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    Catalyst for the Growth of Carbon Single-Walled Nanotubes
    2.
    发明申请
    Catalyst for the Growth of Carbon Single-Walled Nanotubes 有权
    碳单壁纳米管生长催化剂

    公开(公告)号：US20070281087A1

    公开(公告)日：2007-12-06

    申请号：US11669128

    申请日：2007-01-30

    申请人： Avetik Harutyunyan ,  Toshio Tokune ,  Elena Mora

    发明人： Avetik Harutyunyan ,  Toshio Tokune ,  Elena Mora

    IPC分类号： C23C16/26

    CPC分类号： B01J35/0013 ,  B01J21/185 ,  B01J23/28 ,  B01J23/44 ,  B01J23/74 ,  B01J37/0211 ,  B01J37/343 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  C01B2202/02 ,  Y10S977/843

    摘要： Methods and processes for synthesizing single-wall carbon nanotubes are provided. A carbon precursor gas is contacted with metal catalysts deposited on a support material. The metal catalysts are preferably nanoparticles having diameters less than about 3 nm. The reaction temperature is selected such that it is near the eutectic point of the mixture of metal catalyst particles and carbon. Further, the rate at which hydrocarbons are fed into the reactor is equivalent to the rate at which the hydrocarbons react for given synthesis temperature. The methods produce carbon single-walled nanotubes having longer lengths.

    摘要翻译： 提供了合成单壁碳纳米管的方法和方法。 碳前体气体与沉积在载体材料上的金属催化剂接触。 金属催化剂优选直径小于约3nm的纳米颗粒。 选择反应温度使其接近金属催化剂颗粒和碳的混合物的共晶点。 此外，烃进料到反应器中的速率等于烃在给定合成温度下反应的速率。 该方法产生长度较长的碳单壁碳纳米管。

    Method of preparing carbon nanotube containing electrodes
    3.
    发明授权
    Method of preparing carbon nanotube containing electrodes 有权
    制备含有碳纳米管的电极的方法

    公开(公告)号：US08124043B2

    公开(公告)日：2012-02-28

    申请号：US11723185

    申请日：2007-03-16

    申请人： Avetik Harutyunyan ,  Elena Mora

    发明人： Avetik Harutyunyan ,  Elena Mora

    IPC分类号： D01F9/12 ,  B01J23/00 ,  H01B1/06

    CPC分类号： H01M8/0234 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  H01M4/90 ,  H01M4/9083 ,  H01M4/92 ,  H01M4/926 ,  Y10S977/742

    摘要： The present teachings are directed toward a matrix containing nanosized metal components and carbon nanotubes, with the carbon nanotubes being produced in situ by the nanosized metal components upon the contacting of the nanosized metal components with a carbon source under conditions sufficient to produce the carbon nanotubes. Also disclosed are methods of producing the matrix containing the nanosized metal components and carbon nanotubes.

    摘要翻译： 本教导涉及含有纳米尺寸金属组分和碳纳米管的基质，其中在纳米金属组分与碳源在足以产生碳纳米管的条件下接触时，纳米金属组分原位产生碳纳米管。 还公开了制备含有纳米尺寸金属组分和碳纳米管的基质的方法。

    Method of determining lifetime of a nanotube-producing catalyst
    7.
    发明授权
    Method of determining lifetime of a nanotube-producing catalyst 有权
    确定纳米管生产催化剂寿命的方法

    公开(公告)号：US08026100B2

    公开(公告)日：2011-09-27

    申请号：US12108566

    申请日：2008-04-24

    申请人： Elena Mora ,  Avetik Harutyunyan

    发明人： Elena Mora ,  Avetik Harutyunyan

    IPC分类号： G01N23/00

    CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/162 ,  C01B2202/02

    摘要： The present teachings are directed toward methods of determining the lifetime of a catalyst for producing carbon nanotubes. The methods include providing different isotopically-labeled reaction components, primarily hydrocarbon sources containing different carbon isotopes, to the catalyst and measuring the Raman spectra of the carbon nanotubes produced with the different hydrocarbon sources.

