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    AN OXIDIC MATERIAL COMPRISING A ZEOLITE HAVING FRAMEWORK TYPE AEI
    1.
    发明申请
    AN OXIDIC MATERIAL COMPRISING A ZEOLITE HAVING FRAMEWORK TYPE AEI 有权

    公开(公告)号：US20220106192A1

    公开(公告)日：2022-04-07

    申请号：US17423590

    申请日：2020-01-21

    Applicant: BASF SE

    Inventor： Andrei-Nicolae Parvulescu ,  Feng-Shou Xiao ,  Xiangju Meng ,  Qinming Wu ,  Yu Dai ,  Stefan Maurer ,  Ulrich Mueller ,  Hao XU

    IPC: C01B39/48

    Abstract: A process for preparing an oxidic material comprising a zeolitic material having framework type AEI and a framework structure comprising a tetravalent element Y, a trivalent element X, and O, the process comprising preparing a synthesis mixture comprising water, a source of Y, a source of X comprising sodium, an AEI framework structure directing agent, and a source of sodium other than the source of X; and heating the synthesis mixture obtained from (i) to a temperature in the range of from 100 to 180° C. and keeping the synthesis mixture under autogenous pres-sure at a temperature in this range for a time in the range of at least 6 h, obtaining the oxidic material comprising a zeolitic material having framework type AEI and a framework structure comprising a tetravalent element Y, a trivalent element X, and O, comprised in its mother liquor; wherein the AEI framework structure directing agent according to (i) comprises a N, N-diethyl-2,6-dimethylpiperidinium cation.

    Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
    2.
    发明授权
    Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom 有权

    公开(公告)号：US10301185B2

    公开(公告)日：2019-05-28

    申请号：US15518945

    申请日：2015-10-15

    Applicant: BASF SE

    Inventor： Stefan Maurer ,  Ulrich Müller ,  Feng-Shou Xiao ,  Xiangju Meng ,  Qinming Wu

    IPC: B01J29/70 ,  C01B39/48 ,  B01J29/18 ,  C01B39/20 ,  C01B39/26 ,  C01B39/04 ,  B01J29/08 ,  B01J29/40 ,  B01J29/65 ,  C01B37/02 ,  C01B39/08 ,  C01B39/40

    Abstract: The present invention relates to a process for the preparation of a zeolitic material comprising YO2 in its framework structure, wherein Y stands for a tetravalent element, wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO2, one or more fluoride containing compounds, and one or more structure directing agents; (2) crystallizing the mixture obtained in step (1) for obtaining a zeolitic material comprising YO2 in its framework structure; wherein the mixture provided in step (1) and crystallized in step (2) contains 35 wt.-% or less of H2O based on 100 wt.-% of YO2 contained in the mixture provided in step (1) and crystallized in step (2), as well as to a zeolitic material comprising YO2 in its framework structure obtainable and/or obtained according to said process, and to a zeolitic material per se comprising SiO2 in its framework structure, wherein in the 29Si MAS NMR spectrum of the as-synthesized zeolitic material the ratio of the total integration value of the peaks associated to Q3 signals to the total integration value of the peaks associated to Q4 signals is in the range of from 0:100 to 20:80, including the use of the aforementioned zeolitic materials.

    Organotemplate-free solid-state synthetic method for zeolite molecular sieves
    5.
    发明授权
    Organotemplate-free solid-state synthetic method for zeolite molecular sieves 有权

    公开(公告)号：US10160656B2

    公开(公告)日：2018-12-25

    申请号：US14649637

    申请日：2013-12-05

    Applicant: BASF SE

    Inventor： Stefan Maurer ,  Ulrich Müller ,  Feng-Shou Xiao ,  Xiangju Meng ,  Qinming Wu

    IPC: C01B39/46 ,  C01B39/02 ,  C01B39/38 ,  C01B39/20 ,  C01B39/26 ,  B01J29/08 ,  B01J29/18 ,  B01J29/70 ,  B01J35/00 ,  B01J35/10 ,  B01J29/40 ,  B01J37/00 ,  B01J37/04 ,  C01B39/14

