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公开(公告)号：US20230002297A1
公开(公告)日：2023-01-05
申请号：US17777837
申请日：2020-12-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Arne Thaler , Achim Schmidt-Rodenkirchen , Mark W. Muggli , Konstantin Mierdel , Klaus Hintzer , Thorsten Gerdes , Denis Duchesne , Gregg D. Dahlke
IPC: C07C17/367
Abstract: The process produces a fluorinated olefin from a fluorinated copolymer having at least one of sulfonic acid groups, carboxylic acid groups, or salts thereof. The process includes heating the fluorinated copolymer at a first temperature not more than 450° C. to decompose at least one of the sulfonic acid groups, carboxylic acid groups, or salts thereof to form a partially pyrolyzed intermediate and subsequently heating the partially pyrolyzed intermediate at a second temperature of at least 550° C. to produce the fluorinated olefin.
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公开(公告)号：US11905178B2
公开(公告)日：2024-02-20
申请号：US18254671
申请日：2021-12-14
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Markus E. Hirschberg , Klaus Hintzer , Thomas W. Schoettle , Arne Thaler , Achim Schmidt-Rodenkirchen , Thorsten Gerdes , Konstantin Mierdel
Abstract: Methods of converting a variety of fluorinated materials into anhydrous hydrogen fluoride are described. The methods include thermally decomposing the fluorinated materials into a gaseous effluent comprising hydrogen fluoride and carbon dioxide. This gaseous effluent is then treated with carbon at a temperature of at least 830° C., converting the carbon dioxide to carbon monoxide (CO) and producing a gaseous product comprising the hydrogen fluoride, which can be condensed to generate anhydrous hydrogen fluoride. These methods can also be used to convert water contained in the gaseous effluent into hydrogen.
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公开(公告)号：US10358402B2
公开(公告)日：2019-07-23
申请号：US15516124
申请日：2015-09-30
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Tilman C. Zipplies , Klaus Hintzer , Monika A. Willert-Porada , Thorsten Gerdes , Jens Herdegen , Achim Schmidt-Rodenkirchen , Stephan Aschauer
IPC: C07C17/361 , C07C17/23 , B01J19/12 , B01J19/08 , C07C21/185
Abstract: Provided is a process for producing fluorinated alkenes by providing a microwave plasma in a reactor chamber, introducing a protective gas feed into the reactor chamber, and contacting a conversion feed comprising at least one fluorinated linear or branched alkane with the plasma. Also provided are an apparatus and the use of the process and the apparatus.
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公开(公告)号：US20240002228A1
公开(公告)日：2024-01-04
申请号：US18254671
申请日：2021-12-14
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Markus E. Hirschberg , Kalus Hintzer , Thomas W. Schoettle , Arne Thaler , Achim Schmidt-Rodenkirchen , Thorsten Gerdes , Konstantin Mierdel
IPC: C01B7/19
Abstract: Methods of converting a variety of fluorinated materials into anhydrous hydrogen fluoride are described. The methods include thermally decomposing the fluorinated materials into a gaseous effluent comprising hydrogen fluoride and carbon dioxide. This gaseous effluent is then treated with carbon at a temperature of at least 830° C., converting the carbon dioxide to carbon monoxide (CO) and producing a gaseous product comprising the hydrogen fluoride, which can be condensed to generate anhydrous hydrogen fluoride. These methods can also be used to convert water contained in the gaseous effluent into hydrogen.
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公开(公告)号：US09764963B2
公开(公告)日：2017-09-19
申请号：US14696652
申请日：2015-04-27
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Tilman Zipplies , Klaus Hintzer , Thorsten Gerdes , Achim Schmidt-Rodenkirchen , Sebastian Seidl , Thomas Berger
CPC classification number: C01F11/22 , C01B7/191 , C01B7/192 , C01P2004/61 , C01P2006/12 , C01P2006/20 , C01P2006/80
Abstract: The invention relates to a process for producing free-flowing calcium fluoride particles from a diluted aqueous solution of hydrogen fluoride comprising the step of reacting the diluted aqueous solution of hydrogen fluoride with calcium carbonate particles at a temperature of less than 50° C. The invention further relates to the use of the free-flowing calcium fluoride particles for the manufacturing of anhydrous hydrogen fluoride.
