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    Process for the production of a photochromic object
    2.
    发明授权
    Process for the production of a photochromic object 失效
    制备光致变色物体的方法

    公开(公告)号：US06171525B2

    公开(公告)日：2001-01-09

    申请号：US09005754

    申请日：1998-01-12

    申请人： Erhard Effer ,  Manfred Melzig ,  Herbert Zinner ,  Herbert Schuster

    发明人： Erhard Effer ,  Manfred Melzig ,  Herbert Zinner ,  Herbert Schuster

    IPC分类号： G02B523

    CPC分类号： G02B5/23 ,  B29C67/0007 ,  C08F2/44 ,  C08F20/12 ,  C08K5/357 ,  C09K9/02 ,  G02B1/04 ,  C08L33/06

    摘要： Disclosed is a process for the production of a photochromic object, composed of a polymer and containing at least one spirooxazin compound, having the following process steps: an acrylate monomer or a methacrylate monomer, respectively a mixture of a multiple thereof is utilized as the polymerizable monomer, the photochromic dyes as well as a polymerization initiator are mixed in the polymerizable monomer, the mixture yielded thereby is placed in a casting mold, polymerized and hardened. The present invention is distinguished by, in order to obtain a neutral gray, neutral brown or green photochromic tint of the polymerizable mixture, several photochromic dyes being added of which at least one is not a spirooxazin, and by the concentration of the spirooxazin compound(s) amounting to no more than 0.045 weight percent relative to the mass of the utilized monomer, and that of the polymerization initiator(s) amounting to more than 1 weight percent relative to the mass of the utilized monomer.

    摘要翻译： 公开了一种制备由聚合物组成并含有至少一种螺恶嗪化合物的光致变色物体的方法，其具有以下工艺步骤：将丙烯酸酯单体或甲基丙烯酸酯单体分别为其复数的混合物用作可聚合的 单体，光致变色染料以及聚合引发剂混合在可聚合单体中，由此得到的混合物放入铸模中进行聚合和硬化。本发明的区别在于为了获得中性灰色，中性棕色 或可聚合混合物的绿色光致变色色调，加入几种光致变色染料，其中至少一种不是螺恶嗪酮，通过螺环嗪化合物的浓度相对于所用单体的质量不超过0.045重量％ ，聚合引发剂的量相对于所用单体的质量大于1重量％。

    Anti-reflection film for an optical element consisting of an organic material
    3.
    发明授权
    Anti-reflection film for an optical element consisting of an organic material 失效
    用于由有机材料组成的光学元件的防反射膜

    公开(公告)号：US4852974A

    公开(公告)日：1989-08-01

    申请号：US41101

    申请日：1987-03-19

    申请人： Manfred Melzig ,  Erhard Effer

    发明人： Manfred Melzig ,  Erhard Effer

    IPC分类号： G02B1/111 ,  G02C7/10

    CPC分类号： G02B1/111 ,  G02C7/102 ,  G02C2202/16

    摘要： An anti-reflection film of several layers is described for an optical element consisting of an organic material with photochromic properties.The film according to the invention is characterized by the fact that the mean reflection of the film over the spectral range between 330 nm and 380 nm is less than 4% and the mean reflection over the range between 290 nm and 330 nm is greater than 15%. This reflection behavior serves to prevent the stimulation of the photochromic effect by light with too short a wavelength from reducing the useful life of the photochromic effect. In addition, a suitable choice of the reflection properties means that a deliberate stimulation of photochromic molecules situated in certain steric positions and so influence on the kinetics and color of the photochromic effect can be obtained.

    摘要翻译： PCT No.PCT / DE86 / 00299 Sec。 371日期1987年3月19日 102（e）1987年3月19日PCT PCT 1986年7月21日PCT公布。 公开号WO87 / 00641 日本1987年1月29日。对于由具有光致变色性质的有机材料组成的光学元件，描述了几层防反射膜。 根据本发明的膜的特征在于，在330nm和380nm之间的光谱范围上的膜的平均反射小于4％，并且在290nm和330nm之间的范围上的平均反射大于15 ％。 这种反射行为用于防止由于具有太短波长的光刺激光致变色效应而减少光致变色效应的使用寿命。 此外，反射性质的合适选择意味着可以有意地刺激位于某些空间位置的光致变色分子，从而影响光致变色作用的动力学和颜色。

