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公开(公告)号：US09174847B2
公开(公告)日：2015-11-03
申请号：US12113819
申请日：2008-05-01
CPC分类号： C01B32/159 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C23C16/26
摘要： Methods and processes for synthesizing high quality carbon single-walled nanotubes (SWNTs) are provided. A carbon precursor gas at reduced concentration (pressure) is contacted with a catalyst deposited on a support and at temperature about 10° C. above the SWNT synthesis onset temperature, but below the thermal decomposition temperature of the carbon precursor gas for given growth conditions. The concentration (pressure) of the carbon precursor gas can be controlled by reducing the total pressure of the gas, or by diluting with an inert carrier gas, or both. The methods produce SWNTs with the ratio of G-band to D-band in Raman spectra (IG:ID) of about 5 to about 200.
摘要翻译： 提供了合成高品质碳单壁纳米管（SWNT）的方法和工艺。 将降低浓度（压力）的碳前驱体气体与沉积在载体上的催化剂和高于SWNT合成起始温度约10℃的催化剂接触，但低于用于给定生长条件的碳前体气体的热分解温度。 碳前体气体的浓度（压力）可以通过降低气体的总压力，或通过用惰性载气稀释或两者来控制。 该方法产生具有约5至约200的拉曼光谱（IG：ID）中的G带与D带的比率的SWNT。
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2.发明授权公开(公告)号：US08518711B2
公开(公告)日：2013-08-27
申请号：US12846599
申请日：2010-07-29
CPC分类号： G01Q30/02 , B82Y35/00 , C01B32/16 , C01B32/172 , D01F11/14 , G01N21/6489 , Y10S977/842 , Y10S977/854 , Y10T436/23
摘要： Methods and processes for quantitatively determining the ratio of the metallic to semiconductor tubes in the sample single-wall carbon nanotubes is provided. The single-walled carbon nanotubes can be sonicated to debundle the bulk material. The debundled SWNTs can be coated with a polymer, such as sulfonated polystyrene-block-poly(ethylene-ran-butylene)-block-polystyrene (SDPS), and the coated SWNTs can be deposited on a substrate. The total number of tubes can be determined by atomic force microscopy (AFM). The semiconducting nanotubes can be determined by photoluminescence spectroscopy. The combination of photoluminescence and AFM measurements provides a quantitative ratio of the metallic to semiconductor tubes in the sample.
摘要翻译： 提供了用于定量确定样品单壁碳纳米管中金属与半导体管的比例的方法和方法。 单壁碳纳米管可被超声处理以使散装材料脱落。 分解的SWNT可以用聚合物，例如磺化聚苯乙烯 - 嵌段 - 聚（亚乙基 - 丁烯） - 嵌段 - 聚苯乙烯（SDPS））涂覆，并且涂覆的SWNT可以沉积在基材上。 管的总数可以通过原子力显微镜（AFM）来确定。 半导体纳米管可以通过光致发光光谱测定。 光致发光和AFM测量的组合提供了样品中金属对半导体管的定量比。
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公开(公告)号：US20090274609A1
公开(公告)日：2009-11-05
申请号：US12113819
申请日：2008-05-01
IPC分类号： C01B31/02
CPC分类号： C01B32/159 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C23C16/26
摘要： Methods and processes for synthesizing high quality carbon single-walled nanotubes (SWNTs) are provided. A carbon precursor gas at reduced concentration (pressure) is contacted with a catalyst deposited on a support and at temperature about 10° C. above the SWNT synthesis onset temperature, but below the thermal decomposition temperature of the carbon precursor gas for given growth conditions. The concentration (pressure) of the carbon precursor gas can be controlled by reducing the total pressure of the gas, or by diluting with an inert carrier gas, or both. The methods produce SWNTs with the ratio of G-band to D-band in Raman spectra (IG:ID) of about 5 to about 200.
摘要翻译： 提供了合成高品质碳单壁纳米管（SWNT）的方法和工艺。 将降低浓度（压力）的碳前驱体气体与沉积在载体上的催化剂和高于SWNT合成起始温度约10℃的催化剂接触，但低于用于给定生长条件的碳前体气体的热分解温度。 碳前体气体的浓度（压力）可以通过降低气体的总压力，或通过用惰性载气稀释或两者来控制。 该方法产生具有约5至约200的拉曼光谱（IG：ID）中的G带与D带的比率的SWNT。
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4.发明申请公开(公告)号：US20130180018A1
公开(公告)日：2013-07-11
申请号：US12846599
申请日：2010-07-29
IPC分类号： G01Q30/02
CPC分类号： G01Q30/02 , B82Y35/00 , C01B32/16 , C01B32/172 , D01F11/14 , G01N21/6489 , Y10S977/842 , Y10S977/854 , Y10T436/23
摘要： Methods and processes for quantitatively determining the ratio of the metallic to semiconductor tubes in the sample single-wall carbon nanotubes is provided. The single-walled carbon nanotubes can be sonicated to debundle the bulk material. The debundled SWNTs can be coated with a polymer, such as sulfonated polystyrene-block-poly(ethylene-ran-butylene)-block-polystyrene (SDPS), and the coated SWNTs can be deposited on a substrate. The total number of tubes can be determined by atomic force microscopy (AFM). The semiconducting nanotubes can be determined by photoluminescence spectroscopy. The combination of photoluminescence and AFM measurements provides a quantitative ratio of the metallic to semiconductor tubes in the sample.
摘要翻译： 提供了用于定量确定样品单壁碳纳米管中金属与半导体管的比例的方法和方法。 单壁碳纳米管可被超声处理以使散装材料脱落。 分解的SWNT可以用聚合物，例如磺化聚苯乙烯嵌段聚（乙烯 - 丁烯） - 嵌段 - 聚苯乙烯（SDPS））涂覆，并且涂覆的SWNT可以沉积在基材上。 管的总数可以通过原子力显微镜（AFM）来确定。 半导体纳米管可以通过光致发光光谱测定。 光致发光和AFM测量的组合提供了样品中金属对半导体管的定量比。
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公开(公告)号：US5783449A
公开(公告)日：1998-07-21
申请号：US736671
申请日：1996-10-25
申请人： Oleg Kuznetsov
发明人： Oleg Kuznetsov
IPC分类号： G01N33/497 , G01N33/98
CPC分类号： G01N33/98 , G01N33/4972 , G01N2800/307 , Y10S436/90 , Y10T436/204165
摘要： The method for quantifying Alcohol Breakdown Activity (ABA) in humans in vivo is developed to determine an efficiency of alcohol catabolism for any given individual. Unlike other related methods, Index-K uses a biological regularity of ABA and employs a third dimension for integrating the multiple pharmacokinetical data into a single value. As expected, it allows for the discrimination between human differences, including gender and personal levels of alcohol dependency. Its use of pharmacokinetical data from ethanol catabolism makes it absolutely specific to alcohol--a major cause of alcohol disorder. This feature allows us to help diagnose alcoholism even in cases where traditional methods used to evaluate harmful alcohol consumption have failed.
摘要翻译： 开发了在体内定量人类酒精分解活性（ABA）的方法，以确定任何给定个体的酒精分解代谢的效率。 与其他相关方法不同，Index-K使用ABA的生物学规律，并采用第三维将多个药代动力学数据整合为单一值。 正如预期的那样，它允许歧视人与人之间的差异，包括性别和个人水平的酒精依赖。 其使用乙醇分解代谢的药代动力学数据使其绝对具体的酒精是酒精失调的主要原因。 即使在用于评估有害酒精消费的传统方法失败的情况下，这一功能也可帮助我们诊断酒精中毒。
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