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Patent Agency Ranking
公开(公告)号：US11795126B2
公开(公告)日：2023-10-24
申请号：US17904611
申请日：2021-02-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Markus E. Hirschberg , Klaus Hintzer , Thomas G. Kolbeck , Matthias Wieland , Peter Bauer , Achim Schmidt-Rodenkirchen , Thorsten Gerdes
IPC: C07C17/367 , B01J8/08 , B01J8/10 , C08J11/14 , C10B53/07
CPC classification number: C07C17/367 , B01J8/085 , B01J8/10 , C08J11/14 , C10B53/07 , B01J2208/00442 , B01J2208/00867 , B01J2208/00884 , C08J2327/12 , C07C17/367 , C07C21/18 , C07C17/367 , C07C21/185
Abstract: Mechanical stirred bed reactors that incorporate a screen are described. Methods of using such reactors to process perfluoropolymers to form perfluorinated olefin monomers are also described. The reactors and methods may be used to upcycle filled perfluorinated materials.
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公开(公告)号：US20190276329A1
公开(公告)日：2019-09-12
申请号：US16302448
申请日：2017-05-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Tilman C. Zipplies , Klaus Hintzer , Monika A. Willert-Porada , Achim Schmidt-Rodenkirchen , Thomas F. Berger , Thorsten Gerdes , Christoph Schymura , Andreas P. Spiewok
Abstract: A process for generating calcium fluoride particles having a particle size (d50) of from about 15 μm to about 300 μm. The process features contacting a gas stream having gaseous hydrogen fluoride (HF) with a fluidized bed of calcium carbonate particles in a fluidized bed reactor.
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8.发明申请Method for the Production of Free Flowing Synthetic Calcium Fluoride and Use thereof 有权自由流动合成氟化钙的制备方法及其应用公开(公告)号：US20150353372A1
公开(公告)日：2015-12-10
申请号：US14696652
申请日：2015-04-27
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Tilman Zipplies , Klaus Hintzer , Thorsten Gerdes , Achim Schmidt-Rodenkirchen , Sebastian Seidl , Thomas Berger
CPC classification number: C01F11/22 , C01B7/191 , C01B7/192 , C01P2004/61 , C01P2006/12 , C01P2006/20 , C01P2006/80
Abstract: The invention relates to a process for producing free-flowing calcium fluoride particles from a diluted aqueous solution of hydrogen fluoride comprising the step of reacting the diluted aqueous solution of hydrogen fluoride with calcium carbonate particles at a temperature of less than 50° C.The invention further relates to the use of the free-flowing calcium fluoride particles for the manufacturing of anhydrous hydrogen fluoride.
Abstract translation: 本发明涉及从稀释的氟化氢水溶液中产生自由流动的氟化钙颗粒的方法，包括在低于50℃的温度下使稀释的氟化氢水溶液与碳酸钙颗粒反应的步骤。本发明 还涉及使用自由流动的氟化钙颗粒制造无水氟化氢。
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9.发明申请公开(公告)号：US20230090482A1
公开(公告)日：2023-03-23
申请号：US17908265
申请日：2021-04-09
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Arne Thaler , Andreas Rosin , Mark W. Muggli , Klaus Hintzer , Patrick K. Heimerdinger , Thorsten Gerdes , Denis Duchesne , Gregg D. Dahlke
IPC: H01M8/1039 , H01M8/1004 , H01M4/88
Abstract: A composite includes a fluorinated polymer and nanoparticles of a metal salt. The metal salt has a solubility product of not more than 1×10−4. The fluorinated polymer includes a fluorinated polymer backbone chain and a plurality of groups represented by formula —SO2X, in which each X is independently —NZH, —NZSO2(CF2)1-6SO2X′, —NZ[SO2(CF2)dSO2NZ]1-10SO2(CF2)dSO2X′ or —OZ, and Z is independently a hydrogen, an alkali-metal cation, or a quaternary ammonium cation, X′ is independently —NZH or —OZ, and each d is independently 1 to 6. A polymer electrolyte membrane, an electrode, and a membrane electrode assembly including the composite are also provided.
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公开(公告)号：US20170305820A1
公开(公告)日：2017-10-26
申请号：US15516124
申请日：2015-09-30
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Tilman C. Zipplies , Klaus Hintzer , Monika A. Willert-Porada , Thorsten Gerdes , Jens Herdegen , Achim Schmidt-Rodenkirchen , Stephan Aschauer
IPC: C07C17/361 , B01J19/12
CPC classification number: C07C17/361 , B01J19/088 , B01J19/126 , B01J2219/0875 , B01J2219/0896 , B01J2219/1206 , B01J2219/1293 , C07C17/23 , C07C21/185 , C07C21/18
Abstract: Provided is a process for producing fluorinated alkenes by providing a microwave plasma in a reactor chamber, introducing a protective gas feed into the reactor chamber, and contacting a conversion feed comprising at least one fluorinated linear or branched alkane with the plasma. Also provided are an apparatus and the use of the process and the apparatus.
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