Abstract:
A fluidized bed polymerization reactor which is a generally cylindrical vessel having a longitudinal axis and a fluidization grid located in the vessel generally perpendicular to the longitudinal axis of the vessel and defining a fluidized bed region above the fluidization grid. The reactor has an inlet for continuously introducing a gaseous stream of polymerizable monomers into the vessel below the fluidization grid at a gas velocity sufficient to maintain particles in the fluidized bed region in a suspended and fluidized condition; an outlet for removing polymer product from the fluidized bed region and an outlet for continuously removing an outlet stream of gaseous unreacted polymerizable monomer from the fluidized bed region. A cooling device cools at least a part of the outlet stream to a temperature at which liquid condenses out of the outlet stream, and a separating device separates at least a part of the cooled outlet stream into condensed liquid and a cooled gaseous stream. The separated cooled gaseous stream is returned to the inlet and an injection device injects at least a part of the condensed liquid into the fluidized bed region at a point where the gaseous stream of polymerizable monomers passing through the vessel has substantially reached the operating temperature of the polymerization reactor. The injection device includes at least one gas induced atomizing nozzle for injecting an atomized stream of the condensed liquid into the fluidized bed region in a direction generally perpendicular to the longitudinal axis of the vessel.
Abstract:
A continuous gas fluidized bed process for the polymerization of olefins, especially ethylene, propylene, or mixtures thereof with other alpha-olefins by cooling the recycle gas stream to condense some liquid (e.g., a comonomer), separating at least part of the liquid and spraying it under pressure through a nozzle (1) directly into the fluidized bed by pressurizing the liquid and feeding it to a spray nozzle (1) having a mechanical device (6) for atomizing the liquid, under conditions such that the spray is formed within a spray-forming zone (5) of the nozzle outlet. The spray-forming zone (5) is preferably shielded from the fluidized bed particles by a wall or walls which can be, for example, a tube or a plate. Also described is a nozzle having two or more series of outlets, each series being fed and controlled independently to enable improved turn-up/turn-down of the liquid supply to the bed.
Abstract:
The invention relates to continuous gas fluidised bed polymerisation of olefins, especially ethylene, propylene, or mixtures of these with other alpha olefins, wherein the monomer-containing recycle gas employed to fluidise the bed is cooled to condense out at least some liquid hydrocarbon. The condensed liquid, which can be a monomer or an inert liquid, is separated from the recycle gas and is fed directly to the bed to produce cooling by latent heat of evaporation. The liquid feeding to the bed can be through gas-induced atomiser nozzles (FIG. 2), or through liquid-only nozzles. The process provides substantially improved productivity of gas fluidised bed polymerisation of olefins.
Abstract:
The invention relates to continuous gas fluidized bed polymerization of olefins, especially ethylene, propylene, or mixtures of these with other alpha olefins, wherein the monomer-containing recycle gas employed to fluidize the bed is cooled to condense out at least some liquid hydrocarbon. The condensed liquid, which can be a monomer or an inert liquid, is separated from the recycle gas and is fed directly to the bed to produce cooling by latent heat of evaporation. The liquid feeding to the bed can be through gas-induced atomizer nozzles (FIG. 2), or through liquid-only nozzles. The process provides substantially improved productivity of gas fluidized bed polymerization of olefins.
Abstract:
The invention relates to continuous gas fluidised bed polymerisation of olefins, especially ethylene, propylene, or mixtures of these with other alpha olefins, wherein the monomer-containing recycle gas employed to fluidise the bed is cooled to condense out at least some liquid hydrocarbon. The condensed liquid, which can be a monomer or an inert liquid, is separated from the recycle gas and is fed directly to the bed to produce cooling by latent heat of evaporation. The liquid feeding to the bed can be through gas-induced atomiser nozzles (FIG. 2), or through liquid-only nozzles. The process provides substantially improved productivity of gas fluidised bed polymerisation of olefins.
Abstract:
A system and method for detecting faults within an electrosurgical instrument having a shield and an active electrode uses multiple possible fault conditions. In one embodiment the monitoring system comprises an electrosurgical generator coupled to the electrosurgical instrument and adapted to deliver power to the active electrode of the electrosurgical instrument, monitoring circuitry coupled to the electrosurgical generator and the electrosurgical instrument, wherein the monitoring circuitry comprises an active electrode voltage sensor an active electrode current sensor and a shield current sensor. The monitoring circuitry measures at least two of the active voltage, the active or return electrode current, and the shield current.
Abstract:
An electrical switching system for use in various types of electrosurgical instruments and related tools comprises a system adapted to automatically determine which of at least two electrical current modes to deliver through an electrosurgical instrument based on a condition sensed by the electrosurgical instrument. In another embodiment, the electrical switching system comprises a generator, the generator including a first electrical distribution systems for delivering monopolar electrical energy, and a second electrical distribution system for delivering bipolar electrical energy, a controller coupled to the generator for selecting based on an input which of the first and second electrical distribution systems to activate.
Abstract:
An electronic testing machine that tests electronic components using test contacts is disclosed. A contact takes a plurality of electrical readings for a component retained in a test plate as the test plate is moved in microsteps. These electrical readings can be used to determine alignment and/or to correct alignment as necessary using an adjustment mechanism.
Abstract:
A process and apparatus for contacting (a) at least one gaseous reactant and (b) at least one liquid selected from the group consisting of reactants, coolants and mixtures thereof in the presence of a fluidized bed of catalyst, in which the liquid is introduced into the reactor through at least one inlet located within the fluidization zone and the gaseous reactant is introduced into the reactor through at least one inlet located within the fluidization zone adjacent the support means.
Abstract:
Apparatus and process for heat exchange with fluid beds comprises heat-exchange tubes located longitudinally with respect to the axis of a fluidization zone with a rectangular pitch, one side of which having a length at least one and a half times the length of the other side and/or with a triangular pitch, having two sides each at least one and a half times the length of the shortest side reduces the impact of the heat-exchange tubes on the fluidization characteristics of the fluid bed. The invention is particularly suitable for oxidation reactions using molecular oxygen-containing gas in the presence of a fluid bed of fluidizable catalyst, such as (a) the acetoxylation of olefins, (b) the oxidation of ethylene to acetic acid and/or the oxidation of ethane to ethylene and/or acetic acid, (c) the ammoxidation of propylene and/or propane to acrylonitrile and (d) the oxidation of C4's to maleic anhydride.