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1.发明授权Thermal separating process for removing at least one stream containing enriched (meth) acrylic monomers 有权用于除去至少一种含有富含（甲基）丙烯酸单体的物流的热分离方法公开(公告)号：US07393436B2
公开(公告)日：2008-07-01
申请号：US10888933
申请日：2004-07-12
申请人： Bernd Eck , Ulrich Hammon , Klaus Joachim Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
发明人： Bernd Eck , Ulrich Hammon , Klaus Joachim Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
CPC分类号： C07C51/43 , B01D3/14 , B01D3/225 , B01D3/322 , C07C51/215 , C07C51/252 , C07C51/44 , Y10S203/22 , C07C57/04
摘要： A thermal separating process for removing a stream containing enriched (meth)acrylic monomers from a mixture containing (meth)acrylic monomers, in which the liquid phases retained in the separating space at high temperature and high (meth)acrylic monomer content are minimized.
摘要翻译： 一种用于从含有（甲基）丙烯酸单体的混合物中除去含有富含（甲基）丙烯酸单体的物流的热分离方法，其中在高温和高（甲基）丙烯酸单体含量保留在分离空间中的液相被最小化。
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2.发明授权Device for performing the purifying separation of crystals out of their suspension in a contaminated crystal melt 有权用于在受污染的晶体熔体中从其悬浮液中进行晶体的纯化分离的装置公开(公告)号：US07762404B2
公开(公告)日：2010-07-27
申请号：US10494046
申请日：2002-11-08
CPC分类号： B01D9/0013 , B01D9/0036 , B01D9/004 , B01D9/0045
摘要： An apparatus for separating crystals from their suspension in contaminated crystal melt with purification, in which a hydraulic wash column has distributor aids in a distributor space.
摘要翻译： 一种用于在污染的晶体熔体中从其悬浮液中分离晶体的装置，其中液压清洗柱在分配器空间中具有分配器辅助。
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3.发明授权Method for performing the purifying separation of crystals out their suspension in a mother liquor 有权在母液中进行将其晶体纯化分离出悬浮液的方法公开(公告)号：US07540884B2
公开(公告)日：2009-06-02
申请号：US10494721
申请日：2002-11-08
IPC分类号： B01D9/00
CPC分类号： B01D9/0013 , B01D9/0036 , B01D9/004 , B01D9/0045
摘要： A process for purifying removal of crystals from their suspension in mother liquor by means of a washing column having forced transport in which the process chamber is encased by a metal wall which, on its side facing away from the process chamber, is heated at least along the length of the pure melt zone.
摘要翻译： 用于通过强制运输的洗涤塔净化从母液悬浮液中除去晶体的方法，其中处理室被金属壁包围，金属壁在其远离处理室的一侧至少沿着 纯熔体区域的长度。
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公开(公告)号：US07129376B2
公开(公告)日：2006-10-31
申请号：US10476188
申请日：2002-05-02
IPC分类号： C07C51/42 , C07D207/24
CPC分类号： C07D207/267 , C07C51/43 , C07C51/47 , C07C51/48 , C07C57/04
摘要： The invention relates to a method for the production of a purified melt of a monomer melt obtained by condensation, absorption or extraction in a crystallizer, wherein the inlet to the crystallizer is subjected to a mechanical solid/liquid separation operation.
摘要翻译： 本发明涉及通过在结晶器中冷凝，吸收或萃取获得的单体熔体的纯化熔体的制备方法，其中结晶器的入口进行机械固/液分离操作。
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5.发明授权公开(公告)号：US07319166B2
公开(公告)日：2008-01-15
申请号：US10476187
申请日：2002-05-02
IPC分类号： C07C51/43 , C07D207/00
CPC分类号： C07D207/267 , C07C51/43 , C07C57/04
摘要： The invention relates to a method for purifying a raw melt of at least one monomer by crystallization, wherein suspension crystallization is initially used and the resulting remaining melt or the suspension crystals that have been molten once again and separated are subjected to a mechanical separation operation before undergoing subsequent purification by crystallization.
摘要翻译： 本发明涉及一种通过结晶纯化至少一种单体的原料熔体的方法，其中最初使用悬浮液结晶，并将所得剩余熔体或已经再次熔融并分离的悬浮液晶体进行机械分离操作，然后进行机械分离操作 随后通过结晶进行纯化。
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6.发明授权Cleaning of tray columns which have been used for rectificatively treating liquids comprising (meth)acrylic acid and/or esters thereof 有权清洁已经用于整流处理包含（甲基）丙烯酸和/或其酯的液体的塔盘塔公开(公告)号：US07331354B2
公开(公告)日：2008-02-19
申请号：US10505163
申请日：2003-03-04
申请人： Juergen Schroeder , Klaus Joachim Mueller-Engel , Volker Schliephake , Ulrich Hammon , Volker Diehl , Ulrich Jaeger
发明人： Juergen Schroeder , Klaus Joachim Mueller-Engel , Volker Schliephake , Ulrich Hammon , Volker Diehl , Ulrich Jaeger
摘要： In process for cleaning tray columns which are used for the purposes of rectifiying liquids comprising (meth)acrylic compounds, a basic liquid is conveyed downward through the tray column and a gas is passed through the column in countercurrent to the basic liquid at an average gas phase differential pressure over all trays of at least 0.5 mbar/tray.
