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公开(公告)号：US4229365A
公开(公告)日：1980-10-21
申请号：US907912
申请日：1978-05-22
IPC分类号： C07B61/00 , B01J23/00 , C07C67/00 , C07C201/00 , C07C201/12 , C07C205/12 , C07C253/00 , C07C255/50 , C07C121/52 , C07C79/12
CPC分类号： C07C201/12
摘要： Fluorobenzenes are manufactured by reacting substituted chlorobenzenes with potassium fluoride in the presence of catalytic amounts of cesium fluoride and in the presence of certain solvents; m-nitrofluorobenzenes and m-cyanofluorobenzenes can also be manufactured in the absence of cesium fluoride. The products are starting materials for the manufacture of dyes, pharmaceuticals and pesticides.
摘要翻译： 在催化量的氟化铯和某些溶剂的存在下，使取代的氯苯与氟化钾反应制备氟苯; 间硝基氟苯和间 - 氰基氟苯也可以在不存在氟化铯的情况下制造。 该产品是用于制造染料，药物和农药的起始原料。
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公开(公告)号：US4226811A
公开(公告)日：1980-10-07
申请号：US2596
申请日：1979-01-11
IPC分类号： B01J31/00 , C07C67/00 , C07C201/00 , C07C201/12 , C07C205/12 , C07C253/00 , C07C255/50 , C07C79/12
CPC分类号： C07C201/12
摘要： A process for the preparation of substituted fluorobenzenes which contain a nitro group or a cyano group and may or may not contain an aliphatic radical or an additional halogen atom, wherein the corresponding substituted chlorobenzene is reacted with potassium fluoride in the presence of a crown ether and a solvent at from 150.degree. to 230.degree. C.
摘要翻译： 制备含有硝基或氰基的取代氟苯并且可以含有或不含脂肪族基团或另外的卤素原子的方法，其中相应的取代氯苯与氟醚在冠醚存在下反应， 150〜230℃的溶剂
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3.发明授权Preparation of mixtures of 1-monohalogenated isocyanates and 1,2-unsaturated isocyanates 失效1-卤代异氰酸酯和1,2-不饱和异氰酸酯的混合物的制备
公开(公告)号：US4314948A
公开(公告)日：1982-02-09
申请号：US175592
申请日：1980-08-05
IPC分类号： C07C265/06 , A01N47/40 , C07C20060101 , C07C67/00 , C07C241/00 , C07C263/04 , C07C265/04 , C07C118/00 , C07C119/042 , C07C119/045 , C07C119/048
CPC分类号： C07C263/16
摘要： 1-Monohalogenated isocyanates, and a process for the preparation of mixtures of 1-monohalogenated isocyanates and 1,2-unsaturated isocyanates by reacting 1-monohalogenated carbamic acid halides or isocyanates with a halogen-free isocyanate or diisocyanate or by reacting 1,2-unsaturated isocyanates with a carbamic acid halide or a bis-carbamic acid halide.The 1,2-unsaturated isocyanates and 1-monohalogenated isocyanates prepared according to the invention are valuable starting materials for the preparation of pest control agents, dyes, drugs, water-repellent textile finishes, detergents, plastics, bleaches and adhesives.
摘要翻译： 1-单卤代异氰酸酯，以及1-卤代异氰酸酯和1,2-不饱和异氰酸酯的混合物的制备方法，通过使1-单卤代氨基甲酸卤化物或异氰酸酯与无卤素的异氰酸酯或二异氰酸酯反应， 不饱和异氰酸酯与氨基甲酸卤化物或双 - 氨基甲酸卤化物。 根据本发明制备的1,2-不饱和异氰酸酯和1-单卤素异氰酸酯是制备害虫控制剂，染料，药物，拒水织物整理剂，洗涤剂，塑料，漂白剂和粘合剂的有价值的起始材料。
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公开(公告)号：US4294773A
公开(公告)日：1981-10-13
申请号：US175591
申请日：1980-08-05
IPC分类号： C07C265/06 , C07C17/08 , C07C23/28 , C07C67/00 , C07C241/00 , C07C263/04 , C07C263/12 , C07C265/04 , C07C118/00 , C07C119/042
CPC分类号： C07C263/04
摘要： 1-Haloalkyl isocyanates and 1-alkenyl isocyanates are prepared by reacting 1-haloalkylcarbamic acid halides or 1-haloalkyl isocyanates with .alpha.-pinene.The 1-alkenyl isocyanates and 1-haloalkyl isocyanates obtained according to the invention are valuable starting materials for the preparation of pest control agents, dyes, drugs, water-repellent textile finishes, detergents, plastics, bleaches and adhesives.
摘要翻译： 1-卤代烷基异氰酸酯和1-烯基异氰酸酯通过1-卤代烷基氨基甲酸卤化物或1-卤代烷基异氰酸酯与α-蒎烯反应制备。 根据本发明获得的1-烯基异氰酸酯和1-卤代烷基异氰酸酯是制备害虫控制剂，染料，药物，拒水织物整理剂，洗涤剂，塑料，漂白剂和粘合剂的有价值的起始材料。
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公开(公告)号：US4257974A
公开(公告)日：1981-03-24
申请号：US85962
申请日：1979-10-18
IPC分类号： C07C265/02 , A01M20060101 , A61K20060101 , C07C20060101 , C07C67/00 , C07C241/00 , C07C263/16 , C07C265/04 , C09B20060101 , C07C119/042 , C07C119/045 , C07C119/048
CPC分类号： C07C263/16 , C07C2101/14
摘要： .alpha.,.beta.-Dihaloalkyl isocyanates and a process for the preparation of such compounds by reacting .alpha.,.beta.-unsaturated alkyl isocyanates with halogen in the presence of an organic solvent which is inert under the reaction conditions, at from -35.degree. to +90.degree. C. The .alpha.,.beta.-dihaloalkyl isocyanates thus obtainable correspond to the formula ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are identical or different and each is hydrogen, a saturated aliphatic radical of 1 to 10 carbon atoms, a cycloaliphatic radical of 3 to 12 carbon atoms, an araliphatic radical of 7 to 11 carbon atoms or an aromatic radical of 6 to 10 carbon atoms, or R.sup.1 and R.sup.2 together with the carbon atom on which they are present as substituents are cycloalkyl of 3 to 7 ring members, and X is halogen. The compounds are valuable intermediates for the preparation of dyes, surface-coating intermediates, crop protection agents and drugs.
