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公开(公告)号:US20110028605A1
公开(公告)日:2011-02-03
申请号:US12933526
申请日:2009-03-26
申请人: James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人: James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号: C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要: A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译: 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂,使得官能化颗粒占填充树脂的至少约20重量%。 提供官能化颗粒的步骤还可以包括提供(i)未处理颗粒的原料,(ii)与颗粒反应的表面处理剂,和(iii)溶剂,并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面,成品树脂包含至少约20重量%的有机基质中的官能化颗粒。
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公开(公告)号:US08487019B2
公开(公告)日:2013-07-16
申请号:US12933526
申请日:2009-03-26
申请人: James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人: James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号: C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要: A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译: 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂,使得官能化颗粒占填充树脂的至少约20重量%。 提供官能化颗粒的步骤还可以包括提供(i)未处理颗粒的原料,(ii)与颗粒反应的表面处理剂,和(iii)溶剂,并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面,成品树脂包含至少约20重量%的有机基质中的官能化颗粒。
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公开(公告)号:US20110021797A1
公开(公告)日:2011-01-27
申请号:US12933741
申请日:2009-03-26
申请人: Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
发明人: Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
IPC分类号: C07F7/02
CPC分类号: C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要: A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译: 制备官能化颗粒的方法包括提供包含颗粒的原料,与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器,由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号:US08394977B2
公开(公告)日:2013-03-12
申请号:US12933741
申请日:2009-03-26
申请人: Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
发明人: Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
IPC分类号: C07F7/00
CPC分类号: C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要: A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译: 制备官能化颗粒的方法包括提供包含颗粒的原料,与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器,由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号:US20110245376A1
公开(公告)日:2011-10-06
申请号:US13133878
申请日:2009-12-17
申请人: William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
发明人: William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
CPC分类号: C08L63/00
摘要: Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin, and to coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译: 描述了包含分散在可固化树脂中的表面改性纳米碳酸钙颗粒的组合物,以及包含这种组合物的涂料和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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公开(公告)号:US09221970B2
公开(公告)日:2015-12-29
申请号:US13133878
申请日:2009-12-17
申请人: William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
发明人: William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
IPC分类号: C08L63/00
CPC分类号: C08L63/00
摘要: Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin, and to coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译: 描述了包含分散在可固化树脂中的表面改性纳米碳酸钙颗粒的组合物,以及包含这种组合物的涂料和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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公开(公告)号:US07482201B2
公开(公告)日:2009-01-27
申请号:US11972904
申请日:2008-01-11
申请人: Scott B. Charles , Kathleen M. Gross , Steven C. Hackett , Michael A. Kropp , William J. Schultz , Wendy L. Thompson
发明人: Scott B. Charles , Kathleen M. Gross , Steven C. Hackett , Michael A. Kropp , William J. Schultz , Wendy L. Thompson
CPC分类号: H01L23/295 , H01L21/563 , H01L23/293 , H01L24/29 , H01L2224/16 , H01L2224/2929 , H01L2224/29386 , H01L2224/73203 , H01L2224/73204 , H01L2924/01004 , H01L2924/01012 , H01L2924/01019 , H01L2924/0102 , H01L2924/01021 , H01L2924/01029 , H01L2924/01046 , H01L2924/01057 , H01L2924/01063 , H01L2924/01066 , H01L2924/01067 , H01L2924/01068 , H01L2924/01077 , H01L2924/01078 , H01L2924/01079 , H01L2924/01087 , H01L2924/01322 , H01L2924/10253 , H01L2924/14 , H05K3/305 , H01L2924/00 , H01L2924/0665 , H01L2924/05442
摘要: The invention provides electronic articles and methods of making said articles. The electronic articles comprise an electronic component bonded and electrically connected to a substrate using an underfill adhesive comprising the reaction product of a thermosetting resin, curing catalyst, and surface-treated nanoparticles that are substantially spherical, non-agglomerated, amorphous, and solid.
