High-purity cycloaliphatic diepoxy compound and preparation process thereof
    1.
    发明授权
    High-purity cycloaliphatic diepoxy compound and preparation process thereof 失效
    高纯度脂环族二环氧化合物及其制备方法

    公开(公告)号:US07732627B2

    公开(公告)日:2010-06-08

    申请号:US11792782

    申请日:2005-12-27

    IPC分类号: C07D301/14

    CPC分类号: C07D303/04

    摘要: A high-purity cycloaliphatic diepoxy compound of General Formula (II) is an epoxidized product of a cycloaliphatic diolefinic compound of General Formula (I) having an isomer content as detected in gas chromatography (GC) of 15% or less: wherein X represents a bivalent group selected from the group consisting of, for example, O, S, —SO—, —SO2—, —CH2—, and —C(CH3)2—; and R1 to R18 may be the same as or different from each other and each represent hydrogen atom, a halogen atom, a hydrocarbon group which may contain oxygen atom or a halogen atom, or an alkoxy group which may be substituted. Such a high-purity cycloaliphatic diepoxy compound is prepared by producing the cycloaliphatic diolefinic compound through distillation, epoxidizing the compound with an aliphatic percarboxylic acid containing substantially no water, carrying out desolvation, and further purifying the epoxidized compound through distillation.

    摘要翻译: 通式(II)的高纯度脂环族二环氧化合物是通式(I)的脂环族二烯烃化合物的环氧化产物,其具有在气相色谱(GC)中检测到的异构体含量为15%以下:其中X表示 选自例如O,S,-SO-,-SO 2 - , - CH 2 - 和-C(CH 3)2 - 的二价基团; R 1〜R 18可以相同也可以不同,表示氢原子,卤原子,可以含有氧原子或卤素原子的烃基或可以被取代的烷氧基。 这样的高纯度脂环族二环氧化合物是通过蒸馏生产环脂族二烯化合物,通过用基本上不含水的脂肪族过羧酸进行脱氧,进行去溶剂化,并通过蒸馏进一步纯化环氧化合物来制备的。

    High-Purity Cycloaliphatic Diepoxy Compound and Preparation Process Thereof
    2.
    发明申请
    High-Purity Cycloaliphatic Diepoxy Compound and Preparation Process Thereof 失效
    高纯度环脂肪族二环氧化合物及其制备方法

    公开(公告)号:US20080045729A1

    公开(公告)日:2008-02-21

    申请号:US11792782

    申请日:2005-12-27

    IPC分类号: C07D303/04 C07D301/14

    CPC分类号: C07D303/04

    摘要: A high-purity cycloaliphatic diepoxy compound of General Formula (II) is an epoxidized product of a cycloaliphatic diolefinic compound of General Formula (I) having an isomer content as detected in gas chromatography (GC) of 15% or less: wherein X represents a bivalent group selected from the group consisting of, for example, O, S, —SO—, —SO2—, —CH2—, and —C(CH3)2—; and R1 to R18 may be the same as or different from each other and each represent hydrogen atom, a halogen atom, a hydrocarbon group which may contain oxygen atom or a halogen atom, or an alkoxy group which may be substituted. Such a high-purity cycloaliphatic diepoxy compound is prepared by producing the cycloaliphatic diolefinic compound through distillation, epoxidizing the compound with an aliphatic percarboxylic acid containing substantially no water, carrying out desolvation, and further purifying the epoxidized compound through distillation.

    摘要翻译: 通式(II)的高纯度脂环族二环氧化合物是通式(I)的脂环族二烯烃化合物的环氧化产物,其具有在气相色谱(GC)中检测到的异构体含量为15%以下:其中X表示 选自例如O,S,-SO-,-SO 2 - , - CH 2 - 和-C(CH 3) 2→3 R 1〜R 18可以相同或不同,表示氢原子,卤素原子,可含有氧原子的烃基或 卤素原子或可被取代的烷氧基。 这样的高纯度脂环族二环氧化合物是通过蒸馏生产环脂族二烯化合物,通过用基本上不含水的脂肪族过羧酸进行脱氧,进行去溶剂化,并通过蒸馏进一步纯化环氧化合物来制备的。

    Curable resin composition, a method for the preparation thereof, and a coated article thereof
    3.
    发明授权
    Curable resin composition, a method for the preparation thereof, and a coated article thereof 失效
    可固化树脂组合物,其制备方法及其涂布制品

    公开(公告)号:US06924008B2

    公开(公告)日:2005-08-02

    申请号:US09913405

    申请日:2000-12-15

    摘要: There are provided a curable resin composition composed of an epoxy compound having an ionic polymerizability and viscosity of not more than 1,000 cP at 25° C., an acrylic resin having an ionic polymerizable functional group, and a thermally-activating ionic polymerization catalyst which can be dissolved by heating and crystallized by cooling, a method for the preparation thereof, and a coated article using the curable resin composition.The curable resin composition is excellent in storage stability, and a cured coating layer therefrom is excellent in heat resistance, staining resistance, removability of staining substances, or scratch resistance, and an electrical insulating property, and in which dependence of volume resistivity upon temperatures is small, and from which an excellent coated article is obtained, and it is widely utilized in industry.

