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    Polymer comprising fluoroalkyl group, a method of preparation thereof, a surface active agent, a surface treatment agent and a coating composition
    1.
    发明授权
    Polymer comprising fluoroalkyl group, a method of preparation thereof, a surface active agent, a surface treatment agent and a coating composition 失效
    包含氟烷基的聚合物，其制备方法，表面活性剂，表面处理剂和涂料组合物

    公开(公告)号：US5414065A

    公开(公告)日：1995-05-09

    申请号：US262981

    申请日：1994-06-21

    申请人： Hideo Sawada ,  Keiji Komoto ,  Masahiro Sano ,  Yutaka Enokida ,  Mitani Motohiro ,  Takeo Matsumoto ,  Masaharu Nakayama ,  Masato Okajima

    发明人： Hideo Sawada ,  Keiji Komoto ,  Masahiro Sano ,  Yutaka Enokida ,  Mitani Motohiro ,  Takeo Matsumoto ,  Masaharu Nakayama ,  Masato Okajima

    IPC分类号： C08F4/32 ,  C08F4/34 ,  C08F30/08

    CPC分类号： C08F4/34

    摘要： A polymer comprising fluoroalkyl group has a structure in which one or two parts of the fluoroalkyl group at the one or both ends of the molecule are linked to a part of alkylene groups or alkylene groups substituted with halogen, a part of alkylene group substituted with functional groups, such as halogen, cyano group, alkylsulfonic acid group, amidoalkylsulfonic acid group, carboxylic acid group, carboxyl group, oxycarbonyl group, ether group, epoxy group and the like, and/or a part of silicone group. A method of preparation of the polymer comprising fluoroalkyl group contains reaction of a fluoroalkanoyl peroxide with a monomer comprising the functional group or a monomer comprising silicone group. A surface active agent comprises fluoroalkyl group and caroxylic acid salt group. A surface treatment agent comprises the polymer comprising fluoroalkyl group, hydrolysis products thereof, hydrolytic condensation products thereof, and mixtures thereof. A coating composition comprises the polymer comprising fluoroalkyl group. The polymer comprising fluoroalkyl group has excellent water repellency, oil repellency and weatherability because the fluoroalkyl group is introduced into the molecule through carbon-carbon linkage.

    摘要翻译： 包含氟烷基的聚合物具有这样的结构，其中分子的一个或两个末端的一个或两个部分的氟烷基与一部分被卤素取代的亚烷基或亚烷基连接，一部分被官能 卤素，氰基，烷基磺酸基，酰氨基烷基磺酸基，羧酸基，羧基，氧羰基，醚基，环氧基等的基团和/或硅氧烷基的一部分。 包含氟烷基的聚合物的制备方法包括氟代烷酰基过氧化物与包含官能团的单体或包含硅氧烷基团的单体的反应。 表面活性剂包括氟代烷基和羧酸盐基团。 表面处理剂包括含氟烷基的聚合物，其水解产物，其水解缩合产物及其混合物。 涂料组合物包含含氟烷基的聚合物。 包含氟烷基的聚合物由于通过碳 - 碳键将氟代烷基引入到分子中，具有优异的拒水性，拒油性和耐候性。

    Polymer comprising fluoroalkl group, a method of preparation thereof, a surface active agent, a surface treatment agent and a coating composition
    2.
    发明授权
    Polymer comprising fluoroalkl group, a method of preparation thereof, a surface active agent, a surface treatment agent and a coating composition 失效
    包含氟烷基的聚合物，其制备方法，表面活性剂，表面处理剂和涂料组合物

    公开(公告)号：US5324803A

    公开(公告)日：1994-06-28

    申请号：US959372

    申请日：1992-10-13

    申请人： Hideo Sawada ,  Keiji Komoto ,  Masahiro Sano ,  Yutaka Enokida ,  Motohiro Mitani ,  Takeo Matsumoto ,  Masaharu Nakayama ,  Masato Okajima

    发明人： Hideo Sawada ,  Keiji Komoto ,  Masahiro Sano ,  Yutaka Enokida ,  Motohiro Mitani ,  Takeo Matsumoto ,  Masaharu Nakayama ,  Masato Okajima

