Method for solid phase polymerization
    4.
    发明授权
    Method for solid phase polymerization 失效
    固相聚合方法

    公开(公告)号:US5955569A

    公开(公告)日:1999-09-21

    申请号:US757310

    申请日:1996-11-27

    CPC分类号: C08G69/30 Y02P20/584

    摘要: An improved method for increasing the relative viscosity and molecular weight of a polyamide polymer (such as nylon 6,6, nylon 6, and the like) while in the solid state involving the use of a phosphorus-containing catalyst (such as 2(2'-pyridyl) ethyl phosphonic acid or the like) in combination with an oxygen free gas characterized by a low dew point (typically below 30.degree. C. and preferably below -30.degree. C.). The combination of affording commercial operation at greater through put at lower temperature. Such a process is of particular value during the production of terpolyamide and multipolyamide polymer intended for use in colored nylon fiber manufacture.

    摘要翻译: 在涉及使用含磷催化剂的固体状态(例如2(2))中,提高聚酰胺聚合物(例如尼龙6,6,尼龙6等)的相对粘度和分子量的改进方法 乙基膦酸等)与无氧气体组合,其特征在于低露点(通常低于30℃,优选低于-30℃)。 通过在较低温度下提供商业运作的组合。 在制造用于着色尼龙纤维制造中的三聚酰胺和多聚酰胺聚合物的生产期间,这种方法是特别有价值的。

    Analytical sampling valve
    6.
    依法登记的发明

    公开(公告)号:USH1190H

    公开(公告)日:1993-06-01

    申请号:US718943

    申请日:1991-06-21

    申请人: Gregory D. Cramer

    发明人: Gregory D. Cramer

    IPC分类号: G01N1/20 G01N11/08

    摘要: An analytical sampling valve that permits pumping of a side stream of fluid from a main process fluid stream through a monitoring device to measure fluid stream properties, and return of the sample to the main process line downstream of the sampling position, while providing the ability to clean the lines or remove the monitoring or pumping apparatus without shutdown of fluid flow.