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1.发明授权Enzymatic oxidation of glycolic acid in the presence of non-enzymatic catalyst for decomposing hydrogen peroxide 失效在用于分解过氧化氢的非酶催化剂的存在下乙醇酸的酶催化氧化
公开(公告)号：US5262314A
公开(公告)日：1993-11-16
申请号：US755925
申请日：1991-09-06
IPC分类号： C07C51/235 , C12P7/40 , C07C51/16
CPC分类号： C12P7/40 , C07C51/235
摘要： A process for the production of glyoxylic acid by reacting glycolic acid and oxygen in an aqueous solution at pH 7-10 in the presence of the enzyme glycolate oxidase and a non-enzymatic catalyst for the decomposition of hydrogen peroxide, and an amine buffer capable of forming a chemical adduct with glyoxylic acid.
摘要翻译： 在乙醇酸和氧气在pH7-10的水溶液中，在乙醇酸氧化酶的酶和用于分解过氧化氢的非酶催化剂的存在下反应生产乙醛酸的方法，以及能够 与乙醛酸形成化学加合物。
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公开(公告)号：US5182405A
公开(公告)日：1993-01-26
申请号：US761556
申请日：1991-09-18
IPC分类号： C07D233/56 , C07D521/00
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： A process for the preparation of 1,3-disubstituted imidazolium salts that comprises reaction of an .alpha.-dicarbonyl compound, an aldehyde, an amine and an acid is disclosed.
摘要翻译： 公开了一种制备包括α-二羰基化合物，醛，胺和酸的反应的1,3-二取代的咪唑鎓盐的方法。
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3.发明申请STABLE FREE RADICAL CHROMOPHORES, PROCESSES FOR PREPARING THE SAME, NONLINEAR OPTIC MATERIALS AND USES THEREOF IN NONLINEAR OPTICAL APPLICATIONS 审中-公开稳定的自由基色素，其制备方法，非线性光学材料及其在非线性光学应用中的应用公开(公告)号：US20120267583A1
公开(公告)日：2012-10-25
申请号：US13307663
申请日：2011-11-30
申请人： Frederick J. Goetz, JR. , Andrew Ashton , Frederick J. Goetz, SR. , David F. Eaton , Anthony J. Arduengo, III , Howard E. Simmons, III , Jason W. Runyon
发明人： Frederick J. Goetz, JR. , Andrew Ashton , Frederick J. Goetz, SR. , David F. Eaton , Anthony J. Arduengo, III , Howard E. Simmons, III , Jason W. Runyon
IPC分类号： C07D487/04 , C07D471/04 , C07D487/14 , G02B5/23
CPC分类号： H01L51/0061 , C07D241/38 , C07D471/06 , C07D487/04 , C07D487/14 , G02B1/08 , G02B5/3025 , G02F1/3612 , H01L51/0072 , H01L51/42
摘要： Nonlinear optic chromophores comprising stabilized radical structures, mixtures thereof, methods for their production, nonlinear optical materials containing such chromophores, and the use of such materials in electro-optic, solar conversion, photovoltaic and all-optical nonlinear devices are described.
摘要翻译： 描述了包含稳定的自由基结构的非线性视觉发色团，其混合物，它们的制备方法，含有这种发色团的非线性光学材料，以及这些材料在电光，太阳能转换，光伏和全光非线性装置中的应用。
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公开(公告)号：US06177575B1
公开(公告)日：2001-01-23
申请号：US09193700
申请日：1998-11-17
申请人： Anthony J. Arduengo, III , Frederick P. Gentry, Jr. , Prakash K. Taverkere , Howard E. Simmons, III
发明人： Anthony J. Arduengo, III , Frederick P. Gentry, Jr. , Prakash K. Taverkere , Howard E. Simmons, III
IPC分类号： C07D23358
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： Imidazoles may be manufactured by reacting a glyoxal, ammonia, an aldehyde, and optionally a primary amine, in the presence of a Bronsted acid whose pKa is approximately equal to the pKa of the ammonium cation of the primary amine, or if the primary amine is not present, to the pKa of the ammonium (NH4+) cation. The reaction may be used to make in relatively high yields a wide variety of imidazoles using relatively inexpensive starting materials. The imidazoles are useful as chemical intermediates.
摘要翻译： 咪唑可以通过使乙二醛，氨，醛和任选的伯胺在其pKa大约等于伯胺的铵阳离子的pKa的布朗斯台德酸的存在下反应来制备，或者如果伯胺是 不存在于铵（NH 4 +）阳离子的pKa中。 该反应可以用相对高的产率制备各种各样的使用相对便宜的起始原料的咪唑。 咪唑可用作化学中间体。
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公开(公告)号：US5196053A
公开(公告)日：1993-03-23
申请号：US799136
申请日：1991-11-27
CPC分类号： C23C18/31 , H05K2203/073 , H05K3/244
摘要： An environmentally innocuous effective replacement for thiourea is disclosed for use as a complexing agent in displacement plating processes in which the plating solution is applied to the substrate surface to be plated by immersion or by spraying, cascading, pouring and the like. The replacement complexing agent is an imidazole-2-thione compound having the formula: ##STR1## wherein A and B are the same or different --R--Y groups, wherein R is linear, branched or cyclic alkenyl group containing 1 to 12 carbon atoms and Y is a hydrogen, halogen, cyano, vinyl, phenyl, or ether moiety. Of this class of compounds, 1-methyl-3-propyl-imidazole-2-thione is preferred for immersion tin plating. This class of complexing agents is particularly useful in spray displacement tin plating for the manufacture of printed circuit boards wherein free tin metal is added to the plating solution.