摘要翻译： 在清洁用于整流包含（甲基）丙烯酸类化合物的液体的塔盘列的过程中，碱性液体向下传送通过塔盘塔，气体以平均气体与碱性液体逆流通过塔 至少0.5 mbar /托盘的所有托盘上的相位差压。
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公开(公告)号：US07179875B2
公开(公告)日：2007-02-20
申请号：US10485484
申请日：2002-08-02
IPC分类号： C08F220/06
CPC分类号： C08F220/06 , A61L15/24 , A61L15/60 , C07C51/215 , C07C51/235 , C07C51/252 , C07C51/43 , C07C51/44 , C07C51/487 , C07C57/04 , C08L33/02
摘要： In a process for preparing water-absorbent resins based on acrylic acid, crude acrylic acid is firstly isolated from the reaction gases from the catalytic gas-phase oxidation of propane, propylene and/or acrolein. This is treated with an aldehyde scavenger and pure acrylic acid is separated by distillation from the treated crude acrylic acid, and this pure acrylic acid can be subjected directly to a free-radical polymerization.
摘要翻译： 在制备基于丙烯酸的吸水性树脂的方法中，首先从丙烷，丙烯和/或丙烯醛的催化气相氧化反应气体中分离粗丙烯酸。 用醛清除剂进行处理，经处理的粗丙烯酸通过蒸馏分离纯丙烯酸，该纯丙烯酸可直接进行自由基聚合。
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公开(公告)号：US07157598B2
公开(公告)日：2007-01-02
申请号：US10510236
申请日：2003-05-02
CPC分类号： C07C51/412 , C07C51/44 , C07C57/04
摘要： A process prepares an aqueous alkali metal acrylate solution by distillatively removing acrylic acid from a mixture as vapors and taking up the vapors immediately from the gas phase into an aqueous alkali solution.
摘要翻译： 一种方法通过从混合物中蒸馏除去丙烯酸作为蒸气并将蒸气立即从气相中吸收到碱性水溶液中来制备碱金属丙烯酸水溶液。
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9.发明授权公开(公告)号：US08431743B2
公开(公告)日：2013-04-30
申请号：US11131256
申请日：2005-05-18
申请人： Martin Dieterle , Klaus Joachim Mueller-Engel , Claus Hechler , Ulrich Hammon , Armin Diefenbacher
发明人： Martin Dieterle , Klaus Joachim Mueller-Engel , Claus Hechler , Ulrich Hammon , Armin Diefenbacher
IPC分类号： C07C51/42
CPC分类号： C07C51/252 , C07C45/35 , C07C57/04 , C07C47/22
摘要： The present invention relates to a process for preparing acrylic acid by two-stage heterogeneously catalyzed partial gas phase oxidation of propylene, in which the propylene source used is a preceding propane dehydrogenation and in which the first oxidation stage is operated with restricted propylene conversion, and unconverted propane and propylene present in the product gas mixture of the second partial oxidation stage are recycled substantially into the preceding propane dehydrogenation.
摘要翻译： 本发明涉及一种通过丙烯二阶段非均相催化部分气相氧化丙烯制备丙烯酸的方法，其中使用的丙烯源是前面的丙烷脱氢，其中第一氧化段以有限的丙烯转化操作，以及 存在于第二部分氧化阶段的产物气体混合物中的未转化的丙烷和丙烯基本上被再循环到前面的丙烷脱氢中。
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10.发明授权Process for operating a continuous removal of a target product X in the form of fine crystals of the target product X 有权用于以目标产物X的细晶体的形式连续移除靶产物X的方法公开(公告)号：US08106240B2
公开(公告)日：2012-01-31
申请号：US12208559
申请日：2008-09-11
IPC分类号： C07C51/42
CPC分类号： B01D9/0009 , B01D9/0013 , B01D9/005 , B01D9/0063 , C07C51/43 , C07C57/04
摘要： A process for operating a continuous removal of a target product X in the form of fine crystals of a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in the secondary chamber of an indirect heat exchanger to which liquid phase P flows continuously with simultaneous continuous flow through the primary chamber of the indirect heat exchanger with a coolant, and continuous withdrawal of a crystal suspension S having a degree of crystallization Y from the secondary chamber in two operating states I and II, wherein the coolant temperature is lower, the mass flow of liquid phase P is greater and the molar proportion of the constituents other than the target product X in the liquid phase P in operating state II is greater than in operating state I.
摘要翻译： 通过在间接热交换器的二次室中冷却悬浮液结晶来操作以含有目标产物X和除了目标产物X的成分的液相P的细晶体的形式连续除去目标产物X的方法， 该液相P以连续的流动方式连续流过间接热交换器的主室，并具有冷却剂，并且在两个操作状态I和II中连续取出具有结晶Y的程度的结晶悬浮液， 冷却剂温度较低，液相P的质量流量较大，并且在运行状态II下的液相P中除目标产物X以外的成分的摩尔比例大于运行状态I.
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