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公开(公告)号：US20110021797A1
公开(公告)日：2011-01-27
申请号：US12933741
申请日：2009-03-26
申请人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
发明人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
IPC分类号： C07F7/02
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要： A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译： 制备官能化颗粒的方法包括提供包含颗粒的原料，与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器，由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号：US08394977B2
公开(公告)日：2013-03-12
申请号：US12933741
申请日：2009-03-26
申请人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
发明人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
IPC分类号： C07F7/00
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要： A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译： 制备官能化颗粒的方法包括提供包含颗粒的原料，与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器，由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号：US08487019B2
公开(公告)日：2013-07-16
申请号：US12933526
申请日：2009-03-26
申请人： James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人： James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号： C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要： A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译： 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒。
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公开(公告)号：US20110028605A1
公开(公告)日：2011-02-03
申请号：US12933526
申请日：2009-03-26
申请人： James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人： James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号： C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要： A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译： 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒。
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公开(公告)号：US08249409B2
公开(公告)日：2012-08-21
申请号：US13096000
申请日：2011-04-28
申请人： Jun-Ying Zhang , Jimmie R. Baran, Jr. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
发明人： Jun-Ying Zhang , Jimmie R. Baran, Jr. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
CPC分类号： H01L51/5268 , B82Y20/00 , B82Y30/00 , G02B6/0035 , G02F1/133603 , H01L51/5275 , H01L2251/5369
摘要： A multifunctional optical film for enhancing light extraction includes a flexible substrate, a structured layer having nanoparticles of different sizes, and a backfill layer. The structured layer effectively uses microreplicated diffractive or scattering nanostructures located near enough to the light generation region to enable extraction of an evanescent wave from an organic light emitting diode (OLED) device. The backfill layer has a material having an index of refraction different from the index of refraction of the structured layer. The backfill layer also provides a planarizing layer over the structured layer in order to conform the light extraction film to a layer of an OLED display device. The film may have additional layers added to or incorporated within it to an emissive surface in order to effect additional functionalities beyond improvement of light extraction efficiency.
摘要翻译： 用于增强光提取的多功能光学膜包括柔性基板，具有不同尺寸的纳米颗粒的结构化层和回填层。 结构化层有效地使用位于光发生区附近的微复制衍射或散射纳米结构，以便能够从有机发光二极管（OLED）器件中提取ev逝波。 回填层具有折射率不同于结构化层的折射率的材料。 回填层还在结构化层上提供平坦化层，以使光提取膜符合OLED显示器件的层。 为了实现除了光提取效率的提高以外的附加功能，该膜可以具有向发射表面添加或并入其中的附加层。
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公开(公告)号：US07957621B2
公开(公告)日：2011-06-07
申请号：US12336889
申请日：2008-12-17
申请人： Jun-Ying Zhang , Jimmie R. Baran, Jr. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
发明人： Jun-Ying Zhang , Jimmie R. Baran, Jr. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
CPC分类号： H01L51/5268 , B82Y20/00 , B82Y30/00 , G02B6/0035 , G02F1/133603 , H01L51/5275 , H01L2251/5369
摘要： A multifunctional optical film for enhancing light extraction includes a flexible substrate, a structured layer having nanoparticles of different sizes, and a backfill layer. The structured layer effectively uses microreplicated diffractive or scattering nanostructures located near enough to the light generation region to enable extraction of an evanescent wave from an organic light emitting diode (OLED) device. The backfill layer has a material having an index of refraction different from the index of refraction of the structured layer. The backfill layer also provides a planarizing layer over the structured layer in order to conform the light extraction film to a layer of an OLED display device. The film may have additional layers added to or incorporated within it to an emissive surface in order to effect additional functionalities beyond improvement of light extraction efficiency.
摘要翻译： 用于增强光提取的多功能光学膜包括柔性基板，具有不同尺寸的纳米颗粒的结构化层和回填层。 结构化层有效地使用位于光发生区附近的微复制衍射或散射纳米结构，以便能够从有机发光二极管（OLED）器件中提取ev逝波。 回填层具有折射率不同于结构化层的折射率的材料。 回填层还在结构化层上提供平坦化层，以使光提取膜符合OLED显示器件的层。 为了实现除了光提取效率的提高以外的附加功能，该膜可以具有向发射表面添加或并入其中的附加层。
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公开(公告)号：US20110200293A1
公开(公告)日：2011-08-18
申请号：US13096000
申请日：2011-04-28
申请人： Jun-Ying Zhang , Jimmie R. Baran, JR. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
发明人： Jun-Ying Zhang , Jimmie R. Baran, JR. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey A. Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
IPC分类号： G02B6/10
CPC分类号： H01L51/5268 , B82Y20/00 , B82Y30/00 , G02B6/0035 , G02F1/133603 , H01L51/5275 , H01L2251/5369
摘要： A multifunctional optical film for enhancing light extraction includes a flexible substrate, a structured layer having nanoparticles of different sizes, and a backfill layer. The structured layer effectively uses microreplicated diffractive or scattering nanostructures located near enough to the light generation region to enable extraction of an evanescent wave from an organic light emitting diode (OLED) device. The backfill layer has a material having an index of refraction different from the index of refraction of the structured layer. The backfill layer also provides a planarizing layer over the structured layer in order to conform the light extraction film to a layer of an OLED display device. The film may have additional layers added to or incorporated within it to an emissive surface in order to effect additional functionalities beyond improvement of light extraction efficiency.
