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公开(公告)号：US6166276A
公开(公告)日：2000-12-26
申请号：US449621
申请日：1999-11-30
申请人： Fuyuhiko Sakyu , Naoto Takada , Hideaki Imura , Takeo Komata
发明人： Fuyuhiko Sakyu , Naoto Takada , Hideaki Imura , Takeo Komata
摘要： The invention relates to a method for producing 1,1,2,2,3,3,4-heptafluorocyclopentane. This method includes the step of reducing 1,1-dichlorooctafluorocyclopentane by hydrogen in the presence of a hydrogenation catalyst. This catalyst contains at least one first metal selected from metals of 8, 9, and 10 groups of periodic table, such as iron, cobalt, palladium, platinum, rhodium, ruthenium, iridium, and osmium. According to this method, it is possible to produce 1,1,2,2,3,3,4-heptafluorocyclopentane with high yield and high selectivity.
摘要翻译： 本发明涉及一种生产1,1,2,2,3,3,4-七氟环戊烷的方法。 该方法包括在氢化催化剂存在下用氢还原1,1-二氯八氟环戊烷的步骤。 该催化剂含有选自元素周期表8,9和10族金属中的至少一种金属，例如铁，钴，钯，铂，铑，钌，铱和锇。 根据该方法，可以高产率和高选择性制备1,1,2,2,3,3,4-七氟环戊烷。
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公开(公告)号：US06218586B1
公开(公告)日：2001-04-17
申请号：US09434277
申请日：1999-11-05
申请人： Naoto Takada , Masatomi Kanai , Hideaki Imura , Takeo Komata
发明人： Naoto Takada , Masatomi Kanai , Hideaki Imura , Takeo Komata
IPC分类号： C07C1708
CPC分类号： C07C23/08 , C07C17/04 , C07C17/206 , C07C17/21
摘要： The invention relates to a method for preparing a fluorinated product that is a first perhalogenated five-membered cyclic compound (e.g., 1,2-dichlorohexafluorocyclopentene and 1,1-dichlorooctafluorocyclopentane). This method includes reacting in a gas phase a starting material that is a second perhalogenated five-membered cyclic compound having at least one unsaturated bond, at substantially the same time with chlorine and hydrogen fluoride, in the presence of a fluorination catalyst containing an activated carbon optionally carrying thereon a metal compound, thereby to decrease the number of the at least one unsaturated bond and to increase the number of fluorine atoms of the second compound. The method is appropriate for the production of the first perhalogenated five-membered cyclic compound in an industrial scale.
摘要翻译： 本发明涉及一种制备作为第一全卤代五元环化合物（例如1,2-二氯六氟环戊烯和1,1-二氯八氟环戊烷）的氟化产物的方法。 该方法包括在气相中，在含有活性炭的氟化催化剂的存在下，将基本上同时具有至少一个不饱和键的第二全卤化五元环化合物的起始物质与氯和氟化氢反应 任选地带有金属化合物，从而减少至少一个不饱和键的数目并增加第二化合物的氟原子数。 该方法适用于以工业规模生产第一全卤代五元环化合物。
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公开(公告)号：US09012657B2
公开(公告)日：2015-04-21
申请号：US14009483
申请日：2012-06-18
申请人： Masamune Okamoto , Hideaki Imura , Naoto Takada
发明人： Masamune Okamoto , Hideaki Imura , Naoto Takada
IPC分类号： C07D231/10 , C07D231/28 , C07D231/14
CPC分类号： C07D231/28 , C07D231/14
摘要： A method for producing a pyrazole compound of the general formula (5) includes reacting a 2-acyl-3-aminoacrylic acid ester of the general formula (1) with a hydrazine of the general formula (4) in the presence of a base where R1, R2, R3 and R4 each independently represent an alkyl group wherein R5 represents an alkyl group or an aryl group wherein R1, R4 and R5 have the same meanings as above. It is possible by this production method to produce the 1,3-disubstituted pyrazol-4-carboxylic acid ester at a high yield and selectivity and with less discoloration.