    Abstract: Described is a preparation method for zeolite molecular sieves by means of solid-state reactions without the usage of organic templates. The method comprises the following steps: grinding and mixing the solid raw materials comprising the silicon source, the aluminum source and the alkali source, transferring the obtained mixture into an autoclave, conducting the crystallization for a period of 5 hours-20 days at a temperature of 50-200° C. After filtering and drying the crystallized products, molecular sieves in a powder form can be obtained. The method provides different molecular sieves, including ZSM-5 zeolite, Beta zeolite, FAU zeolite, MOR zeolite, LTA zeolite, and GIS zeolite, with a high crystallinity and an adjustable Si/Al ratio within a certain range. The obtained products exhibit a high crystallinity and a high purity, and the method does not require the use of organic templates and solvents, which avoids unnecessary consumptions during the production, simplifies the synthetic process, and also increases the yield from the autoclave reactor.

    Organotemplate-Free Solid-State Synthetic Method For Zeolite Molecular Sieves
    6.
    发明申请
    Organotemplate-Free Solid-State Synthetic Method For Zeolite Molecular Sieves 审中-公开
    无机固体合成方法用于沸石分子筛

    公开(公告)号：US20150298983A1

    公开(公告)日：2015-10-22

    申请号：US14649637

    申请日：2013-12-05

    Applicant: BASF SE

    Inventor： Stefan Maurer ,  Ulrich Müller ,  Feng-Shou Xiao ,  Xiangju Meng ,  Qinming Wu

    IPC: C01B39/46 ,  C01B39/20 ,  B01J29/40 ,  C01B39/14 ,  B01J37/04 ,  B01J37/00 ,  C01B39/38 ,  C01B39/26

    CPC classification number: C01B39/46 ,  B01J29/08 ,  B01J29/18 ,  B01J29/40 ,  B01J29/70 ,  B01J35/002 ,  B01J35/1023 ,  B01J35/1038 ,  B01J37/009 ,  B01J37/04 ,  C01B39/02 ,  C01B39/14 ,  C01B39/20 ,  C01B39/26 ,  C01B39/38

    Abstract: Described is a preparation method for zeolite molecular sieves by means of solid-state reactions without the usage of organic templates. The method comprises the following steps: grinding and mixing the solid raw materials comprising the silicon source, the aluminum source and the alkali source, transferring the obtained mixture into an autoclave, conducting the crystallization for a period of 5 hours-20 days at a temperature of 50-200° C. After filtering and drying the crystallized products, molecular sieves in a powder form can be obtained. The method provides different molecular sieves, including ZSM-5 zeolite, Beta zeolite, FAU zeolite, MOR zeolite, LTA zeolite, and GIS zeolite, with a high crystallinity and an adjustable Si/Al ratio within a certain range. The obtained products exhibit a high crystallinity and a high purity, and the method does not require the use of organic templates and solvents, which avoids unnecessary consumptions during the production, simplifies the synthetic process, and also increases the yield from the autoclave reactor.

    Abstract translation: 描述了通过固相反应而不使用有机模板的沸石分子筛的制备方法。 该方法包括以下步骤：将包含硅源，铝源和碱源的固体原料研磨并混合，将得到的混合物转移到高压釜中，在温度下进行5小时-20天的结晶 50-200℃。过滤并干燥结晶产物后，可获得粉末形式的分子筛。 该方法提供了不同的分子筛，包括ZSM-5沸石，β沸石，FAU沸石，MOR沸石，LTA沸石和GIS沸石，在一定范围内具有高结晶度和可调Si / Al比。 得到的产物具有高结晶度和高纯度，并且该方法不需要使用有机模板和溶剂，这避免了在生产过程中不必要的消耗，简化了合成过程，并且还提高了高压釜反应器的产率。

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