Nano-material
    1.
    发明授权

    公开(公告)号:US10239046B2

    公开(公告)日:2019-03-26

    申请号:US14549701

    申请日:2014-11-21

    摘要: A fluffy nano-material and method of manufacture are described. At 2000× magnification the fluffy nanomaterial has the appearance of raw, uncarded wool, with individual fiber lengths ranging from approximately four microns to twenty microns. Powder-based nanocatalysts are dispersed in the fluffy nanomaterial. The production of fluffy nanomaterial typically involves flowing about 125 cc/min of organic vapor at a pressure of about 400 torr over powder-based nano-catalysts for a period of time that may range from approximately thirty minutes to twenty-four hours.

    Nano-Material
    5.
    发明申请
    Nano-Material 审中-公开
    纳米材料

    公开(公告)号:US20150104646A1

    公开(公告)日:2015-04-16

    申请号:US14549701

    申请日:2014-11-21

    摘要: A fluffy nano-material and method of manufacture are described. At 2000× magnification the fluffy nanomaterial has the appearance of raw, uncarded wool, with individual fiber lengths ranging from approximately four microns to twenty microns. Powder-based nanocatalysts are dispersed in the fluffy nanomaterial. The production of fluffy nanomaterial typically involves flowing about 125 cc/min of organic vapor at a pressure of about 400 torr over powder-based nano-catalysts for a period of time that may range from approximately thirty minutes to twenty-four hours.

    摘要翻译: 描述了蓬松的纳米材料和制造方法。 在2000×放大倍数下,蓬松的纳米材料具有原始的未梳理羊毛的外观,单个纤维长度范围约为4微米至20微米。 粉末状纳米催化剂分散在蓬松的纳米材料中。 蓬松的纳米材料的生产通常涉及在约400托的压力下将大约125cc / min的有机蒸气流过粉末基纳米催化剂,持续时间可以在约30分钟至24小时的范围内。

    LOW TEMPERATURE STABILIZATION PROCESS FOR PRODUCTION OF CARBON FIBER HAVING STRUCTURAL ORDER
    6.
    发明申请
    LOW TEMPERATURE STABILIZATION PROCESS FOR PRODUCTION OF CARBON FIBER HAVING STRUCTURAL ORDER 有权
    生产具有结构订单的碳纤维的低温稳定工艺

    公开(公告)号:US20160258082A1

    公开(公告)日:2016-09-08

    申请号:US14640788

    申请日:2015-03-06

    申请人: UT-Battelle, LLC

    IPC分类号: D01F9/20

    摘要: A method for producing a carbon fiber, the method comprising: (i) subjecting a continuous carbon fiber precursor having a polymeric matrix in which strength-enhancing particles are incorporated to a stabilization process during which the carbon fiber precursor is heated to within a temperature range ranging from the glass transition temperature to no less than 20° C. below the glass transition temperature of the polymeric matrix, wherein the maximum temperature employed in the stabilization process is below 400° C., for a processing time within said temperature range of at least 1 hour in the presence of oxygen and in the presence of a magnetic field of at least 1 Tesla, while said carbon fiber precursor is held under an applied axial tension; and (ii) subjecting the stabilized carbon fiber precursor, following step (i), to a carbonization process. The stabilized carbon fiber precursor, resulting carbon fiber, and articles made thereof are also described.

    摘要翻译: 一种碳纤维的制造方法,其特征在于,包括:(i)使具有强化增强粒子的聚合物基质的连续碳纤维前体在碳纤维前体被加热至温度范围内的稳定化工序中进行 范围从玻璃化转变温度到低于聚合物基质的玻璃化转变温度的不低于20℃,其中稳定过程中使用的最高温度低于400℃,对于在所述温度范围内的加工时间 在氧的存在下和至少1特斯拉的磁场的存在下至少1小时,同时所述碳纤维前体保持在施加的轴向张力下; 和(ii)在步骤(i)之后对稳定化的碳纤维前体进行碳化处理。 还描述了稳定的碳纤维前体,所得碳纤维及其制成的制品。

    SUPERLUBRICITY COATING CONTAINING CARBON NANOTUBES

    公开(公告)号:US20210222290A1

    公开(公告)日:2021-07-22

    申请号:US17090216

    申请日:2020-11-05

    申请人: UT-Battelle, LLC

    摘要: A method for producing a structure containing an array of MWCNTs on a metal substrate, comprising: (i) subjecting a metal substrate to a surface oxidation process at a first elevated temperature in an oxygen-containing atmosphere and under a first reduced pressure; (ii) subjecting the metal substrate to a surface reduction process at a second elevated temperature in a reducing atmosphere and under a second reduced pressure of at least 0.01 atm and less than 1 atm to result in reduction of the surface of said metal substrate, wherein the reducing atmosphere contains hydrogen gas; (iii) subjecting the metal substrate to a third reduced pressure of no more than 0.1 atm; and (iv) contacting the metal substrate, while at the third reduced pressure and under an inert or reducing atmosphere, with an organic substance at a third elevated temperature for suitable time to produce the MWCNTs on the metal substrate.