    IPC分类号： C08F4/32 ,  C08F4/34 ,  C08F30/08

    CPC分类号： C08F4/34

    摘要： A polymer comprising fluoroalkyl group has a structure in which one or two parts of the fluoroalkyl group at the one or both ends of the molecule are linked to a part of alkylene groups or alkylene groups substituted with halogen, a part of alkylene group substituted with functional groups, such as halogen, cyano group, alkylsulfonic acid group, amidoalkylsulfonic acid group, carboxylic acid group, carboxyl group, oxycarbonyl group, ether group, epoxy group and the like, and/or a part of silicone group. A method of preparation of the polymer comprising fluoroalkyl group contains reaction of a fluoroalkanoyl peroxide with a monomer comprising the functional group or a monomer comprising silicone group. A surface active agent comprises fluoroalkyl group and caroxylic acid salt group. A surface treatment agent comprises the polymer comprising fluoroalkyl group, hydrolysis products thereof, hydrolytic condensation products thereof, and mixtures thereof. A coating composition comprises the polymer comprising fluoroalkyl group. The polymer comprising fluoroalkyl group has excellent water repellency, oil repellency and weatherability because the fluoroalkyl group is introduced into the molecule through carbon-carbon linkage.

    摘要翻译： 包含氟烷基的聚合物具有这样的结构，其中分子的一端或两端的一个或两个氟代烷基部分与一部分被卤素取代的亚烷基或亚烷基连接，一部分被官能团取代的亚烷基 卤素，氰基，烷基磺酸基，酰氨基烷基磺酸基，羧酸基，羧基，氧羰基，醚基，环氧基等的基团和/或硅氧烷基的一部分。 包含氟烷基的聚合物的制备方法包括氟代烷酰基过氧化物与包含官能团的单体或包含硅氧烷基团的单体的反应。 表面活性剂包括氟代烷基和羧酸盐基团。 表面处理剂包括含氟烷基的聚合物，其水解产物，其水解缩合产物及其混合物。 涂料组合物包含含氟烷基的聚合物。 包含氟烷基的聚合物由于通过碳 - 碳键将氟代烷基引入到分子中，具有优异的拒水性，拒油性和耐候性。

    Fluoroalkyl group-containing organosilicon oligomer, method for preparing same and surface treating agent
    3.
    发明授权
    Fluoroalkyl group-containing organosilicon oligomer, method for preparing same and surface treating agent 失效
    含氟烷基的有机硅低聚物，其制备方法和表面处理剂

    公开(公告)号：US5338877A

    公开(公告)日：1994-08-16

    申请号：US111183

    申请日：1993-08-24

    申请人： Hideo Sawada ,  Motohiro Mitani ,  Masaharu Nakayama ,  Takeo Matsumoto

    发明人： Hideo Sawada ,  Motohiro Mitani ,  Masaharu Nakayama ,  Takeo Matsumoto

    IPC分类号： C07F7/08 ,  C07F7/18

    CPC分类号： C07F7/0818 ,  C07F7/0852 ,  C07F7/0858 ,  C07F7/182 ,  C07F7/1832 ,  C07F7/1836 ,  C07F7/1896

    摘要： A fluoroalkyl group-containing organosilicon oligomer is represented by the following formula (I) or (IV) of: ##STR1## wherein R, R.sub.1, R.sub.2, X and Y each are the same or different groups and stand for an alkyl, alkoxy or alkylcarbonyloxy group having 1 to 10 carbon atoms, n represents an integer of 1 to 3, m.sub.1 and m.sub.3 represent an integer of 1 to 10, m.sub.2 represents an integer of 0 to 10, m.sub.4 represents an integer of 1 to 5 and R.sub.F represents ##STR2## where A stands for a hydrogen atom, a fluorine atom or a chlorine atom, n.sub.1 represents an integer of 1 to 10 and n.sub.2 represents an integer of 0 to 8. A surface treating agent contains the oligomer defined by the formula (I) or (IV).

