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公开(公告)号：US20060183882A1
公开(公告)日：2006-08-17
申请号：US11276275
申请日：2006-02-22
IPC分类号： C08G65/04
CPC分类号： C08G65/2654 , C08G18/4866 , C08G65/2696
摘要： A continuous process for preparation of a polyether polyol in a reactor includes introducing an initial starter/catalyst mixture into the reactor. The initial starter/catalyst mixture comprises an initial starter and a catalyst with the catalyst selected from aluminum phosphate catalysts and/or aluminum phosphonate catalysts and/or residues of these catalysts. In this continuous process, one or more alkylene oxide is continuously introduced into the reactor. Additional amounts of the catalyst and a continuous starter are also continuously introduced into the reactor. The polyether polyol prepared herein is continuously withdrawn from the reactor.
摘要翻译： 在反应器中制备聚醚多元醇的连续方法包括将初始起始物/催化剂混合物引入反应器。 初始起始物/催化剂混合物包含初始起始物和催化剂，催化剂选自磷酸铝催化剂和/或磷酸铝酯催化剂和/或这些催化剂的残余物。 在该连续方法中，将一种或多种环氧烷连续引入反应器。 额外量的催化剂和连续起动器也被连续引入反应器。 本文制备的聚醚多元醇从反应器中连续取出。
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公开(公告)号：US09132387B2
公开(公告)日：2015-09-15
申请号：US13712536
申请日：2012-12-12
CPC分类号： B01D61/246 , B01D11/0288 , B01D11/0292 , B01D11/0415 , B01D61/243 , C07C41/38
摘要： The invention relates to a process for working-up a reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst, wherein at least alkali metal ions of the dissolved alkali metal comprising catalyst are partially or completely removed from the mixture by a membrane separation process, the process comprising following steps: (a) feeding the reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst into a first chamber (1) of a separation unit (3), (b) feeding a solvent into a second chamber (7) of the separation unit (3), the first chamber (1) and the second chamber (7) being separated by a membrane (9), (c) transporting at least the alkali metal ions of the alkali metal comprising catalyst from the first chamber (1) into the second chamber by passing through the membrane (9).
摘要翻译： 本发明涉及一种用于处理包含聚醚醚和包含催化剂的溶解的碱金属的反应混合物（5）的方法，其中至少包含催化剂的溶解的碱金属的碱金属离子通过膜分离部分或完全从混合物中除去 方法包括以下步骤：（a）将包含聚乙烯醇和包含催化剂的溶解的碱金属的反应混合物（5）进料到分离单元（3）的第一室（1）中，（b）将溶剂进料到第二 分离单元（3）的室（7），第一室（1）和第二室（7）被隔膜（9）隔开，（c）至少输送包含催化剂的碱金属的碱金属离子 从第一腔室（1）通过膜（9）进入第二腔室。
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3.发明授权Process for preparing a C4-olefin mixture by selective hydrogenation and metathesis process for using this stream 有权通过选择性氢化和复分解方法制备C4烯烃混合物的方法公开(公告)号：US08362308B2
公开(公告)日：2013-01-29
申请号：US13042142
申请日：2011-03-07
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
IPC分类号： C07C5/02
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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4.发明授权Process for preparing a C4-olefin mixture by selective hydrogenation and metathesis process for using this stream 有权通过选择性氢化和复分解方法制备C4烯烃混合物的方法公开(公告)号：US07923588B2
公开(公告)日：2011-04-12
申请号：US11665161
申请日：2005-10-13
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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5.发明申请Process For Preparing A C4-Olefin Mixture By Selective Hydrogenation And Metathesis Process For Using This Stream 有权通过选择性氢化和复分解方法制备C4-烯烃混合物的方法公开(公告)号：US20080188696A1
公开(公告)日：2008-08-07
申请号：US11665161
申请日：2005-10-13
申请人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
发明人： Jurgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Roper , Thomas Hill
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译： 描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。 本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。
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公开(公告)号：US08957257B2
公开(公告)日：2015-02-17
申请号：US13551936
申请日：2012-07-18
申请人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Loffler , Fatemeh Admadnian , Ralf Bohling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
发明人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Loffler , Fatemeh Admadnian , Ralf Bohling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
CPC分类号： C07C41/03 , B01J4/004 , B01J19/248 , B01J2219/00768 , B01J2219/182 , B01J2219/1943 , C08G65/2609 , C08G65/2696 , C07C43/11
摘要： A process for a continuous production of a polyetherol first involves reacting a catalyst (5) with an alcohol starter (3) or an alkoxylated precursor, to give a mixture comprising an alcoholate and water. Water is then removed from the mixture. The process further involves feeding the alcoholate into a bubble column and feeding an alkylene oxide into the bottom of a compartment of the bubble column, such that the alkylene oxide rises in the alcoholate. The alkylene oxide then reacts with the alcoholate or a secondary product from the reaction between the alcoholate and alkylene oxide, to give the polyetherol.