摘要翻译： 制备通式（5）的吡唑化合物的方法包括在碱的存在下使通式（1）的2-酰基-3-氨基丙烯酸酯与通式（4）的肼反应， R 1，R 2，R 3和R 4各自独立地表示烷基，其中R 5表示烷基或芳基，其中R 1，R 4和R 5具有与上述相同的含义。 通过这种制备方法可以以高产率和选择性和较少的变色产生1,3-二取代的吡唑-4-羧酸酯。
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公开(公告)号：US08785689B2
公开(公告)日：2014-07-22
申请号：US14000754
申请日：2012-03-28
申请人： Naoto Takada , Masamune Okamoto , Hideaki Imura
发明人： Naoto Takada , Masamune Okamoto , Hideaki Imura
摘要： A method for purifying difluoroacetic acid chloride, including the step of bringing a difluoroacetic acid chloride composition that contains at least difluoroacetic acid fluoride into contact with calcium chloride at a temperature enabling reaction thereof thereby converting difluoroacetic acid fluoride into difluoroacetic acid chloride.
摘要翻译： 一种纯化二氟乙酰氯的方法，包括使含有至少二氟乙酸氟化物的二氟乙酰氯组合物与氯化钙接触的步骤，使其反应，从而将二氟乙酸氟化物转化为二氟乙酸氯化物。
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公开(公告)号：US08716526B2
公开(公告)日：2014-05-06
申请号：US13635577
申请日：2011-03-16
申请人： Masamune Okamoto , Hideaki Imura , Naoto Takada
发明人： Masamune Okamoto , Hideaki Imura , Naoto Takada
CPC分类号： C07C29/149 , C07C51/58 , C07C31/38 , C07C53/48
摘要： A production method of difluoroacetyl chloride according to the present invention includes a chlorination step of bringing a raw material containing at least either a 1-alkoxy-1,1,2,2-tetrafluoroethane or difluoroacetyl chloride into contact with calcium chloride at a reaction enabling temperature. A production method of 2,2-difluoroethyl alcohol according to the present invention includes a catalytic reduction step of causing catalytic reduction of the difluoroacetyl chloride obtained by the above production method. By these methods, the difluoroacetyl fluoride can be efficiently converted to the difluoroacetyl chloride and to the 2,2-difluoroethyl alcohol.
摘要翻译： 根据本发明的二氟乙酰氯的制备方法包括在反应使含有至少含有1-烷氧基-1,1,2,2-四氟乙烷或二氟乙酰氯的原料与氯化钙接触的氯化步骤 温度。 本发明的2,2-二氟乙醇的制造方法具有通过上述制造方法得到的二氟乙酰氯的催化还原工序。 通过这些方法，可以将二氟乙酰氟有效地转化为二氟乙酰氯和2,2-二氟乙醇。
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公开(公告)号：US20140107347A1
公开(公告)日：2014-04-17
申请号：US14009483
申请日：2012-06-18
申请人： Masamune Okamoto , Hideaki Imura , Naoto Takada
发明人： Masamune Okamoto , Hideaki Imura , Naoto Takada
IPC分类号： C07D231/28
CPC分类号： C07D231/28 , C07D231/14
摘要： A method for producing a pyrazole compound of the general formula (5) includes reacting a 2-acyl-3-aminoacrylic acid ester of the general formula (1) with a hydrazine of the general formula (4) in the presence of a base where R1, R2, R3 and R4 each independently represent an alkyl group wherein R5 represents an alkyl group or an aryl group wherein R1, R4 and R5 have the same meanings as above. It is possible by this production method to produce the 1,3-disubstituted pyrazol-4-carboxylic acid ester at a high yield and selectivity and with less discoloration.
摘要翻译： 制备通式（5）的吡唑化合物的方法包括在碱的存在下使通式（1）的2-酰基-3-氨基丙烯酸酯与通式（4）的肼反应， R 1，R 2，R 3和R 4各自独立地表示烷基，其中R 5表示烷基或芳基，其中R 1，R 4和R 5具有与上述相同的含义。 通过这种制备方法可以以高产率和选择性和较少的变色产生1,3-二取代的吡唑-4-羧酸酯。
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公开(公告)号：US20140031588A1
公开(公告)日：2014-01-30
申请号：US14000754
申请日：2012-03-28
申请人： Naoto Takada , Masamune Okamoto , Hideaki Imura
发明人： Naoto Takada , Masamune Okamoto , Hideaki Imura
IPC分类号： C07C51/64
摘要： A method for purifying difluoroacetic acid chloride, including the step of bringing a difluoroacetic acid chloride composition that contains at least difluoroacetic acid fluoride into contact with calcium chloride at a temperature enabling reaction thereof thereby converting difluoroacetic acid fluoride into difluoroacetic acid chloride.