    摘要翻译： 含氟烷基的有机硅低聚物由下式（I）或（IV）表示：其中R，R 1，R 2，X和Y各自相同或不同， 并且代表具有1-10个碳原子的烷基，烷氧基或烷基羰基氧基，n表示1至3的整数，m1和m3表示1至10的整数，m2表示0至10的整数，m4表示 1〜5的整数，RF表示，其中A表示氢原子，氟原子或氯原子，n1表示1〜10的整数，n2表示0〜8的整数。表面处理剂含有 由式（I）或（IV）定义的低聚物。

    Fluoralykyl group-containing organosilicon oligomer, method for preparing same and surface treating agent
    4.
    发明授权
    Fluoralykyl group-containing organosilicon oligomer, method for preparing same and surface treating agent 失效
    含氟烷基的有机硅低聚物，其制备方法和表面处理剂

    公开(公告)号：US5288891A

    公开(公告)日：1994-02-22

    申请号：US791989

    申请日：1991-11-14

    申请人： Hideo Sawada ,  Motohiro Mitani ,  Masaharu Nakayama ,  Takeo Matsumoto

    发明人： Hideo Sawada ,  Motohiro Mitani ,  Masaharu Nakayama ,  Takeo Matsumoto

    IPC分类号： C07F7/08 ,  C07F7/18

    CPC分类号： C07F7/0818 ,  C07F7/0852 ,  C07F7/0858 ,  C07F7/182 ,  C07F7/1832 ,  C07F7/1836 ,  C07F7/1896

    摘要： A fluoroalkyl group-containing organosilicon oligomer is represented by the following formula (I) or (IV) of: ##STR1## wherein R, R.sub.1, R.sub.2, X and Y each are the same or different groups and stand for an alkyl, alkoxy or alkylcarbonyloxy group having 1 to 10 carbon atoms, n represents an integer of 1 to 3, m.sub.1 and m.sub.3 represent an integer of 1 to 10, m.sub.2 represents an integer of 0 to 10, m.sub.4 represents an integer of 1 to 5 and R.sub.F represents --CF.sub.2).sub.n.sbsb.1 A or ##STR2## where A stands for a hydrogen atom, a fluorine atom or a chlorine atom, n.sub.1 represents an integer of 1 to 10 and n.sub.2 represents an integer of 0 to 8. A surface treating agent contains the oligomer defined by the formula (I) or (IV).

    摘要翻译： 含氟烷基的有机硅低聚物由下式（I）或（IV）表示：（*化学结构*）（I）（*化学结构*）（Ⅳ）其中R，R1，R2，X和Y 各自为相同或不同的基团，代表具有1-10个碳原子的烷基，烷氧基或烷基羰基氧基，n表示1至3的整数，m1和m3表示1至10的整数，m2表示0的整数 10，m4表示1〜5的整数，RF表示-CF 2）n1A或（*化学结构*）其中A表示氢原子，氟原子或氯原子，n1表示1〜10的整数， n2表示0〜8的整数。表面处理剂含有式（I）或（IV）所定义的低聚物。

    Fluoroalkyl derivative and process for preparing the same
    5.
    发明授权
    Fluoroalkyl derivative and process for preparing the same 失效
    氟代醇衍生物及其制备方法

    公开(公告)号：US5118879A

    公开(公告)日：1992-06-02

    申请号：US601736

    申请日：1990-10-25

    申请人： Nobumasa Kamigata ,  Masato Yoshida ,  Hideo Sawada ,  Masaharu Nakayama

    发明人： Nobumasa Kamigata ,  Masato Yoshida ,  Hideo Sawada ,  Masaharu Nakayama

    IPC分类号： C07C19/10 ,  C07C21/18 ,  C07C22/08 ,  C07C25/13 ,  C07C25/24 ,  C07C43/225 ,  C07C205/11

    CPC分类号： C07C25/24 ,  C07C19/10 ,  C07C205/11 ,  C07C21/18 ,  C07C22/08 ,  C07C25/13 ,  C07C43/225

    摘要： Fluoroalkyl derivatives which are novel compounds represented by the following general formula (I) or (II) of: ##STR1## orR.sub.1 --CH.dbd.CR.sub.2 (CF.sub.2).sub.n F (II)(wherein R.sub.1 stands for ##STR2## (where X stands for a hydrogen atom, a chlorine atom, a bromine atom, a fluorine atom, an iodine atom, a methyl group, an ethyl group, a methoxy group, an ethoxy group or a nitro group), an aroyloxy group, or an alkyl or alkoxycarbonyl group having 1 to 20 carbon atoms, and R.sub.2 stands for a hydrogen atom or a methyl group; and n stands for an integer of from 1 to 20.) A process for the preparation of the derivative is a process comprising reacting an olefin compound and a fluoroalkanesulfonyl chloride in the presence of a metal catalyst, or a process comprising an additional alkali treatment step which follows the aforementioned process.

