摘要:
A device for carrying out a chemical reaction by a continuous method has a reactor with at least two reactor sections which define a direction of flow. The reactor has plug flow properties along the direction of flow. A recirculation line is present to withdraw a partial flow from the reactor at a first point and return it to the reactor at a second point located above the first point in the direction of flow. Means are provided which prevent a temperature increase in the reactor over a predetermined temperature range, for example change of more than approximately 50 K.
摘要:
There is provided a method and an apparatus for preparing graphite oxide. In accordance with the present disclosure, when an oxidizer is added by stages into a sequencing batch oxidizer mixer connected in multiple stages at a constantly low temperature, the oxidizer is mixed therein while suppressing an oxidation reaction. During an oxidation reaction of graphite, in a risky range of overheating and explosion, a tube type reactor equipped within a heat exchanger is used to accurately control a local temperature and the oxidizer can permeate between layers of the graphite with increased efficiency under ultrasonication. In an additional reaction range out of the risky range, a continuous stirred tank reactor is used to mature the oxidation reaction, so that a risk of explosion during manufacturing of graphite oxide can be reduced and a great amount of graphite oxide can be mass-produced economically.
摘要:
Method of processing and handling solids and mixtures capable of deflagration, in particular of processing materials capable of deflagration in the chemical and pharmaceutical industry, wherein the processing and handling is carried out in an environment under a reduced pressure of ≦500 mbara and the processing and/or handling comprises one or more process steps selected from the group consisting of filtration, milling, sieving, mixing, homogenization, granulation, compacting, packaging, drying, storage and transport in a transport container and other steps in apparatuses having mechanical internals.
摘要:
One exemplary embodiment can be a method for altering an operation of an alkylation unit during a process upset. The method may include blocking an outlet of a settler to a separation zone, and recycling at least a portion of a hydrocarbon stream to the separation zone to prevent an uncontrolled pressure rise in one or more distillation columns during shutdown of an alkylation reactor.
摘要:
A hydrocarbon-containing gas is mixed with an oxygen gas in a gas mixer in the presence of coarse water droplet environment, e.g., a ‘rainy’ or ‘driving rainstorm’ environment in which the water droplets generally have a size greater than 200 microns SMD. The water droplets surround and contact entrained particles in either the oxygen gas stream or the hydrocarbon-containing gas stream. The water acts to suppress, prevent and quench ignition of the hydrocarbon gas in the mixer which would otherwise be caused by energetic collisions between such particles and structures within the gas mixer. In one configuration the gas mixer includes water pipes having coarse water droplet-producing nozzles at the peripheral end thereof concentrically located within oxygen supply pipes. Additionally, nozzles introduce coarse water droplets into a pipe carrying the hydrocarbon gas and forming a mixing chamber for the hydrocarbon and oxygen gases.
摘要:
Safely processing fluid via monitoring and decreasing explosiveness of vapor-gas species formed therefrom, or contained therein. Fluid input unit 12, for transporting source fluid 24; first fluid processing unit 14, for receiving and processing fluid 26, and forming processed fluid including vapor-gas portion 30; vapor-gas explosiveness monitoring and decreasing unit 16, for measuring at least an indication of explosiveness level of vapor-gas portion 30, wherein if the measurement exceeds a pre-determined threshold explosiveness level (PDTEL), then vapor-gas portion 30 is condensed, for forming condensate and output vapor-gas 32 whose explosiveness level is less than lower explosion limit (LEL) of output vapor-gas 32; second fluid processing unit 18, for processing output vapor-gas 32, and forming processed vapor-gas product 34. Includes an output unit 20 for transporting processed vapor-gas product 34 as (vapor-gas, liquid, or/and solid) output products 36, for disposal, storage, or/and additional processing, and a central process control unit 22.
摘要:
[Problem] There is provided a method for producing an oxygen-containing compound safely and with improved reaction efficiency, in which an undesired peroxide is unlikely to be produced, and efficient heat exchange of the ozonization can be achieved.[Mean for solving the Problem] The method comprises an ozonization reaction step of continuously supplying, together with an organic compound, ozone having an oxygen content of less than 10% in a dissolved state in high-pressure carbon dioxide to an ozonization reaction section having a thin tubular shape, and reacting the ozone and the organic compound under conditions that suppress generation of oxygen due to thermal decomposition of the ozone, thereby continuously producing an ozonide; and a decomposition reaction step of continuously supplying the ozonide produced in the ozonization reaction step to a decomposition reaction section having a thin tubular shape, thereby continuously producing an oxygen-containing compound, the decomposition reaction step being provided in a manner continuous with the ozonization reaction step.
摘要:
A gas mixer (10) for mixing a first gas stream with a second gas stream includes an impact labyrinth (24) in the first gas stream having structures (25), e.g., corrugated walls, forming a tortuous path through which the first gas stream must pass en route to a mixing point (20) in the gas mixer. The labyrinth fosters ignition of particles entrained in the first gas stream. Elongate, straight pipes (30) receive the first gas stream from the impact labyrinth (24) and carrying the first gas stream to the mixing point (20) the pipes (30) are positioned with a vessel (12) carrying the second gas stream. The pipes (30) have openings which are substantially aligned with the flow direction of the second gas stream at the mixing point (20) thereby introducing the first gas stream into the second gas stream in a low shear manner.
摘要:
A tank (10) for storing a liquid with a device (11, 12) for feeding one or more substances thixotroping the liquid to the liquid in the tank (10) is characterised in that the device (11, 12) is designed so that it feeds the thixotroping substance or substances to the liquid in the tank (10) as a result of a signal from a signal transmitter, so that the liquid completely thixotropes, at least in a closed outer layer inside the tank (10) that cannot be penetrated by a residue of the liquid, not thixotroped if necessary. This ensures that by simple means the liquid present in the tank (10) is pretended from being discharged or from escaping under certain defined conditions, particularly in emergency situations.
摘要:
A method of treating a gas stream containing silane or other silicon-containing gas is described, in which the gas stream is conveyed to a liquid ring pump or screw-mechanism pump, to which are also supplied an oxidant for oxidising the silicon-containing gas within the pump, and a liquid for forming a liquid ring or intermittent flushing within the pump. A liquid stream containing said liquid and a by-product of the oxidation of the silicon-containing gas is exhaust from the pump.