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    Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups
    4.
    发明申请
    Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups 失效
    制备9,10-二氢-9-OXA-10-有机氧基菲啶-10-氧化物或硫代酮的方法及其在苯基上取代的衍生物

    公开(公告)号：US20050038278A1

    公开(公告)日：2005-02-17

    申请号：US10918836

    申请日：2004-08-13

    申请人： Uwe Dittrich ,  Berthold Just ,  Manfred Doring ,  Michael Ciesielski

    发明人： Uwe Dittrich ,  Berthold Just ,  Manfred Doring ,  Michael Ciesielski

    IPC分类号： C07F9/6571 ,  C07F9/02

    CPC分类号： C08K5/5313 ,  C07F9/657181 ,  C07F9/65719

    摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of oxidation agent into 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione or a derivative of same substituted on the phenyl groups.

    摘要翻译： 提供了用于制备9,10-二氢-9-氧杂-10-有机氧基菲啶-10-氧化物或硫代酮及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢 - 9-氧杂-10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b） 来自步骤（a）的中间产物任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入氧化来转化来自步骤（a）或（b）的中间产物 试剂转化成9,10-二氢-9-氧杂-10-有机氧基亚磷酰-10-氧化物或硫代酮或其在苯基上取代的相同衍生物。

    Process for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups
    5.
    发明授权
    Process for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups 失效
    制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物的方法及其在苯基上取代的衍生物

    公开(公告)号：US07317120B2

    公开(公告)日：2008-01-08

    申请号：US10918838

    申请日：2004-08-13

    申请人： Uwe Dittrich ,  Berthold Just ,  Manfred Döring ,  Michael Ciesielski

    发明人： Uwe Dittrich ,  Berthold Just ,  Manfred Döring ,  Michael Ciesielski

    IPC分类号： C07F9/02

    CPC分类号： C07F9/657172 ,  C07F9/4841 ,  C08K5/5313

    摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of catalytic quantities of alkylation agent into 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide or a derivative of same substituted on the phenyl groups.

    摘要翻译： 提供了制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢-9-氧杂 -10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）中间产物 步骤（a）任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入催化量的烷基化来转化来自步骤（a）或（b）的中间产物 试剂转化成9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物或其在苯基上取代的相同衍生物。

    Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups
    6.
    发明授权
    Process for the preparation of 9, 10-dihydro-9-OXA-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of the same substituted on the phenyl groups 失效
    制备9,10-二氢-9-OXA-10-有机氧基菲啶-10-氧化物或硫代酮的方法及其在苯基上取代的衍生物

    公开(公告)号：US07317119B2

    公开(公告)日：2008-01-08

    申请号：US10918836

    申请日：2004-08-13

    申请人： Uwe Dittrich ,  Berthold Just ,  Manfred Döring ,  Michael Ciesielski

    发明人： Uwe Dittrich ,  Berthold Just ,  Manfred Döring ,  Michael Ciesielski

    IPC分类号： C07F9/02

    CPC分类号： C08K5/5313 ,  C07F9/657181 ,  C07F9/65719

    摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of oxidation agent into 9,10-dihydro-9-oxa-10-organyloxyphosphaphenanthrene-10-oxide or -thione or a derivative of same substituted on the phenyl groups.

    摘要翻译： 提供了用于制备9,10-二氢-9-氧杂-10-有机氧基菲啶-10-氧化物或硫代酮及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢 - 9-氧杂-10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b） 来自步骤（a）的中间产物任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入氧化来转化来自步骤（a）或（b）的中间产物 试剂转化成9,10-二氢-9-氧杂-10-有机氧基亚磷酰-10-氧化物或硫代酮或其在苯基上取代的相同衍生物。

    Proces for the preparation of 9, 10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups
    8.
    发明申请
    Proces for the preparation of 9, 10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of the same substituted on the phenyl groups 失效
    制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物的方法及其在苯基上取代的衍生物

    公开(公告)号：US20050038279A1

    公开(公告)日：2005-02-17

    申请号：US10918838

    申请日：2004-08-13

    申请人： Uwe Dittrich ,  Berthold Just ,  Manfred Doring ,  Michael Ciesielski

    发明人： Uwe Dittrich ,  Berthold Just ,  Manfred Doring ,  Michael Ciesielski

    IPC分类号： C07F9/02 ,  C07F9/28 ,  C07F9/48 ,  C07F9/50 ,  C07F9/6571 ,  C08K5/5313 ,  C08L23/02 ,  C08L25/06 ,  C08L61/04 ,  C08L63/00 ,  C08L67/00 ,  C08L69/00 ,  C08L77/00

    CPC分类号： C07F9/657172 ,  C07F9/4841 ,  C08K5/5313

    摘要： A process is provided for the preparation of 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide and derivatives of same substituted on the phenyl groups, in which: (a) 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOP) or a derivative of same is reacted in the presence of at least one mono- or polyhydric alcohol with at least one ortho ester with formation of a first intermediate product, (b) the intermediate product from step (a) is optionally reacted with at least one further mono- or polyhydric alcohol with formation of a further intermediate product and (c) the intermediate product from steps (a) or (b) is transformed by addition of catalytic quantities of alkylation agent into 9,10-dihydro-9-oxa-10-organylphosphaphenanthrene-10-oxide or a derivative of same substituted on the phenyl groups.

    摘要翻译： 提供了制备9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物及其在苯基上取代的相同衍生物的方法，其中：（a）9,10-二氢-9-氧杂 -10-磷杂菲-10-氧化物（DOP）或其衍生物在至少一种一元醇或多元醇与至少一种原酸酯的存在下反应，形成第一中间产物，（b）中间产物 步骤（a）任选地与至少一种另外的一元醇或多元醇反应形成另外的中间产物，和（c）通过加入催化量的烷基化来转化来自步骤（a）或（b）的中间产物 试剂转化成9,10-二氢-9-氧杂-10-有机基膦菲-10-氧化物或其在苯基上取代的相同衍生物。