摘要翻译： α，β-二卤代烷基异氰酸酯和通过使α，β-不饱和烷基异氰酸酯与卤素在有效溶剂存在下反应来制备这些化合物的方法，所述有机溶剂在-35℃至+ 90℃的反应条件下是惰性的 C.由此获得的α，β-二卤代烷基异氰酸酯对应于式Ia，其中R 1，R 2和R 3相同或不同，各自为氢，1至10个碳原子的饱和脂族基团，3个脂环族基团 碳原子数为7〜11的芳脂族基团或6〜10个碳原子的芳香族基团，或者R1，R2与它们作为取代基存在的碳原子一起形成3〜7个环成员的环烷基， X为卤素。 这些化合物是制备染料，表面涂层中间体，作物保护剂和药物的有价值的中间体。
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公开(公告)号：US3992444A
公开(公告)日：1976-11-16
申请号：US506604
申请日：1974-09-16
IPC分类号： C07D271/06 , C07D271/07 , C07C143/72
CPC分类号： C07D271/07
摘要： The production of sulfamic acid halides by reaction of sulfamic acids with acid halides, and the new sulfamic acid halides. The products are starting materials for the production of plant protection agents, dyes and pharmaceuticals.
摘要翻译： 通过氨基磺酸与酰卤的反应和新的氨基磺酸卤化物生产氨基磺酰卤。 该产品是用于生产植物保护剂，染料和药物的起始材料。
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公开(公告)号：US4095034A
公开(公告)日：1978-06-13
申请号：US675580
申请日：1976-04-09
IPC分类号： C07C271/08 , C07C20060101 , C07C67/00 , C07C239/00 , C07C125/06
CPC分类号： C07C271/06
摘要： Process for the manufacture of N-alkyl and N-alkenyl carbamates by reacting a hydroxyl compound with a carbamyl chloride essentially free from phosgene and hydrogen chloride at a temperature of from 60.degree. to 130.degree. C in alkyl or halogen benzenes as solvent.
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公开(公告)号：US4235814A
公开(公告)日：1980-11-25
申请号：US921312
申请日：1978-07-03
IPC分类号： C07C125/03
摘要： .alpha.-haloalkylcarbamyl halides are manufactured by reacting N-tert.-alkyl-N-1-alkenyl-carbamyl halides with a hydrogen halide at from -78.degree. C. to +80.degree. C.The .alpha.-haloalkylcarbamyl halides, e.g. .alpha.-chloroalkylcarbamyl chlorides, especially .alpha.-chloroethylcarbamyl chloride, prepared by the process of the invention, are valuable starting materials for the manufacture of surface-coating raw materials, textile coatings, dyes, drugs and crop protection agents.
摘要翻译： α-卤代烷基氨基甲酰卤通过N-叔烷基-N 1 - 烯基 - 氨基甲酰基卤化物与卤化氢在-78℃至+ 80℃下反应来制备。 通过本发明的方法制备的α-氯代烷基氨基甲酰氯，特别是α-氯乙基氨基甲酰氯，是用于制造表面包衣原料，纺织品涂料，染料，药物和作物保护剂的有价值的原料。
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公开(公告)号：US4137261A
公开(公告)日：1979-01-30
申请号：US754598
申请日：1976-12-27
IPC分类号： C07C271/04 , C07C20060101 , C07C67/00 , C07C239/00 , C07C125/03
CPC分类号： C07C51/60
摘要： N-Vinyl-N-alkyl-carbamic acid chlorides are manufactured by reacting crude Schiff bases, which have advantageously been manufactured in the presence of pentane, with phosgene and tertiary amines, treating the reaction mixture with water and then isolating the end product, after having separated off the aqueous phase containing the amine salt. The products are starting materials for the manufacture of surface-coating intermediates, plastics, paints and crop protection agents.
摘要翻译： N-乙烯基-N-烷基 - 氨基甲酸氯化物是通过将有利地在戊烷存在下制备的粗制希夫碱与光气和叔胺反应制备的，然后用水处理反应混合物，然后分离最终产物 已经分离出含有胺盐的水相。 该产品是用于制造表面涂层中间体，塑料，油漆和作物保护剂的起始原料。
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公开(公告)号：US3935201A
公开(公告)日：1976-01-27
申请号：US522630
申请日：1974-11-11
IPC分类号： C07D285/14 , C07D285/16
CPC分类号： C07D285/16
摘要： 2,1,3-Benzothiadiazin-4-one-2,2-dioxides are produced by the reaction of esters of anthranilic acid with a sulfamic acid halide in the presence of a solvent and a base at a temperature of from 20.degree. to 100.degree.C. The products are starting materials for the production of dyes and plant protection agents.
摘要翻译： 2,1,3-苯并噻二嗪-4-酮-2,2-二氧化物是通过在溶剂和碱的存在下，在20〜100℃的温度下，邻氨基苯甲酸的酯与氨基磺酰卤反应制备的 DEG。该产品是用于生产染料和植物保护剂的起始原料。
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