    摘要翻译： PCT No.PCT / JP90 / 00242 Sec。 371 1990年10月25日第 102（e）1990年10月25日日期PCT提交1990年2月27日PCT公布。 出版物WO90 / 09972 1990年9月7日，由以下通式（I）或（II）表示的新化合物：（I）或R1-CH = CR2（CF2）nF（Ⅱ）（其中R1 代表（其中X代表氢原子，氯原子，溴原子，氟原子，碘原子，甲基，乙基，甲氧基，乙氧基或硝基） 芳氧基，碳原子数1〜20的烷基或烷氧基羰基，R2表示氢原子或甲基，n表示1〜20的整数）。 衍生物是一种方法，包括在金属催化剂存在下使烯烃化合物和氟烷基磺酰氯反应，或包括依照上述方法的另外的碱处理步骤的方法。

    Hetero-aromatic polymer containing fluoroalkyl group
    7.
    发明授权
    Hetero-aromatic polymer containing fluoroalkyl group 失效
    含氟烷基的异芳族聚合物

    公开(公告)号：US5247062A

    公开(公告)日：1993-09-21

    申请号：US884852

    申请日：1992-05-13

    申请人： Hideo Sawada ,  Masaharu Nakayama

    发明人： Hideo Sawada ,  Masaharu Nakayama

    IPC分类号： C08G61/12 ,  H01B1/12

    CPC分类号： H01B1/127 ,  C08G61/123

    摘要： A hetero-aromatic polymer containing a fluoroalkyl group is a novel polymer and has a polymerization degree of 5 to 5000, the polymer including the following structural unit represented by the general formula (I) of: ##STR1## (wherein R stands for a hydrogen atom or an alkyl group having 1 to 25 carbon atoms, X stands for a sulfur atom, an imino or an oxygen atom, and n is an integer of from 1 to 9.)

    摘要翻译： 含有氟代烷基的杂芳族聚合物是新型聚合物，聚合度为5〜5000，该聚合物包含以下通式（I）表示的结构单元：其中R表示 对于氢原子或碳原子数1〜25的烷基，X表示硫原子，亚氨基或氧原子，n表示1〜9的整数。

    Process for preparing a non-aqueous liquid dispersion of polymer made with a polymeric peroxide
    10.
    发明授权
    Process for preparing a non-aqueous liquid dispersion of polymer made with a polymeric peroxide 失效
    制备由聚合物过氧化物制成的聚合物的非水性液体分散体的方法

    公开(公告)号：US4659769A

    公开(公告)日：1987-04-21

    申请号：US465074

    申请日：1983-02-09

    申请人： Hiroshi Ohmura ,  Masaharu Nakayama

    发明人： Hiroshi Ohmura ,  Masaharu Nakayama

    IPC分类号： C08F2/08 ,  C08F2/14 ,  C08F4/36 ,  C08F4/38 ,  C08F293/00 ,  C08F299/00

    CPC分类号： C08F4/36 ,  C08F293/00

    摘要： A specialized polymeric peroxide is copolymerized with vinyl type monomers in the presence of organic liquid, thereby obtaining a solution of a copolymer having peroxy bonds therein.This solution is admixed with vinyl type monomers which are different in composition from the ones used in the first copolymerization, and the resultant mixture is subjected to block copolymerization.The obtained block copolymer solution is admixed with an organic liquid which exert solubility to one of polymers of the vinyl type monomers which are employed in the first or second copolymerization, whereby a non aqueous system liquid dispersion is obtained.This dispersion contains a block copolymer in a high concentration and it also is splendid in uniformity of dispersion and dispersion stability.

    摘要翻译： 在有机液体存在下，将特殊的聚合过氧化物与乙烯基类单体共聚，从而得到其中具有过氧键的共聚物的溶液。 将该溶液与在第一共聚合中使用的组合物不同的乙烯基类单体混合，将所得混合物进行嵌段共聚。 将获得的嵌段共聚物溶液与在第一次或第二次共聚中使用的乙烯基型单体的聚合物之一中溶解度的有机液体混合，从而得到非水系统液体分散体。 该分散体含有高浓度的嵌段共聚物，并且还具有分散稳定性和分散稳定性的均匀性。