摘要翻译： 用于增强光提取的多功能光学膜包括柔性基板，具有不同尺寸的纳米颗粒的结构化层和回填层。 结构化层有效地使用位于光发生区附近的微复制衍射或散射纳米结构，以便能够从有机发光二极管（OLED）器件中提取ev逝波。 回填层具有折射率不同于结构化层的折射率的材料。 回填层还在结构化层上提供平坦化层，以使光提取膜符合OLED显示器件的层。 为了实现除了光提取效率的提高以外的附加功能，该膜可以具有向发射表面添加或并入其中的附加层。
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公开(公告)号：US20100150513A1
公开(公告)日：2010-06-17
申请号：US12336889
申请日：2008-12-17
申请人： Jun-Ying Zhang , Jimmie R. Baran, JR. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
发明人： Jun-Ying Zhang , Jimmie R. Baran, JR. , Terry L. Smith , William J. Schultz , William Blake Kolb , Cheryl A. Patnaude , Sergey Lamansky , Brian K. Nelson , Naiyong Jing , Brant U. Kolb
CPC分类号： H01L51/5268 , B82Y20/00 , B82Y30/00 , G02B6/0035 , G02F1/133603 , H01L51/5275 , H01L2251/5369
摘要： A multifunctional optical film for enhancing light extraction includes a flexible substrate, a structured layer having nanoparticles of different sizes, and a backfill layer. The structured layer effectively uses microreplicated diffractive or scattering nanostructures located near enough to the light generation region to enable extraction of an evanescent wave from an organic light emitting diode (OLED) device. The backfill layer has a material having an index of refraction different from the index of refraction of the structured layer. The backfill layer also provides a planarizing layer over the structured layer in order to conform the light extraction film to a layer of an OLED display device. The film may have additional layers added to or incorporated within it to an emissive surface in order to effect additional functionalities beyond improvement of light extraction efficiency.
摘要翻译： 用于增强光提取的多功能光学膜包括柔性基板，具有不同尺寸的纳米颗粒的结构化层和回填层。 结构化层有效地使用位于光发生区附近的微复制衍射或散射纳米结构，以便能够从有机发光二极管（OLED）器件中提取ev逝波。 回填层具有折射率不同于结构化层的折射率的材料。 回填层还在结构化层上提供平坦化层，以使光提取膜符合OLED显示器件的层。 为了实现除了光提取效率的提高以外的附加功能，该膜可以具有向发射表面添加或并入其中的附加层。
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公开(公告)号：US06586483B2
公开(公告)日：2003-07-01
申请号：US09756422
申请日：2001-01-08
申请人： Brant U. Kolb , Jimmie R. Baran, Jr. , Michael A. Johnson , Gordon G. Johnson , Megan P. Lehmann , John S. Sokalski
发明人： Brant U. Kolb , Jimmie R. Baran, Jr. , Michael A. Johnson , Gordon G. Johnson , Megan P. Lehmann , John S. Sokalski
IPC分类号： C08J900
CPC分类号： C08J9/0066 , C08J9/12 , C08J2207/02 , C09J7/38 , C09J11/04 , C09J2433/00
摘要： A foam composition that includes a vehicle and surface-modified nanoparticles disposed in the vehicle. The individual nanoparticles having a particle diameter of less than about 100 nanometers.
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公开(公告)号：US09102690B2
公开(公告)日：2015-08-11
申请号：US12810041
申请日：2008-12-17
CPC分类号： C07F5/069 , Y10T428/2991
摘要： Acicular boehmite nanoparticles, methods of making acicular boehmite nanoparticles, and composite materials that contain acicular boehmite nanoparticles are described. The acicular boehmite nanoparticles are prepared in a continuous hydrothermal reactor from a feedstock solution containing a soluble aluminum-containing precursor.
摘要翻译： 针状勃姆石纳米粒子，制备针状勃姆石纳米粒子的方法，以及包含针状勃姆石纳米粒子的复合材料。 针状勃姆石纳米颗粒在含有可溶性含铝前体的原料溶液的连续水热反应器中制备。
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