摘要翻译: 本发明提供了制造所述制品的电子制品和方法。 电子制品包括使用包含热固性树脂,固化催化剂和基本上球形,非聚集,无定形和固体的表面处理纳米颗粒的反应产物的底部填充粘合剂粘合并电连接到基底的电子部件。
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公开(公告)号:US07327039B2
公开(公告)日:2008-02-05
申请号:US10441879
申请日:2003-05-20
申请人: Scott B. Charles , Kathleen M. Gross , Steven C. Hackett , Michael A. Kropp , William J. Schultz , Wendy L. Thompson
发明人: Scott B. Charles , Kathleen M. Gross , Steven C. Hackett , Michael A. Kropp , William J. Schultz , Wendy L. Thompson
CPC分类号: H01L23/295 , H01L21/563 , H01L23/293 , H01L24/29 , H01L2224/16 , H01L2224/2929 , H01L2224/29386 , H01L2224/73203 , H01L2224/73204 , H01L2924/01004 , H01L2924/01012 , H01L2924/01019 , H01L2924/0102 , H01L2924/01021 , H01L2924/01029 , H01L2924/01046 , H01L2924/01057 , H01L2924/01063 , H01L2924/01066 , H01L2924/01067 , H01L2924/01068 , H01L2924/01077 , H01L2924/01078 , H01L2924/01079 , H01L2924/01087 , H01L2924/01322 , H01L2924/10253 , H01L2924/14 , H05K3/305 , H01L2924/00 , H01L2924/0665 , H01L2924/05442
摘要: The invention provides electronic articles and methods of making said articles. The electronic articles comprise an electronic component bonded and electrically connected to a substrate using an underfill adhesive comprising the reaction product of a thermosetting resin, curing catalyst, and surface-treated nanoparticles that are substantially spherical, non-agglomerated, amorphous, and solid.
摘要翻译: 本发明提供了制造所述制品的电子制品和方法。 电子制品包括使用包含热固性树脂,固化催化剂和基本上球形,非聚集,无定形和固体的表面处理纳米颗粒的反应产物的底部填充粘合剂粘合并电连接到基底的电子部件。
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公开(公告)号:US06572693B1
公开(公告)日:2003-06-03
申请号:US09698986
申请日:2000-10-27
申请人: Dong Wu , Brian N. Holmes , Brant U. Kolb , Sumita B. Mitra , Wendy L. Thompson
发明人: Dong Wu , Brian N. Holmes , Brant U. Kolb , Sumita B. Mitra , Wendy L. Thompson
IPC分类号: A61K700
CPC分类号: B82Y30/00 , A61K6/0017 , A61K6/0023 , A61K6/007 , A61K6/083 , A61K6/087 , B01J13/0008 , C01G25/02 , C01P2004/62 , C01P2004/64 , C08K3/22 , C08K2003/2244 , C08K2201/011 , C08K2201/014 , C08L33/00 , C08L63/00
摘要: The invention provides for a material comprising(a) a hardenable resin; and (b) a filler comprising (i) clusters of nano-sized particles, the clusters comprising non-beavy metal oxide particles and heavy metal oxides, and being not fully densified particles and (ii) non-agglomerated nano-sized particles selected from the group consisting of non-heavy metal oxide particles, heavy metal oxide particles, and combinations thereof. The material is suitable for use as dental materials.
摘要翻译: 本发明提供了包含(a)可硬化树脂的材料; 和(b)填料,其包含(i)纳米尺寸颗粒簇,所述簇包含非金属氧化物颗粒和重金属氧化物,并且不是完全致密化的颗粒,和(ii)非聚集的纳米尺寸颗粒, 由非重金属氧化物颗粒,重金属氧化物颗粒及其组合组成的组。 该材料适用于牙科材料。
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10.
公开(公告)号:US20090306277A1
公开(公告)日:2009-12-10
申请号:US12438966
申请日:2007-08-29
申请人: Emily S. Goenner , Howard S. Creel , Andrew M. Hine , Brant U. Kolb , Gene B. Portelli , Wendy L. Thompson
发明人: Emily S. Goenner , Howard S. Creel , Andrew M. Hine , Brant U. Kolb , Gene B. Portelli , Wendy L. Thompson
CPC分类号: C09D167/06 , C08K3/36 , C08K9/06 , C09D7/62 , C09D7/67 , C09D7/68 , C08L2666/54
摘要: Resin systems comprising a crosslinkable resin, a reactive diluent, and a plurality of reactive, surface-modified nanoparticles; and gel coats including such resin systems are described. Articles having such compositions attached to a surface of a substrate, e.g., a fibrous reinforced substrate, are also described.
摘要翻译: 包括可交联树脂,反应性稀释剂和多种反应性表面改性纳米颗粒的树脂体系; 并描述包括这种树脂体系的凝胶涂层。 还描述了具有附着到基底表面,例如纤维增强基底上的这种组合物的制品。
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