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    Crystalline lactitol monohydrate and a process for the preparation thereof, use thereof, and sweetening agent
    1.
    发明授权
    Crystalline lactitol monohydrate and a process for the preparation thereof, use thereof, and sweetening agent 失效
    结晶乳糖醇一水合物及其制备方法，其用途和甜味剂

    公开(公告)号：US5516763A

    公开(公告)日：1996-05-14

    申请号：US995856

    申请日：1992-12-23

    申请人： Heikki O. Heikkila ,  Juha V. Nurmi

    发明人： Heikki O. Heikkila ,  Juha V. Nurmi

    IPC分类号： A23G3/00 ,  A23G3/34 ,  A23G3/38 ,  A23G9/52 ,  A23L27/30 ,  A61K8/60 ,  A61K31/715 ,  A61Q11/00 ,  C07H1/00 ,  C07H15/04 ,  A23L1/00

    CPC分类号： A23G3/38 ,  A23G3/346 ,  A23G9/52 ,  A23L27/34 ,  A61K8/60 ,  A61Q11/00 ,  C07H15/04 ,  A23G2200/06

    摘要： A crystalline lactitol monohydrate having lattice cell constants a =7.815.+-.0.008 .ANG., b=12.682.+-.0.008 .ANG., and c=15.927.+-.0.008 .ANG., and a melting range between 90.degree. and 105.degree. C., and a water content between 4.85 and 5.15%, as well as a process of preparing said crystalline lactitol monohydrate by evaporating the aqueous solution of lactitol to a concentration between 75 and 88% by weight, cooling the resultant mixture at a temperature ranging between 30 and 75.degree. C., subsequently separating the lactitol monohydrate crystals from the mother liquor, and subsequently drying with air having a temperature between 120.degree. C., and a relative humidity between 0 and 40%, for a time period less than 24 hours. The invention also relates to the use of said crystalline lactitol monohydrate as a bulk sweetener for the total or partial replacement of sucrose, in dietetic products, confectionery, bakery products, cereals, desserts, jams, beverages, chocolate, chewing gum and ice-cream, and in pharmaceuticals and cosmetic products, such as tooth paste, as well as a special sweetening agent resembling sucrose, mainly composed of said crystalline lactitol monohydrate.

    摘要翻译： 具有晶格单元常数a = 7.815 +/- 0.008 ANGSTROM，b = 12.682 +/- 0.008 ANGSTROM和c = 15.927 +/- 0.008的晶体乳糖醇一水合物，熔点范围为90-105℃，和 水含量在4.85至5.15％之间，以及通过将乳糖醇水溶液蒸发至75至88重量％的浓度来制备所述结晶乳糖醇一水合物的方法，在30至75℃的温度范围内冷却所得混合物 随后将乳糖醇一水合物晶体与母液分离，随后用温度在120℃和相对湿度在0至40％之间的空气干燥少于24小时的时间。 本发明还涉及所述结晶乳糖醇一水合物作为增量甜味剂用于在饮食产品，糖果，面包店产品，谷物，甜点，果酱，饮料，巧克力，口香糖和冰淇淋中的总或部分替代蔗糖 ，以及主要由所述结晶乳糖醇一水合物组成的药物和化妆品，例如牙膏，以及类似于蔗糖的特殊甜味剂。

    Process of recovering lactose from whey
    3.
    发明授权
    Process of recovering lactose from whey 失效
    从乳清中回收乳糖的方法

    公开(公告)号：US4955363A

    公开(公告)日：1990-09-11

    申请号：US256600

    申请日：1988-10-12

    申请人： Matti E. Harju ,  Heikki O. Heikkila

    发明人： Matti E. Harju ,  Heikki O. Heikkila

    IPC分类号： A23C9/146 ,  C13K5/00

    CPC分类号： C13K5/00 ,  A23C9/1465

    摘要： A method of recovering lactose from milk whey or cheese whey with a high yield, wherein the whey is concentrated, part of the lactose is crystallized, and the crystals are separated and dried; the mother liquor is purified by heating it to about 60.degree. to 70.degree. C. at a pH of about 5.8 to 7.0 and by removing the resultant precipitate by centrifugation; the purified mother liquor is fractionated chromatographically, using sulphonated polystyrene resin which is in sodium ion form and cross-linked by a 3-6% per weight divinylbenzene and which is even-grained, the flow rate is about 0.4 to 1.5 m.sup.3 /h, the temperature about 50.degree. to 75.degree. C., and the pH about 5.5 to 7; whereafter elution is carried out with water, and the following fractions are recovered: a protein fraction which may also contain salts, an intermediate fraction which is recirculated to the fractionating step, and a lactose fraction which is passed to the crystallization step.

    Betaine recovery process
    4.
    发明授权
    Betaine recovery process 失效
    甜菜碱恢复过程

    公开(公告)号：US4359430A

    公开(公告)日：1982-11-16

    申请号：US237649

    申请日：1981-02-24

    申请人： Heikki O. Heikkila ,  Jaakko A. Melaja ,  Dan E. D. Millner ,  Jouko J. Virtanen

    发明人： Heikki O. Heikkila ,  Jaakko A. Melaja ,  Dan E. D. Millner ,  Jouko J. Virtanen

    IPC分类号： B01J39/26 ,  C13B20/14 ,  C07C101/12

    CPC分类号： C13B20/148 ,  B01J39/26

    摘要： Betaine is recovered from natural sources such as beet molasses, rest molasses and vinasse by diluting the molasses to 25-50% solids, introducing the molasses to the top of a chromatographic column containing a salt of a polystyrene sulfonate cation exchange resin cross-coupled with from about 2 to about 12 weight percent of divinylbenzene, eluting with water and collecting a fraction of betaine from the downstream side of the resin. When successive feeds with predetermined intervals are made, the feeds may be partly overlapped. The betaine from the preceding feed is then eluted by the dilute molasses from the following feed. The betaine fraction is evaporated under vacuum and the betaine crystallized as anhydrous crystals or as betaine monohydrate.

    摘要翻译： 甜菜碱通过将糖蜜稀释至25-50％固体从天然来源例如甜菜糖蜜，休息糖蜜和葡萄酒中回收，将糖蜜引入到含有交联偶联的聚苯乙烯磺酸盐阳离子交换树脂的盐的色谱柱的顶部 约2至约12重量％的二乙烯基苯，用水洗脱并从树脂的下游侧收集一部分甜菜碱。 当进行具有预定间隔的连续进料时，进料可以部分重叠。 然后将来自前述进料的甜菜碱用稀释的糖浆从下列进料中洗脱出来。 在真空下蒸发甜菜碱级分，甜菜碱以无水晶体或一水合甜菜碱结晶。