    摘要翻译： 本教导涉及确定用于生产碳纳米管的催化剂的寿命的方法。 这些方法包括向催化剂提供不同的同位素标记的反应组分，主要是含有不同碳同位素的烃源，并测量用不同烃源生产的碳纳米管的拉曼光谱。

    Method of Determining Lifetime of a Nanotube-Producing Catalyst
    8.
    发明申请
    Method of Determining Lifetime of a Nanotube-Producing Catalyst 有权
    确定纳米管生产催化剂寿命的方法

    公开(公告)号：US20080292532A1

    公开(公告)日：2008-11-27

    申请号：US12108566

    申请日：2008-04-24

    申请人： Elena Mora ,  Avetik Harutyunyan

    发明人： Elena Mora ,  Avetik Harutyunyan

    IPC分类号： G01N31/10 ,  D01F9/127

    CPC分类号： B82Y40/00 ,  B82Y30/00 ,  C01B32/162 ,  C01B2202/02

    摘要： The present teachings are directed toward methods of determining the lifetime of a catalyst for producing carbon nanotubes. The methods include providing different isotopically-labeled reaction components, primarily hydrocarbon sources containing different carbon isotopes, to the catalyst and measuring the Raman spectra of the carbon nanotubes produced with the different hydrocarbon sources.

    摘要翻译： 本教导涉及确定用于生产碳纳米管的催化剂的寿命的方法。 这些方法包括向催化剂提供不同的同位素标记的反应组分，主要是含有不同碳同位素的烃源，并测量用不同烃源生产的碳纳米管的拉曼光谱。

    Methods for growing long carbon single-walled nanotubes
    9.
    发明授权
    Methods for growing long carbon single-walled nanotubes 有权
    生长长碳单壁纳米管的方法

    公开(公告)号：US07871591B2

    公开(公告)日：2011-01-18

    申请号：US11329499

    申请日：2006-01-10

    申请人： Avetik Harutyunyan ,  Elena Mora ,  Toshio Tokune

    发明人： Avetik Harutyunyan ,  Elena Mora ,  Toshio Tokune

    IPC分类号： D01F9/12

    CPC分类号： D01F9/1272 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/162 ,  C01B2202/02

    摘要： Methods and processes for synthesizing single-wall carbon nanotubes are provided. A carbon precursor gas is contacted with metal catalysts deposited on a support material. The metal catalysts are preferably nanoparticles having diameters less than about 3 nm. The reaction temperature is selected such that it is near the eutectic point of the mixture of metal catalyst particles and carbon. Further, the rate at which hydrocarbons are fed into the reactor is equivalent to the rate of formation of carbon SWNTs for given synthesis temperature. The methods produce carbon single-walled nanotubes having longer lengths.

    摘要翻译： 提供了合成单壁碳纳米管的方法和方法。 碳前体气体与沉积在载体材料上的金属催化剂接触。 金属催化剂优选直径小于约3nm的纳米颗粒。 选择反应温度使其接近金属催化剂颗粒和碳的混合物的共晶点。 此外，烃类进料到反应器中的速率等于给定合成温度下碳SWNTs的形成速率。 该方法产生长度较长的碳单壁碳纳米管。

    Catalyst for synthesis of carbon single-walled nanotubes
    10.
    发明授权
    Catalyst for synthesis of carbon single-walled nanotubes 有权
    用于合成碳单壁纳米管的催化剂

    公开(公告)号：US07485600B2

    公开(公告)日：2009-02-03

    申请号：US10992277

    申请日：2004-11-17

    申请人： Avetik Harutyunyan ,  Toshio Tokune ,  Elena Mora Fernandez

    发明人： Avetik Harutyunyan ,  Toshio Tokune ,  Elena Mora Fernandez

    IPC分类号： B01J23/00 ,  B01J23/70 ,  B01J23/08 ,  B01J20/00 ,  B01J21/00

    CPC分类号： D01F9/127 ,  B82Y30/00 ,  D01F9/1272

    摘要： Methods and processes for preparing supported metal catalysts are provided, where the supported metal catalysts can be used for the bulk synthesis of carbon nanotubes. The salts of the metal and the support are selected such that they are soluble in the same solvent. The catalyst can be prepared from the liquid phase through joint precipitation of the metal and the support material. The methods can be used to increase the metal load on the support. Use of the catalysts increases the yield of the carbon nanotubes.

    摘要翻译： 提供了制备载体金属催化剂的方法和方法，其中负载的金属催化剂可用于碳纳米管的本体合成。 选择金属和载体的盐，使得它们可溶于相同的溶剂。 可以通过金属和载体材料的接合沉淀从液相制备催化剂。 这些方法可用于增加支撑体上的金属负载。 催化剂的使用增加了碳纳米管的产率。