摘要翻译： 一种纯化二氟乙酰氯的方法，包括使含有至少二氟乙酸氟化物的二氟乙酰氯组合物与氯化钙接触的步骤，使其反应，从而将二氟乙酸氟化物转化为二氟乙酸氯化物。
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公开(公告)号：US20130012740A1
公开(公告)日：2013-01-10
申请号：US13635577
申请日：2011-03-16
申请人： Masamune Okamoto , Hideaki Imura , Naoto Takada
发明人： Masamune Okamoto , Hideaki Imura , Naoto Takada
IPC分类号： C07C29/147 , C07C51/58
CPC分类号： C07C29/149 , C07C51/58 , C07C31/38 , C07C53/48
摘要： A production method of difluoroacetyl chloride according to the present invention includes a chlorination step of bringing a raw material containing at least either a 1-alkoxy-1,1,2,2-tetrafluoroethane or difluoroacetyl chloride into contact with calcium chloride at a reaction enabling temperature. A production method of 2,2-difluoroethyl alcohol according to the present invention includes a catalytic reduction step of causing catalytic reduction of the difluoroacetyl chloride obtained by the above production method. By these methods, the difluoroacetyl fluoride can be efficiently converted to the difluoroacetyl chloride and to the 2,2-difluoroethyl alcohol.
摘要翻译： 根据本发明的二氟乙酰氯的制备方法包括在反应使含有至少含有1-烷氧基-1,1,2,2-四氟乙烷或二氟乙酰氯的原料与氯化钙接触的氯化步骤 温度。 本发明的2,2-二氟乙醇的制造方法具有通过上述制造方法得到的二氟乙酰氯的催化还原工序。 通过这些方法，可以将二氟乙酰氟有效地转化为二氟乙酰氯和2,2-二氟乙醇。
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公开(公告)号：US20070008845A1
公开(公告)日：2007-01-11
申请号：US11482126
申请日：2006-07-07
申请人： Naoto Takada
发明人： Naoto Takada
IPC分类号： G11B5/09
CPC分类号： G11B20/00086 , G11B19/122 , G11B20/00144 , G11B20/00152
摘要： An optical disk apparatus is provided with a recording/reading unit that records data and reads recorded data with respect to an optical disk. Further, the optical disk apparatus is provided with a control unit that judges whether an account name recorded on the optical disk matches an account name selected by the operation unit. The control unit permits the recording/reading unit to record data to the optical disk if the account names match. And the control unit prohibits the recording/reading unit from recording data to the optical disk if it is judged that the account names do not match.
摘要翻译： 光盘装置具有记录数据并读取相对于光盘的记录数据的记录/读取单元。 此外，光盘装置设置有控制单元，其判断记录在光盘上的帐户名称是否与由操作单元选择的帐户名称相匹配。 如果帐户名称匹配，则控制单元允许记录/读取单元将数据记录到光盘。 并且如果判断出该帐户名称不匹配，则控制单元禁止记录/读取单元向光盘记录数据。
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公开(公告)号：US20050254369A1
公开(公告)日：2005-11-17
申请号：US11121946
申请日：2005-05-05
申请人： Naoto Takada
发明人： Naoto Takada
IPC分类号： G11B20/10 , G11B5/09 , G11B7/005 , G11B7/007 , G11B7/28 , G11B19/12 , G11B27/00 , G11B27/10 , G11B27/34
CPC分类号： G11B19/122 , G11B7/0079 , G11B7/28 , G11B20/10 , G11B27/105 , G11B27/34 , G11B2220/211 , G11B2220/2545
摘要： A disc reproducing apparatus is constructed so that an identification code of an optical disc is read out and contents of the optical disc are selected and the contents reproduced by a reproduction program of the optical disc are selected and a reproduction mode of the contents reproduced by the reproduction program of the optical disc is selected and the contents of the optical disc and the reproduction program for reproducing the optical disc together with the identification code of the optical disc are stored and the reproduction program of the optical disc set is executed and the optical disc is reproduced.
摘要翻译： 光盘重放装置被构造成读出光盘的识别码，并且选择光盘的内容，并且选择由光盘的再现程序再现的内容，并且再现由 选择光盘的再现程序，并且存储光盘的内容和用于再现光盘的再现程序以及光盘的识别码，并且执行光盘组的再现程序，并且光盘 被转载。
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