PROCESS FOR SYNTHESIZING ALKENYL DISILOXANE

    公开(公告)号:US20230056138A1

    公开(公告)日:2023-02-23

    申请号:US17784082

    申请日:2020-12-11

    IPC分类号: C07F7/08 C07F7/20

    摘要: Described herein are methods for making alkenyl disiloxanes, comprising combining an alkenyl halosilane with a bis-hydrido terminated alkyl disiloxane and adding the mixture to water, an acidic aqueous solution, or a basic aqueous solution. The ratio of the alkenyl halosilane to the bis-hydrido terminated alkyl disiloxane is about 1:10 to about 10:1. The alkenyl halosilane and bis-hydrido terminated alkyl disiloxane are mixed at about 20° C. to about 45° C. In an example, no organic solvent is present. The reaction product is separated and washed with saturated NaHCO3 solution (e.g., sodium bicarbonate).

    PROCESSES FOR SYNTHESIZING UNSYMMETRICAL DISILOXANES

    公开(公告)号:US20230099625A1

    公开(公告)日:2023-03-30

    申请号:US17784084

    申请日:2020-12-11

    IPC分类号: C07F7/08

    摘要: Described herein are methods for making alkenyl disiloxanes, comprising combining an alkenyl halosilane with an alkyl halosilane and adding the mixture to water, an acidic aqueous solution, or a basic aqueous solution. The ratio of the alkenyl halosilane to the alkyl halosilane is about 10:1 to about 1:10. The alkenyl halosilane and the alkyl halosilane are mixed at about 20° C. to about 45° C. The reaction product is separated and washed with saturated alkali carbonate solution.