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    Production of isocyanate compounds
    4.
    发明授权
    Production of isocyanate compounds 失效
    异氰酸酯化合物的生产

    公开(公告)号：US4925982A

    公开(公告)日：1990-05-15

    申请号：US220887

    申请日：1988-06-16

    申请人： Satoshi Urano ,  Ryuzo Mizuguchi

    发明人： Satoshi Urano ,  Ryuzo Mizuguchi

    IPC分类号： C07C263/10 ,  C07C263/12 ,  C07C265/04 ,  C07C265/06

    CPC分类号： C07C263/10 ,  C07C263/18

    摘要： Production of an alkenoyl isocyanate of the formula: ##STR1## wherein R is a hydrogen atom or a lower alkyl group by reacting an acrylamide of the formula: ##STR2## wherein R is as defined above with an oxalyl halide of the formula(COX).sub.2wherein X is a halogen atom to give a reaction mixture comprising a haloalkanoyl isocyanate of the formula: ##STR3## wherein R and X are each as defined above with or without the alkenoyl isocyanate, recovering the haloalkanoyl isocyanate and, when present, the alkenoyl isocyanate separately from the reaction mixture and reacting the recovered haloalkanoyl isocyanate with a hydrogen halide-eliminating agent to give the alkenoyl isocyanate.

    摘要翻译： 制备下式的烯酰基异氰酸酯：其中R是氢原子或低级烷基，通过下式的丙烯酰胺与式（COX）的草酰卤反应，其中R如上定义， 2其中X是卤素原子，得到包含下式的卤代烷酰基异氰酸酯的反应混合物：其中R和X各自如上所定义或不与链烯酰基异氰酸酯反应，回收卤代烷酰基异氰酸酯，当存在烯酰基 异氰酸酯与反应混合物分开并使回收的卤代烷酰基异氰酸酯与卤化氢消除剂反应，得到烯酰基异氰酸酯。

    Process for preparation of ethylenically unsaturated isocyanates
    7.
    发明授权
    Process for preparation of ethylenically unsaturated isocyanates 失效
    制备烯属不饱和异氰酸酯的方法

    公开(公告)号：US5990345A

    公开(公告)日：1999-11-23

    申请号：US982654

    申请日：1997-12-02

    申请人： Dieter Lohmann ,  Rudolf Duthaler

    发明人： Dieter Lohmann ,  Rudolf Duthaler

    IPC分类号： C07C263/00 ,  C07C263/04 ,  C07C265/04 ,  C07C265/06 ,  C08F12/22 ,  C08F12/26 ,  C08F20/10 ,  C08F20/36 ,  C08G18/81

    CPC分类号： C07C263/04

    摘要： A process for the preparation of ethylenically unsaturated isocyanates is described, which process comprises silylating an appropriate ethylenically unsaturated urethane precursor at the urethane nitrogen and converting the resulting unsaturated N-silyl-urethane by means of thermolysis at elevated temperature into the desired isocyanate. The unsaturated isocyanates obtainable according to the process are suitable, for example, as monomers or comonomers in the preparation of polymerisates or copolymerisates.

    摘要翻译： 描述了制备烯属不饱和异氰酸酯的方法，该方法包括在氨基甲酸乙酯氮上甲酰化适当的烯属不饱和氨基甲酸酯前体，并通过在升高的温度下热解将所得的不饱和N-甲硅烷基 - 氨基甲酸酯转化成所需的异氰酸酯。 根据该方法可获得的不饱和异氰酸酯在制备聚合物或共聚物时适用于例如单体或共聚单体。

    Trans-beta-isocyanatoacrylate esters, their preparation, and polymers made therefrom
    8.
    发明授权
    Trans-beta-isocyanatoacrylate esters, their preparation, and polymers made therefrom 失效
    反式-β-异氰酸根合丙烯酸酯，其制备方法和由其制备的聚合物

    公开(公告)号：US5347044A

    公开(公告)日：1994-09-13

    申请号：US864236

    申请日：1992-04-06

    申请人： Thomas J. Byerley ,  Cecil C. Chappelow ,  J. David Eick

    发明人： Thomas J. Byerley ,  Cecil C. Chappelow ,  J. David Eick

    IPC分类号： C07C265/06 ,  C08F22/32 ,  C07C265/08

    CPC分类号： C07C265/06 ,  C08F22/32 ,  C07C2101/14

    摘要： Novel trans-beta-isocyanatoacrylate esters, their preparation and use in forming novel polymeric compositions, including polymers useful as adhesives, are disclosed. The trans-beta-isocyanatoacrylate esters have the formula: ##STR1## wherein R is C.sub.1 -C.sub.18 linear or branched alkyls; C.sub.5 -C.sub.6 cycloalkyl; aryl; alkaryl; aralkyl; C.sub.1 -C.sub.18 halogenated alkyl; halogenated aryl; C.sub.1 -C.sub.8 alkoxyalkyl; or alkoxyaryl.

    摘要翻译： 新型反式-β-异氰酸酯丙酯酯，其制备和用于形成新型聚合物组合物，包括可用作粘合剂的聚合物。 反式-β-异氰酸根合丙烯酸酯具有下式：其中R是C1-C18直链或支链烷基; C5-C6环烷基; 芳基; 烷芳基 芳烷基 C1-C18卤代烷基; 卤代芳基; C1-C8烷氧基烷基; 或烷氧基芳基。