摘要:
Process for preparing high-concentration gaseous formaldehyde having a molar CH2O:H2O ratio of ≧0.6 from an aqueous formaldehyde solution by evaporation of at least part of the solution, in which the aqueous formaldehyde solution is heated to a vaporization temperature T and the gas phase formed is taken off, wherein the evaporation temperature T obeys the relationship: T[° C.]≧T′min[° C.] where T′min(c)=A+B×(c/100)+C×(c/100)2+D×(c/100)3 and A=+68.759, B=+124.77, C=−12.851, D=−10.095, where c is the instantaneous CH2O content of the aqueous formaldehyde solution during the evaporation in percent by weight and is from 20 to 99% by weight.
摘要:
Process for preparing high-concentration formaldehyde solutions having a CH2O content of ≧50% by weight from an aqueous formaldehyde solution having a lower CH2O content by evaporation of part of this solution (partial evaporation), in which the aqueous formaldehyde solution is heated to an evaporation temperature T at which the gas phase becomes enriched in water relative to the liquid phase and the gas phase formed is taken off continuously or discontinuously, wherein the evaporation temperature T obeys the relationship: T[° C.]
摘要:
Process for preparing high-concentration formaldehyde solutions having a CH2O content of ≧50% by weight from an aqueous formaldehyde solution having a lower CH2O content by evaporation of part of this solution (partial evaporation), in which the aqueous formaldehyde solution is heated to an evaporation temperature T at which the gas phase becomes enriched in water relative to the liquid phase and the gas phase formed is taken off continuously or discontinuously, wherein the evaporation temperature T obeys the relationship: T[° C.]
摘要翻译:通过蒸发具有较低CH 2 O 2含量的甲醛水溶液制备CH 2 O 2含量> 50重量%的高浓度甲醛溶液的方法 该部分溶液(部分蒸发),其中甲醛水溶液被加热到气相相对于液相富集水的蒸发温度T,形成的气相连续或不连续地取出,其中 蒸发温度T遵循以下关系:<?in-line-formula description =“In-line Formulas”end =“lead”?> T [°C。] <°C] (c)= A + Bx(c / 100)+ Cx(c / 100) ) 2 + Dx(c / 100)3和A = + 68.759,B = + 124.77,C = -12.851,D = -10.095,其中c是瞬时 蒸发期间甲醛水溶液的CH 2 O 2 O含量为重量百分比,为20〜99% ht。
摘要:
A process for removing trioxane from a mixture I of formaldehyde, trioxane and water, by a) distilling the mixture I in a first distillation stage at a pressure of from 0.1 to 2 bar to obtain a stream II which comprises formaldehyde and a stream III which comprises predominantly trioxane and additionally water and formaldehyde, b) mixing the stream III with a recycle stream VII which comprises predominantly trioxane and additionally water and formaldehyde to obtain a stream IIIa which comprises predominantly trioxane and additionally water and formaldehyde, c) distilling the stream IIIa, if appropriate after removing low boilers from the stream III or IIIa in a further distillation stage, in a second distillation stage at a pressure of from 0.2 to 10 bar, the pressure in the second distillation stage being at least 0.1 bar higher than the pressure in the first distillation stage, to obtain a stream IV of trioxane and a stream V which comprises predominantly trioxane and additionally water and formaldehyde, d) distilling the stream V in a third distillation stage at a pressure of from 0.1 to 4 bar to obtain a stream VI which comprises predominantly water and additionally formaldehyde, and the recycle stream VII which comprises predominantly trioxane and additionally water and formaldehyde, e) if appropriate, distilling the stream VI in a fourth distillation stage to obtain a stream VIII which comprises predominantly water, and a stream IX which comprises predominantly formaldehyde.
摘要:
A method of welding workpieces of high-temperature superalloys is provided. Welding filler is applied in a plurality of layers to a surface of the workpiece via a heat input zone and a supply zone for supplying the welding filler into the heat input zone. The heat input zone and the supply zone on the one hand and the workpiece surface on the other hand are moved in relation to one another. A polycrystalline weld seam is generated by remelting a previously applied layer of the plurality of layers. Welding parameters are chosen such that a cooling rate during a solidifying of the material is at least 8000 Kelvins per second. Further, a welding apparatus for carrying out such a method is provided.
摘要:
In a method for repairing a machinery component, one or more defects are detected on the machinery component. At least one portion of the component is removed, wherein the at least one portion includes at least one of the one or more defects. One or more data points are determined for at least one slot, wherein the at least one slot is created by removing the at least one portion of the component. At least one repair coupon is generated from the one or more data points. The at least one repair coupon is attached with the at least one slot.
摘要:
In one aspect, a repair method for repairing components comprising a base material with a directed microstructure is provided. The repair is performed in such a way that the repaired location correspondingly has a directed microstructure like the surrounding base material. A solder is applied in the region of a location to be repaired and is soldered to the component via heat exposure, a temperature gradient, i.e., for instance a temperature variation from a higher temperature to a lower temperature, is thereby produced in the region of the location to be repaired.
摘要:
A welding apparatus for welding workpieces of high-temperature superalloys is provided. The welding apparatus includes a heat source for producing a heat input zone on the workpiece surface, a supplying device for supplying welding filler into the heat input zone and a transporting device for producing a relative movement between the heat source and the supplying device on the one hand and the workpiece surface on the other hand. The welding apparatus further includes a control unit with a control program, which carries out the relative movement in such a way that the welding power and the diameter of the heat input zone are set such that the cooling rate during the solidifying of the material is at least 8000 Kelvins per second.
摘要:
A method of welding workpieces of high-temperature superalloys is provided. Welding filler is applied in a plurality of layers to a surface of the workpiece via a heat input zone and a supply zone for supplying the welding filler into the heat input zone. The heat input zone and the supply zone on the one hand and the workpiece surface on the other hand are moved in relation to one another. A polycrystalline weld seam is generated by remelting a previously applied layer of the plurality of layers. Welding parameters are chosen such that a cooling rate during a solidifying of the material is at least 8000 Kelvins per second. Further, a welding apparatus for carrying out such a method is provided.
摘要:
The disclosure relates to a method of inhibiting synthesis of viral DNA in a mammal infected with a hepatitis B virus. This method includes administering at least one Phyllanthus component or substance to a mammal infected with the hepatitis B virus. It also includes inhibiting hepatitis B viral DNA synthesis in the mammal using the Phyllanthus component or substance. The disclosure also relates to a method of inhibiting viral gene expression in a mammal infected with a hepatitis B virus. This method includes administering at least one Phyllanthus component or substance to a mammal infected with the hepatitis B virus. It also includes inhibiting expression of at least one hepatitis B viral gene in the mammal using the Phyllanthus component or substance. These methods may form part of a method of preventing or treating hepatitis B infection.