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公开(公告)号：US3404131A
公开(公告)日：1968-10-01
申请号：US41026764
申请日：1964-11-10
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
CPC classification number: C08G18/724 , C08G18/10 , C08G18/4854 , Y10S528/903 , Y10S528/906 , C08G18/75 , C08G18/73 , C08G18/3234
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公开(公告)号：US3211781A
公开(公告)日：1965-10-12
申请号：US6561460
申请日：1960-10-28
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB , HINO JOHN B
CPC classification number: C07C227/22 , C07C2601/14 , C07C229/08
Abstract: An amino-acid ester is produced in the form of a salt with a halogen acid in a single operation by heating a lactam with an alcohol in the presence of a gaseous halogen acid and a substantial quantity of water until at least part of the lactam has undergone ring opening, and subsequently removing water from the reaction mixture by distillation. The halogen acid is preferably hydrogen chloride or hydrogen bromide and the water is preferably removed by azeotropic distillation, preferably with benzene or one of its inert substitution derivatives. The lactam and alcohol are preferably heated in the presence of 0,6-1,5 moles of water per mole of lactam and alcohols boiling at 100 DEG C. or above are preferred, several being specified. The free esters may be obtained from their salts by dissolution of the salt in water, neutralisation of the acid with a base, and extraction of the liberated ester with an organic solvent. Examples describe the preparation of the hydrochlorides of: (1) butyl e -aminocaproate; (2) 2-ethylhexyl e -aminocaproate; (3) n-octyl e -aminocaproate; (4) cyclohexyl e -aminocaproate; (5) n-decyl e -aminocaproate; (6) lauryl e -aminocaproate; (7) benzyl e -aminocaproate; (8) ethylene bise -aminocaproate; (9) n-butyl g -aminobutyrate.
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公开(公告)号：US3078301A
公开(公告)日：1963-02-19
申请号：US6589060
申请日：1960-10-31
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
IPC: C07C271/22 , C08K5/205
CPC classification number: C07C271/22 , C08K5/205
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公开(公告)号：US3383366A
公开(公告)日：1968-05-14
申请号：US41025764
申请日：1964-11-10
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
CPC classification number: C08G18/724 , C08G18/10 , Y10S528/906 , C08G18/75 , C08G18/3234 , C08G18/73
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公开(公告)号：US3047482A
公开(公告)日：1962-07-31
申请号：US83074359
申请日：1959-07-31
Applicant: ALLIED CHEM
Inventor： CHAO-SHING CHENG , BERNARD TAUB
IPC: B01J31/02 , C07C249/06 , C07C251/44
CPC classification number: B01J31/0231 , B01J31/0202 , B01J31/0207 , B01J31/0208 , B01J31/04 , C07C249/06 , Y10S204/903 , Y10S204/911 , Y10S204/912 , Y10S204/913 , Y10S204/914 , C07C251/44
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Patent Agency Ranking6.发明授权Preparation of polyurethane foam using arylenedicarbamic acid ester catalyst 失效使用亚芳基二氨基甲酸酯催化剂制备聚氨酯泡沫
公开(公告)号：US3001955A
公开(公告)日：1961-09-26
申请号：US71756658
申请日：1958-02-26
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
IPC: C08G18/18
CPC classification number: C08G18/1841
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7.发明授权Process for producing stable, undistilled tolylene diisocyanate compositions 失效用于生产稳定的，未蒸馏的甲苯二异氰酸酯组合物的方法
公开(公告)号：US3282975A
公开(公告)日：1966-11-01
申请号：US29328063
申请日：1963-07-08
Applicant: ALLIED CHEM
Inventor： FRIEDMAN CECIL A , BERNARD TAUB , WAGNER CHARLES R
IPC: C07C265/14 , C07C67/00 , C07C241/00
CPC classification number: C07C263/18 , C07C265/14
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8.发明授权Esters of epsilon-dicarboximido-caproic acids and polyvinyl resins plasticized therewith 失效ε-二羧酰基己酸和聚乙烯树脂的酯用其增塑
公开(公告)号：US3210313A
公开(公告)日：1965-10-05
申请号：US20557062
申请日：1962-06-27
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
IPC: C07D207/40 , C07D207/404 , C07D207/412 , C07D209/48 , C08K5/3417
CPC classification number: C07D207/404 , C07D207/412 , C07D209/48 , C08K5/3417
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公开(公告)号：US3194845A
公开(公告)日：1965-07-13
申请号：US34705264
申请日：1964-02-24
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB , HINO JOHN B
IPC: C07C201/16 , C07C205/05
CPC classification number: C07C201/16 , C07C2601/14 , C07C205/05
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公开(公告)号：US3036975A
公开(公告)日：1962-05-29
申请号：US78445259
申请日：1959-01-02
Applicant: ALLIED CHEM
Inventor： BERNARD TAUB
IPC: C08L63/00
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