摘要翻译： 首先连续生产聚醚醚的方法包括使催化剂（5）与醇起始物（3）或烷氧基化前体反应，得到包含醇化物和水的混合物。 然后从混合物中取出水。 该方法进一步包括将醇化物进料到气泡塔中并将环氧烷进料到泡罩塔的隔室的底部，使得烯化氧在醇化物中上升。 然后烯化氧与醇化物或醇化物和环氧烷之间的反应产生的次生物反应，得到聚醚。
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公开(公告)号：US08546606B2
公开(公告)日：2013-10-01
申请号：US10546890
申请日：2004-02-20
申请人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Woelfert , Steffen Oehlenschlaeger
发明人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Woelfert , Steffen Oehlenschlaeger
IPC分类号： C07C249/00
CPC分类号： B01J19/242 , B01J19/243 , B01J2219/00166 , B01J2219/182 , B01J2219/185 , B01J2219/187 , C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting primary amines with phosgene, which comprises the steps a) mixing the amine with the phosgene, b) reacting the amine with the phosgene in a residence reactor and, if desired, c) transferring the output from the reactor of step b) into a distillation column, wherein the residence reactor in step b) is configured as a tube reactor.
摘要翻译： 本发明涉及通过使伯胺与光气反应制备多异氰酸酯的方法，其包括以下步骤：a）将胺与光气混合，b）使胺与光气在停留反应器中反应，如果需要，c）将 从步骤b）的反应器输出到蒸馏塔中，其中步骤b）中的停留反应器被配置为管式反应器。
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公开(公告)号：US20130023700A1
公开(公告)日：2013-01-24
申请号：US13551936
申请日：2012-07-18
申请人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Löffler , Fatemeh Ahmadnian , Ralf Böhling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
发明人： Vinit Chilekar , Oliver Bey , Andreas Brodhagen , Achim Löffler , Fatemeh Ahmadnian , Ralf Böhling , Christoph Grossmann , Ulrich Kammel , Ronald Adelmann , Thomas Ostrowski , Milind Joshi , Gerrit Waters , Dirk Meckelnburg
IPC分类号： C07C41/02
CPC分类号： C07C41/03 , B01J4/004 , B01J19/248 , B01J2219/00768 , B01J2219/182 , B01J2219/1943 , C08G65/2609 , C08G65/2696 , C07C43/11
摘要： A process for a continuous production of a polyetherol first involves reacting an alcohol with a starter or an alkoxylated precursor, to give a mixture comprising an alcoholate and water. Water is then removed from the mixture. The process further involves feeding the alcoholate into a bubble column and feeding an alkylene oxide into the bottom of a compartment of the bubble column, such that the alkylene oxide rises in the alcoholate. The alkylene oxide then reacts with the alcoholate or a secondary product from the reaction between the alcoholate and alkylene oxide, to give the polyetherol.