    High index curable photochromic composition and its process
    4.
    发明授权
    High index curable photochromic composition and its process 失效
    高指数固化光致变色组合物及其工艺

    公开(公告)号：US06933325B2

    公开(公告)日：2005-08-23

    申请号：US10269091

    申请日：2002-10-11

    申请人： Qiang Zheng ,  Donald Scott Nelson ,  Charles William Carper, Jr. ,  Manfred Melzig ,  Herbert Schuster ,  Herbert Zinner

    发明人： Qiang Zheng ,  Donald Scott Nelson ,  Charles William Carper, Jr. ,  Manfred Melzig ,  Herbert Schuster ,  Herbert Zinner

    IPC分类号： C08F222/10 ,  G02B1/04 ,  C08F2/46 ,  C08F2/50

    CPC分类号： C08F222/1006 ,  G02B1/041 ,  C08L33/14

    摘要： A high refractive index, curable, synthetic resin composition comprising a core resin composition composed of a mixture of ethylenically unsaturated compounds, and an initiation system containing both photo and thermal initiators, particularly a photochromic resin composition which further includes at least one photochromic dye. Also a curing process, which includes a combination of multi-step radiation curing and thermal annealing. Articles produced of cured composition exhibit superior physical and, in appropriate cases, photochromic properties and can be easily mass produced on a commercial scale due to short processing time and use of readily available chemicals.

    摘要翻译： 高折射率可固化的合成树脂组合物，其包含由烯属不饱和化合物的混合物组成的芯树脂组合物和含有光引发剂和热引发剂的引发体系，特别是进一步包含至少一种光致变色染料的光致变色树脂组合物。 还有一个固化过程，包括多步辐射固化和热退火的组合。 由固化的组合物制成的制品表现出优异的物理性质，在合适的情况下表现出光致变色性质，并且由于加工时间短和使用容易获得的化学品，可以以商业规模容易地批量生产。

    Photochromic benzopyrans
    6.
    发明授权
    Photochromic benzopyrans 失效
    光致变色苯并吡喃

    公开(公告)号：US07892296B2

    公开(公告)日：2011-02-22

    申请号：US12738124

    申请日：2008-11-25

    申请人： Manfred Melzig ,  Yven Rohlfing ,  Udo Weigand

    发明人： Manfred Melzig ,  Yven Rohlfing ,  Udo Weigand

    IPC分类号： C07D311/00

    CPC分类号： G03C1/73 ,  C07D311/94 ,  C09B57/00 ,  G02B5/23

    摘要： The present invention relates to photochromic benzopyrans and to the use thereof in plastics of all kinds, especially for ophthalmic purposes. The inventive compounds are photochromic benzopyran compounds in which a polycyclic aromatic is joined to the 5 and 6 positions of a benzopyran, where the bond in the 6 position is direct and the bond in the 5 position is via a mono- or diatomic bridge.

    摘要翻译： 本发明涉及光致变色苯并吡喃及其在各种塑料中的用途，特别是用于眼用目的。 本发明化合物是其中多环芳族化合物连接到苯并吡喃的5和6位的光致变色苯并吡喃化合物，其中6位上的键是直接的，并且5位的键通过单原子或双原子桥。

    Photochromic naphthopyrans
    7.
    发明授权
    Photochromic naphthopyrans 失效
    光致变色萘并吡喃

    公开(公告)号：US07459555B2

    公开(公告)日：2008-12-02

    申请号：US10013518

    申请日：2001-12-13

    申请人： Manfred Melzig ,  Claudia Mann ,  Udo Weigand

    发明人： Manfred Melzig ,  Claudia Mann ,  Udo Weigand

    IPC分类号： C07D265/30 ,  C07D405/00 ,  C07D311/78 ,  C07D307/77

    CPC分类号： C07D493/04 ,  C07D311/78 ,  C07D311/94 ,  C07D311/96 ,  C07D493/10 ,  G02B5/23

    摘要： The present invention relates to photochromic 2H-naphtho[1,2-b]pyrans as well as their use in synthetic resins of all types, especially for ophthalmic purposes. In particular, the present invention relates to photochromic naphthopyran compounds, for which a further ring system is bonded to the f side of the naphthopyran. The inventive photochromic dyes generally have the general formula (I) wherein n, R1, R2, R3, X, B and B′ are defined as in claim 1. The inventive compounds are distinguished by good darkening and decolorizing properties and a very good service life.

