分类号： G02C7/04 , A61L27/00 , C08F290/00 , C08F290/06 , C08F299/08 , C08L55/00 , G02B1/04 , C08F18/20 , C08F230/08 , C08F283/00
CPC分类号： C08L55/005 , G02B1/043
摘要： A soft ocular lens material prepared by copolymerizing copolymer components consisting essentially of:(A) from 5 to 70 parts by weight of a fluorine-containing (meth)acrylate;(B) from 5 to 60 parts by weight of an alkoxy-containing (meth)acrylate;(C) from 3 to 45 parts by weight of a polysiloxane macromonomer having polymerizable groups at both terminals, of the formula I: ##STR1## (D) from 3 to 40 parts by weight of a polysiloxane macromonomer having polymerizable groups bonded via one or two urethane bonds to the siloxane main chain, of the formula II: ##STR2##
摘要翻译： 通过使基本上由以下组成的共聚物组分共聚得到的柔软眼透镜材料：（A）5-70重量份的含氟（甲基）丙烯酸酯; （B）5〜60重量份的含烷氧基的（甲基）丙烯酸酯; （C）3〜45重量份式（I）（D）的末端具有聚合性基团的聚硅氧烷大分子单体，3〜40重量份具有聚合性基团的聚硅氧烷大分子单体 通过与硅氧烷主链的一个或两个氨基甲酸酯键，式II（II）
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公开(公告)号：US5416180A
公开(公告)日：1995-05-16
申请号：US149530
申请日：1993-11-09
申请人： Yasuhiro Yokoyama , Noriko Iwata , Eri Ito , Shoji Ichinohe , Toshio Yamazaki
发明人： Yasuhiro Yokoyama , Noriko Iwata , Eri Ito , Shoji Ichinohe , Toshio Yamazaki
IPC分类号： C08F220/22 , C08F20/22 , C08F20/26 , C08F30/08 , C08F220/28 , C08F230/08 , G02B1/04 , G02C7/04 , C08F18/20
CPC分类号： G02B1/043 , C08F220/28 , C08F230/08
摘要： A soft ocular lens material obtained by copolymerizing polymerizable components comprising (A) a fluorine-containing (meth)acrylate having a hydroxyl group of the formula (I): ##STR1## wherein R.sup.1 is a hydrogen atom or a methyl group, R.sup.2 is a C.sub.5-15 perfluoroalkyl group, and n is 0 or 1, (B) a hydrophilic monomer, and (C) at least one monomer selected from the group consisting of silicon-containing (meth)acrylates and siloxane-containing styrene derivatives, wherein the ratio of the amount of the fluorine-containing (meth)acrylate (A) to the amount of the hydrophilic monomer (B) is from 20/80 to 70/30 by weight ratio, and the ratio of the total amount of the fluorine-containing (meth)acrylate (A) and the hydrophilic monomer (B) to the amount of the monomer (C) is from 30/70 to 90/10 by weight ratio.
摘要翻译： 通过使包含（A）具有式（I）的羟基的含氟（甲基）丙烯酸酯：其中R 1为氢原子或甲基的式（I）表示的可聚合组分共聚合得到的柔软的眼用透镜材料， R2是C5-15全氟烷基，n是0或1，（B）亲水性单体，和（C）至少一种选自含硅（甲基）丙烯酸酯和含硅氧烷的苯乙烯衍生物的单体 其中，所述含氟（甲基）丙烯酸酯（A）的量与所述亲水性单体（B）的配合量的比例为20/80〜70/30重量比， 含氟（甲基）丙烯酸酯（A）和亲水性单体（B）相对于单体（C）的含量为30/70〜90/10重量比。
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8.发明授权
公开(公告)号：US5276122A
公开(公告)日：1994-01-04
申请号：US929548
申请日：1992-08-14
申请人： Hisashi Aoki , Shoji Ichinohe , Kazuaki Sutoh
发明人： Hisashi Aoki , Shoji Ichinohe , Kazuaki Sutoh
CPC分类号： C08G77/26
摘要： A method of manufacturing aminogroup-containing polysiloxanes of uniform quality characterized in that a cyclic organopolysiloxane represented by the following general formula: ##STR1## and an aminoalkylpolysiloxane represented by the following general formula: ##STR2## are heated together in the presence of a basic catalyst.
摘要翻译： 一种制造均匀质量的含氨基聚硅氧烷的方法，其特征在于由以下通式表示的环状有机聚硅氧烷（*化学结构*）和由以下通式表示的氨基烷基聚硅氧烷（*化学结构*）在 碱性催化剂的存在。
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9.发明授权
公开(公告)号：US5104998A
公开(公告)日：1992-04-14
申请号：US703618
申请日：1991-05-21
申请人： Shoji Ichinohe
发明人： Shoji Ichinohe
CPC分类号： B01F17/0071 , C08G77/46
摘要： A novel organopolysiloxane compound, which has high surface activity to form an emulsion of the water-in-oil type of various hardly emulsifiable materials, is proposed. The organopolysiloxane compound is a dimethylpolysiloxane having two types of modifying groups including polyether or polyoxyalkylene groups on one hand and higher alkyl groups bonded to the silicon atoms through an ether linkage on the other hand bonded to the silicon atoms. Different from conventional dually modified dimethylpolysiloxanes as an emulsifying agent having modifying groups of polyether groups and higher alkyl groups directly bonded to the silicon atoms, the dually modified dimethylpolysiloxane of the invention can be synthesized easily in a one-step process of the reaction in addition to the advantage of excellent emulsifying activity for various kinds of hardly emulsifiable liquids as compared with conventional emulsifying agents.
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10.发明申请公开(公告)号：US20090299022A1
公开(公告)日：2009-12-03
申请号：US12472066
申请日：2009-05-26
申请人： Shoji Ichinohe
发明人： Shoji Ichinohe
IPC分类号： C07F7/08 , C08F230/08
CPC分类号： C08G77/045 , C07F7/0838 , C08G77/08 , G02B1/043 , C08L51/085
摘要： The present invention provides a hydrophilic silicone which has a predetermined number of silicon atoms and a high purity and is suitable for producing an ophthalmic device and a process for preparing the same.The silicone compound is represented by formula (1) with a purity of 95% by weight or higher, wherein m is one value out of the integers of from 3 to 10, n is one value out of the integers of from 1 to 10, R1 is one out of alkyl groups having 1 to 4 carbon atoms, and R2 is one out of a hydrogen atom and a methyl group.
摘要翻译： 本发明提供了具有预定数量的硅原子并且具有高纯度并且适于制造眼科装置的亲水性硅氧烷及其制备方法。 硅氧烷化合物由纯度为95重量％以上的式（1）表示，其中m为3〜10的整数中的1个，n为1〜10的整数之一， R 1是具有1至4个碳原子的烷基中的一个，R 2是氢原子和甲基中的一个。
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