摘要翻译： 首先连续生产聚乙二醇的方法包括使醇与起始物或烷氧基化前体反应，得到包含醇化物和水的混合物。 然后从混合物中取出水。 该方法进一步包括将醇化物进料到气泡塔中并将环氧烷进料到泡罩塔的隔室的底部，使得烯化氧在醇化物中上升。 然后烯化氧与醇化物或醇化物和环氧烷之间的反应产生的次生物反应，得到聚醚。
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公开(公告)号：US07482500B2
公开(公告)日：2009-01-27
申请号：US10584758
申请日：2004-12-30
申请人： Thorsten Johann , Götz-Peter Schindler , Andreas Brodhagen , Sven Crone , Regina Benfer , Thomas Hill , Mark Duda
发明人： Thorsten Johann , Götz-Peter Schindler , Andreas Brodhagen , Sven Crone , Regina Benfer , Thomas Hill , Mark Duda
CPC分类号： C07C5/333 , C07C5/48 , C07C11/167
摘要： The disclosure relates to a process for preparing butadiene. The process involves nonoxidatively catalytically dehydrogenating butane to obtain a product gas stream containing butane, 1-butene, 2-butene, butadiene, hydrogen and secondary constituents. The 1-butene and 2-butene of the product gas stream is then oxidatively dehydrogenated to give a second gas stream containing butane,2-butene, butadiene, hydrogen, steam and secondary constituents. Next, the butane,2-butene and butadiene are separated from the second gas stream and the butane and 2-butene are then separated from the butadiene product. The butane and 2-butene are then recycled into the nonoxidative catalytic dehydrogenating zone.
摘要翻译： 本公开涉及一种制备丁二烯的方法。 该方法涉及非氧化催化脱氢丁烷，以获得含有丁烷，1-丁烯，2-丁烯，丁二烯，氢和二次成分的产物气流。 然后将产物气流的1-丁烯和2-丁烯氧化脱氢，得到含有丁烷，2-丁烯，丁二烯，氢气，蒸汽和二级成分的第二气流。 接下来，将丁烷，2-丁烯和丁二烯与第二气流分离，然后从丁二烯产物中分离丁烷和2-丁烯。 然后将丁烷和2-丁烯循环到非氧化催化脱氢区。
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公开(公告)号：US20070179330A1
公开(公告)日：2007-08-02
申请号：US10584785
申请日：2004-12-30
CPC分类号： C07C5/333 , C07C5/48 , C07C11/167
摘要： The invention relates to a process for preparing butadiene from n-butane having the steps of A) providing a feed gas stream a comprising n-butane; B) feeding the feed gas stream a comprising n-butane into at least one first dehydrogenation zone and nonoxidatively catalytically dehydrogenating n-butane to obtain a product gas stream b comprising n-butane, 1-butene, 2-butene, butadiene, hydrogen, low-boiling secondary constituents and in some cases steam; C) feeding the product gas stream b of the nonoxidative catalytic dehydrogenation and an oxygenous gas into at least one second dehydrogenation zone and oxidatively dehydrogenating 1-butene and 2-butene to obtain a product gas stream c comprising n-butane, 2-butene, butadiene, hydrogen, low-boiling secondary constituents and steam, said product gas stream c having a higher content of butadiene than the product gas stream b; D) removing hydrogen, the low-boiling secondary constituents and steam to obtain a C4 product gas stream d substantially consisting of n-butane, 2-butene and butadiene; E) feeding the C4 product gas stream d into a distillation zone and removing a butadiene/butane mixture as the product of value stream e1, to leave a stream e2 consisting substantially of n-butane and 2-butene; F) recycling the stream e2 into the first dehydrogenation zone.
摘要翻译： 本发明涉及一种从正丁烷制备丁二烯的方法，该方法具有以下步骤：A）提供包含正丁烷的进料气流a; B）将包含正丁烷的进料气流（a）进料到至少一个第一脱氢区和非氧化催化脱氢的正丁烷中，以获得包含正丁烷，1-丁烯，2-丁烯，丁二烯，氢， 低沸点次生成分，有时还有蒸汽; C）将非氧化催化脱氢的产物气流b和氧气输送到至少一个第二脱氢区，并使1-丁烯和2-丁烯氧化脱氢得到包含正丁烷，2-丁烯， 丁二烯，氢，低沸点二次成分和蒸汽，所述产物气流c具有比产物气流b更高含量的丁二烯; D）除去氢气，低沸点次级组分和蒸汽，得到基本上由正丁烷，2-丁烯和丁二烯组成的C 4 H 4产物气流d; E）将C 4 H 4产物气流d进料到蒸馏区中并除去作为值流e1的产物的丁二烯/丁烷混合物，以留下基本上由正丁烷和2- 丁烯 F）将流e2再循环到第一脱氢区。
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