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    Methods of preparing casting resins and coating compositions using polyols derived from high oleic acid content fatty acid mixtures
    1.
    发明授权
    Methods of preparing casting resins and coating compositions using polyols derived from high oleic acid content fatty acid mixtures 有权
    使用衍生自高油酸含量脂肪酸混合物的多元醇制备浇铸树脂和涂料组合物的方法

    公开(公告)号：US06730768B2

    公开(公告)日：2004-05-04

    申请号：US09297956

    申请日：1999-05-11

    申请人： Andreas Heidbreder ,  Roland Gruetzmacher ,  Ulrich Nagorny ,  Alfred Westfechtel

    发明人： Andreas Heidbreder ,  Roland Gruetzmacher ,  Ulrich Nagorny ,  Alfred Westfechtel

    IPC分类号： C08G1836

    CPC分类号： C08G18/36

    摘要： A method for preparing a polyol useful in the formation of an isocyanate casting resin or coating composition is presented involving the reaction of an essentially C18 fatty acid mixture with a monofunctional alcohol to form a fatty acid ester mixture, forming a epoxidized fatty acid ester mixture from the fatty acid ester mixture, and reacting the epoxidized mixture with an aliphatic alcohol to form a polyol. The polyol can be further reacted with an isocyanate to form a casting resin or coating composition. The fatty acid mixture contains at least 80 percent oleic acid. Polyols prepared by this method provide good color quality and improved color stability during storage when used in the production of isocyanate casting resins and coating compositions.

    摘要翻译： 提出了一种制备用于形成异氰酸酯浇铸树脂或涂料组合物的多元醇的方法，其涉及基本上C18脂肪酸混合物与单官能醇的反应以形成脂肪酸酯混合物，从而形成环氧化脂肪酸酯混合物 脂肪酸酯混合物，并使环氧化混合物与脂族醇反应形成多元醇。 多元醇可以进一步与异氰酸酯反应以形成浇铸树脂或涂料组合物。 脂肪酸混合物含有至少80％的油酸。 通过该方法制备的多元醇在用于异氰酸酯浇铸树脂和涂料组合物的制备中时，在储存期间提供了良好的颜色质量和改善的颜色稳定性。

    Polyurethanes with improved tear propagation resistance
    4.
    发明授权
    Polyurethanes with improved tear propagation resistance 失效
    具有改善的抗撕裂传播性的聚氨酯

    公开(公告)号：US06610811B1

    公开(公告)日：2003-08-26

    申请号：US09379938

    申请日：1999-08-24

    申请人： Alfred Westfechtel ,  Roland Gruetzmacher ,  Rainer Hoefer

    发明人： Alfred Westfechtel ,  Roland Gruetzmacher ,  Rainer Hoefer

    IPC分类号： C08J300

    CPC分类号： C09K3/1021 ,  C08G18/10 ,  C08G18/3212 ,  C08G18/4233 ,  C08G18/4875 ,  C09K2200/0252 ,  C08G18/36 ,  C08G18/42 ,  C08G18/48

    摘要： Polyurethanes having improved tear resistance which are the reaction product of the following components: A) a polyol component containing dimer diol and/or trimer triol and/or an OH-terminated polyester produced from polycarboxylic acids, preferably dimer fatty acid and/or trimer fatty acid, and diols and B) an isocyanate component containing prepolymers obtained by reacting polyfunctional isocyanates with dimer diol and/or trimer triol and/or an OH-terminated polyester produced from polycarboxylic acids, preferably dimer fatty acid and/or trimer fatty acid, and diols; and processes for their manufacture.