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6.发明授权Process for preparing a strengthened polyimide film containing organometallic compounds for improving adhesion 失效制备含有机金属化合物的强化聚酰亚胺膜以提高粘合性的方法
公开(公告)号：US5272194A
公开(公告)日：1993-12-21
申请号：US822501
申请日：1992-01-17
CPC分类号： H05K1/0346 , C08K5/56 , C08K5/57 , H01B3/306 , Y10T428/31681 , Y10T428/31721
摘要： A strengthened polyimide film is described, which has improved adhesion when bonded to a metal foil through a heat-resistant adhesive, containing from 0.02 to 1% by weight, based on the weight of the film, of an organo-metallic compound wherein the metal is tin, bismuth or antimony. A process for preparing a strengthened polyimide film is also described wherein an organometallic compound is introduced into a film-forming polyamic acid polymer prior to the casting step.
摘要翻译： 描述了一种强化的聚酰亚胺膜，其通过耐热粘合剂与金属箔接合时具有改善的粘合性，该耐热粘合剂含有基于该膜重量的0.02-1重量％的有机金属化合物，其中金属 是锡，铋或锑。 还描述了制备强化聚酰亚胺膜的方法，其中在浇铸步骤之前将有机金属化合物引入成膜聚酰胺酸聚合物中。
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7.发明授权
公开(公告)号：US5162482A
公开(公告)日：1992-11-10
申请号：US649430
申请日：1991-01-31
IPC分类号： C07D233/84 , C08G59/68 , C09D163/00
CPC分类号： C08G59/687 , C07D233/84 , C09D163/00
摘要： The present invention discloses 1,3-dialkylimidazole-2-thiones catalysts for epoxy/anhydride reactions (and other reactions) and a method of making these catalysts. Epoxy/anhydride coatings containing these improved catalysts offer the following advantages: improved appearance (especially since even weeks after application the coatings still have a "wet" look); better pot-life; improved resistance to alkaline substances which will improve durability; improved solubility; and coatings which have a reduced volatile organic content (VOC).
摘要翻译： 本发明公开了用于环氧/酸酐反应的1,3-二烷基咪唑-2-硫酮催化剂（和其它反应）和制备这些催化剂的方法。 含有这些改进的催化剂的环氧/酸酐涂层具有以下优点：外观改善（特别是涂层后几周甚至还具有“湿”外观）; 更好的适应期; 改善耐碱性，提高耐久性; 改善溶解度; 和具有降低的挥发性有机物含量（VOC）的涂层。
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8.发明授权公开(公告)号：US07868182B2
公开(公告)日：2011-01-11
申请号：US11622883
申请日：2007-01-12
IPC分类号： C07D233/30
CPC分类号： C07D233/84
摘要： A novel solventless process is described for the preparation of imidazole-2-thiones. The new solventless process tolerates a variety of bases as co-reactants which introduces feedstock flexibility into the process while the solventless feature renders the process more environmentally friendly by eliminating volatile organic solvents from the process, reducing energy consumption (associated with solvent recovery and/or recycling), and allows shorter reaction time and workup. Furthermore, the elimination of solvents enhances workplace safety by obviating the need for flammable and/or toxic solvents.
摘要翻译： 描述了用于制备咪唑-2-硫酮的新型无溶剂方法。 新的无溶剂方法耐受各种碱作为共反应物，其将原料灵活性引入该方法，而无溶剂特征通过从该方法中除去挥发性有机溶剂使得该方法更环保，降低能量消耗（与溶剂回收和/或 回收），并允许更短的反应时间和后处理。 此外，消除溶剂通过消除对易燃和/或有毒溶剂的需要增强了工作场所的安全性。
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公开(公告)号：US5332800A
公开(公告)日：1994-07-26
申请号：US134141
申请日：1993-10-12
IPC分类号： C07D245/02 , C07D255/04 , C07D257/02 , C07D257/10 , C07D259/00 , C08G69/00 , C08G69/32 , C08G69/16 , C08G73/00
CPC分类号： C07D255/04 , C07D257/10 , C07D259/00 , C08G69/00 , C08G69/32
摘要： This invention concerns cyclic aromatic amide oligomer compositions and a process for preparing such cyclic oligomers.
摘要翻译： 本发明涉及环状芳族酰胺低聚物组合物和制备这种环状低聚物的方法。
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10.发明授权Curable compositions containing 1,3-dialkylimidazole-2-thione catalysts 失效含有1,3-二烷基咪唑-2-硫酮催化剂的固化组合物
公开(公告)号：US5091498A
公开(公告)日：1992-02-25
申请号：US657737
申请日：1991-02-19
IPC分类号： C08G59/68 , C08K5/405 , C09D133/14 , C09D163/00
CPC分类号： C09D163/00 , C08G59/687 , C08K5/405 , C09D133/14
摘要： The present invention describes the use of 1,3-dialkylimidazole-2-thiones as a catalyst for epoxy/anhydride reactions (and other reactions) and a method of making these catalysts. Epoxy/anhydride coatings containing these improved catalysts offer the following advantages: improved appearance (especially since even weeks after application the coatings still have a "wet" look); better pot-life; improved resistance to alkaline substances which will improve durability; improved solubility; and coatings which have a reduced volatile organic content (VOC).
摘要翻译： 本发明描述了1,3-二烷基咪唑-2-硫酮作为环氧/酸酐反应（和其他反应）的催化剂的用途和制备这些催化剂的方法。 含有这些改进的催化剂的环氧/酸酐涂层具有以下优点：外观改善（特别是涂层后几周甚至还具有“湿”外观）; 更好的适应期; 改善耐碱性，提高耐久性; 改善溶解度; 和具有降低的挥发性有机物含量（VOC）的涂层。
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