    摘要翻译： 本发明涉及光致变色2H-萘并[1,2-b]吡喃，以及它们在所有类型的合成树脂中的用途，特别是用于眼用目的。 特别地，本发明涉及光致变色萘并吡喃化合物，其另外的环系结合在萘并吡喃的f侧。 本发明的光致变色染料通常具有通式（I），其中n，R 1，R 2，R 3，X，B和B'如权利要求1中所定义。本发明化合物的特征在于良好的变暗和脱色性能以及良好的服务 生活。

    Photochromic Plastic Object
    8.
    发明申请
    Photochromic Plastic Object 有权
    光致变色塑料对象

    公开(公告)号：US20080251772A1

    公开(公告)日：2008-10-16

    申请号：US12138117

    申请日：2008-06-12

    申请人： Yven Rohlfing ,  Udo Weigand ,  Manfred Melzig

    发明人： Yven Rohlfing ,  Udo Weigand ,  Manfred Melzig

    IPC分类号： G02B5/23 ,  G02C7/10

    CPC分类号： G03C1/73 ,  B82Y20/00 ,  B82Y30/00 ,  C09K9/02 ,  G02B1/04 ,  G02B5/23

    摘要： A photochromic plastic object which is composed of a transparent polymeric synthetic resin material, into or onto which at least one substantially mesoporous inorganic host structure is introduced or applied containing one or more embedded organic photochromic dye molecules so as to form a photochromic nanocomposite material. In contrast to prior techniques of adding or applying the photochromic organic dyes to the monomer mixture or prepolymer of a transparent synthetic resin material in a molecular form, in the photochromic plastic article of the present invention color is generated by using the photochromic nanocomposite particles or photochromic nanocomposite structures.

    摘要翻译： 由透明聚合物合成树脂材料构成的光致变色塑料物体被引入或涂覆有至少一个基本上介孔的无机主体结构，其中含有一个或多个嵌入的有机光致变色染料分子以形成光致变色纳米复合材料。 与将光致变色有机染料加入或应用于分子形式的透明合成树脂材料的单体混合物或预聚物的现有技术相反，在本发明的光致变色塑料制品中，通过使用光致变色纳米复合材料颗粒或光致变色 纳米复合结构。

    Photochromically colored object
    10.
    发明授权
    Photochromically colored object 失效
    光彩色物体

    公开(公告)号：US6102543A

    公开(公告)日：2000-08-15

    申请号：US878

    申请日：1997-12-30

    申请人： Manfred Melzig

    发明人： Manfred Melzig

    IPC分类号： C08F20/10 ,  C08F220/20 ,  C08J7/00 ,  C08K5/34 ,  C08L31/04 ,  C08L33/08 ,  C09B57/00 ,  C09K3/00 ,  C09K9/02 ,  G02B1/04 ,  G02B5/23 ,  G02C7/10

    CPC分类号： C09K9/02 ,  G02B5/23 ,  G02C7/102

    摘要： Disclosed is an object made of plastic material, in particular a plastic ophthalmic lens, colored with at least one photochromic substance which is also excited by light in the UV range of the spectrum and has a higher absorption in the excited state, judged by the spectral light sensitivity of the human eye, than in the not excited state and to which, in addition, at least one UV absorbing material is added in such a concentration that darkening of the photochromic substance(s) is independent of the UV fraction of the excitation light.But rather the intensity of the darkening depends on brightness, i.e. the intensity integrated over the spectral light sensitivity of the human eye V.sub.2.

    摘要翻译： 公开了由塑料材料制成的物体，特别是用至少一种光致变色物质着色的塑料眼镜片，该光致变色物质在光谱的UV范围内被光激发，并且在激发状态下具有更高的吸收，由光谱 人的眼睛的光敏感性比在非激发状态下还要加入至少一种UV吸收材料，其浓度使得光致变色物质的变暗与激发的紫外分数无关 光。 而是，变暗的强度取决于亮度，即在人眼V2的光谱光敏度上积分的强度。