    摘要翻译： 具有改善的抗撕裂性的聚氨酯是以下组分的反应产物：A）含有二聚体二醇和/或三聚体三醇和/或由多元羧酸制成的OH封端的聚酯，优选二聚脂肪酸和/或三聚体脂肪 酸和二醇和B）含有预聚物的异氰酸酯组分，其通过多官能异氰酸酯与二聚二醇和/或三聚体三醇和/或由多元羧酸，优选二聚脂肪酸和/或三聚体脂肪酸制备的OH-端聚酯反应获得，和二醇 ; 及其制造工艺。

    Polyurethane resins
    5.
    发明授权
    Polyurethane resins 有权
    聚氨酯树脂

    公开(公告)号：US6046298A

    公开(公告)日：2000-04-04

    申请号：US125995

    申请日：1998-09-15

    申请人： Bernd Beuer ,  Roland Gruetzmacher ,  Andreas Heidbreder ,  Johann Klein

    发明人： Bernd Beuer ,  Roland Gruetzmacher ,  Andreas Heidbreder ,  Johann Klein

    IPC分类号： C08G18/32 ,  C08G18/08 ,  C08G18/36 ,  C08G18/42 ,  C08G18/40 ,  C08G18/64

    CPC分类号： C08G18/36 ,  C08G18/089 ,  C08G2101/00

    摘要： A process for producing a polyurethane resin having an extended gel time by reacting a polyol component with a polyisocyanate in an NCO:OH ratio of from 10:1 to 1:10 wherein the polyol component contains from 0.1% to 100% by weight of a randomized castor oil prepared by heating castor oil for between about 0.1 and 15 hours at a temperature of between about 100.degree. C. and 280.degree. C. in the presence of a basic lithium salt.

    摘要翻译： PCT No.PCT / EP97 / 00774 371日期：1998年9月15日 102（e）1998年9月15日PCT PCT 1997年2月19日PCT公布。 公开号WO97 / 31959 日本公报1997年9月4日制造通过使多元醇成分与多异氰酸酯以10:1〜1:10的比例反应而得到凝胶时间延长的聚氨酯树脂的制造方法，其中多元醇成分含有0.1〜100 通过在碱性锂盐存在下，在约100℃至280℃的温度下加热蓖麻油约0.1至15小时制备的随机蓖麻油的重量％。

    Method for producing compounds with terminal OH groups
    6.
    发明授权
    Method for producing compounds with terminal OH groups 有权
    生产具有末端OH基团的化合物的方法

    公开(公告)号：US06566563B1

    公开(公告)日：2003-05-20

    申请号：US09720890

    申请日：2001-05-04

    申请人： Alfred Westfechtel ,  Roland Gruetzmacher ,  Elke Grundt

    发明人： Alfred Westfechtel ,  Roland Gruetzmacher ,  Elke Grundt

    IPC分类号： C07C3118

    CPC分类号： C08G64/0208 ,  C08G18/44 ,  C08G64/305

    摘要： A process for making OH-terminated compounds involving: (a) combining at least one CH2OH-terminated diol and a titanium-containing catalyst to form a reaction mixture; (b) heating the reaction mixture to a temperature of from 110 to 160° C. to form a heated reaction mixture; (c) continuously adding dimethyl carbonate to the heated reaction mixture; (d) continuously distilling all methanol released from the heated reaction mixture; (e) heating the reaction mixture to a temperature of from 190 to 240° C. to form an OH-terminated product; (f) removing unreleased methanol and dimethyl carbonate from the reaction mixture under a pressure of less than 100 mbar; and (g) deactivating the titanium-containing catalyst by adding from 0.8 to 2 equivalents, based on the catalyst, of a 1 to 20% by weight aqueous solution of phosphoric acid to the reaction mixture, at a temperature of from 80 to 120° C.

    摘要翻译： 一种制备OH封端化合物的方法，包括：（a）将至少一种CH 2 OH封端的二醇和含钛催化剂混合以形成反应混合物; （b）将反应混合物加热至110至160℃的温度以形成加热的反应混合物; （c）向加热的反应混合物中连续加入碳酸二甲酯; （d）连续蒸馏从加热的反应混合物中释出的所有甲醇; （e）将反应混合物加热至190-240℃的温度以形成OH封端的产物; （f）在小于100毫巴的压力下从反应混合物中除去未发酵的甲醇和碳酸二甲酯; 和（g）通过向反应混合物中加入基于催化剂的0.8至2当量的1至20重量％的磷酸水溶液，在80至120℃的温度下使含钛催化剂失活 C。

    Polyurethane dispersions and their use as binders in stoving lacquers
    8.
    发明授权
    Polyurethane dispersions and their use as binders in stoving lacquers 失效
    聚氨酯分散体及其作为粘合剂在烤漆中的应用

    公开(公告)号：US5563206A

    公开(公告)日：1996-10-08

    申请号：US433485

    申请日：1995-05-11

    申请人： Ulrich Eicken ,  Alfred Westfechtel ,  Rainer Hoefer ,  Roland Gruetzmacher

    发明人： Ulrich Eicken ,  Alfred Westfechtel ,  Rainer Hoefer ,  Roland Gruetzmacher

    IPC分类号： C08G18/00 ,  C08G18/08 ,  C08G18/10 ,  C08G18/12 ,  C08G18/32 ,  C08G18/65 ,  C08G18/66 ,  C09D175/00 ,  C09D175/04 ,  C08G18/62

    CPC分类号： C08G18/6607 ,  C08G18/0804 ,  C08G18/0823 ,  C08G18/12 ,  C08G18/3212

    摘要： Aqueous polyurethane dispersions prepared in several stages by reactingA) aliphatic and/or aromatic di- and/or tri-isocyanates withB1) polyol mixtures containing dimer diols of 25 to 100% by weight of dimer diols and 0 to 75% by weight of other hydrophobic diols and/or polyols, the equivalent ratio of OH to NCO being 1:1.1 to 1:4, and simultaneously or subsequently withB2) chain-extending agents containing two terminal NCO-reactive groups, the chain-extending agents additionally containing either artionic or cationic groups or groups convertible into anionic or cationic groups by neutralization, the equivalent ratio of NCO-reactive groups to NCO groups theoretically still present after the reaction of A) with B1) being 1:0.9 to 1:4, and then optionally reactingC) the NCO groups theoretically still present in the polyurethanes after the reaction of A) with B1) and B2) with polyols containing at least three hydroxyl groups and/or amino alcohols containing at least two hydroxyl groups in an equivalent ratio of OH+amino groups to NCO of at least 3:1, and finally dispersing the polyurethanes obtained in water, the polyurethanes obtained being at least partly neutralized before or during dispersion where the chain extending agents B2) contain as additional groups those groups which are only converted into anionic or cationic groups by neutralization, are provided. Also provided is a process for the production of aqueous polyurethane dispersions and methods of using aqueous polyurethane dispersions so prepared as stoving lacquers.

    摘要翻译： PCT No.PCT / EP93 / 03045 Sec。 371日期1995年5月11日 102（e）日期1995年5月11日PCT 1993年11月2日PCT公布。 公开号WO94 / 11413 日期1994年5月26日通过使A）脂族和/或芳族二 - 和/或三异氰酸酯与B1二元醇混合物反应制备水性聚氨酯分散体，所述B1）多元醇混合物含有25至100重量％的二聚体二醇和0至75的二聚体二醇 重量％的其它疏水性二醇和/或多元醇，OH与NCO的当量比为1:1.1至1:4，同时或随后与含有两个末端NCO-反应性基团的B2）增链剂反应， 通过中和，另外含有芳香族或阳离子基团或基团可以转化为阴离子或阳离子基团的延伸剂，理论上仍然存在的NCO反应性基团与NCO反应基团的当量比在A）与B1）反应后为1:0.9至1： 4，然后任选地使C）在A）与B1）和B2反应后理论上仍然存在于聚氨酯中的NCO基团与含有至少三个羟基的多元醇和/或至少含有tw的氨基醇反应 o羟基以OH +氨基与NCO的当量比至少为3:1，最后分散在水中得到的聚氨酯，得到的聚氨酯在扩链剂B2所含的分散之前或期间至少部分中和 作为附加基团，提供了仅通过中和转化成阴离子或阳离子基团的那些基团。 还提供了制备水性聚氨酯分散体的方法和使用如烘烤漆制备的水性聚氨酯分散体的方法。