    摘要翻译: 提供了一种固化树脂组合物,其由在25℃下具有不超过1,000cP的离子聚合性和粘度不超过1,000cP的环氧化合物,具有离子可聚合官能团的丙烯酸树脂和可热固化的离子聚合催化剂组成 通过加热溶解并通过冷却结晶,其制备方法和使用该固化性树脂组合物的涂布制品。 固化性树脂组合物的保存稳定性优异,其固化涂层的耐热性,耐污染性,染色物质的可除去性,耐划伤性,电绝缘性优异,体积电阻率对温度的依赖性为 小,从中获得优良的涂层制品,并被广泛应用于工业。

    Alicyclic diepoxy compound, epoxy resin composition comprising the same, and cured article therefrom
    4.
    发明授权
    Alicyclic diepoxy compound, epoxy resin composition comprising the same, and cured article therefrom 有权
    脂环式二环氧化合物,包含该环氧化合物的环氧树脂组合物及其固化物

    公开(公告)号:US07989523B2

    公开(公告)日:2011-08-02

    申请号:US12305906

    申请日:2007-06-29

    摘要: Disclosed is an alicyclic diepoxy compound which gives a cured article suffering from no deterioration in properties even when used in hot and humid surroundings or used under such conditions as to give a strong acid, which is highly reactive upon curing, and which gives a cured article superior typically in thermal stability. Specifically, the alicyclic diepoxy compound includes a 3,4,3′,4′-diepoxybicyclohexyl compound represented by following Formula (1): wherein R1 to R18 each represent a hydrogen atom, a halogen atom, a hydrocarbon group which may have an oxygen atom or a halogen atom, or a substituted or unsubstituted alkoxy group, in which the alicyclic diepoxy compound contains isomers of the 3,4,3′,4′-diepoxybicyclohexyl compound in a content of less than 20% based on the total of the 3,4,3′,4′-diepoxybicyclohexyl compound and the isomers thereof in terms of peak area ratio as determined by gas chromatography.

    摘要翻译: 公开了一种脂环式二环氧化合物,即使在热湿环境下使用也不会劣化的固化物,或者在固化时具有高反应性的强酸的条件下使用,得到固化物 优良的热稳定性。 具体地,脂环族二环氧化合物包括由下式(1)表示的3,4,3',4'-二环氧双环己基化合物:其中R 1至R 18各自表示氢原子,卤素原子,可具有氧的烃基 原子或卤素原子或取代或未取代的烷氧基,其中脂环式二环氧化合物含有3,4,3',4'-二环氧基双环己基化合物的异构体,其含量小于20% 3,4,3',4'-二环氧双环己基化合物及其异构体,以气相色谱法测定的峰面积比。

    Electrophotographic photosensitive member, process cartridge including
same and electrophotographic apparatus
    6.
    发明授权
    Electrophotographic photosensitive member, process cartridge including same and electrophotographic apparatus 失效
    电子照相感光构件,包括其的处理盒和电子照相设备

    公开(公告)号:US5543257A

    公开(公告)日:1996-08-06

    申请号:US345707

    申请日:1994-11-22

    IPC分类号: G03G5/06

    CPC分类号: G03G5/0681

    摘要: An electrophotographic photosensitive member is constituted by an electroconductive support and a photosensitive layer disposed on the electroconductive support. The photosensitive layer contains a specific disazo pigment having a 2,2'-bis-1,3-benzdithiolene-diyl skeleton or a thiophene-diyl skeleton. The photosensitive member is effective for providing a process cartridge and an electrophotographic apparatus respectively including the photosensitive member with an excellent photosensitivity and a stable electric potential in repetitive use.

    摘要翻译: 电子照相感光构件由导电载体和设置在导电载体上的感光层构成。 感光层含有具有2,2'-双-1,3-苯并二硫戊烯 - 二基骨架或噻吩 - 二基骨架的特定双偶氮颜料。 感光构件有效地提供分别包括感光构件的处理盒和电子照相装置,其具有优异的光敏性和重复使用的稳定的电位。

    Electrophotographic photosensitive member and electrophotographic
apparatus, device unit and facsimile machine using the same
    7.
    发明授权
    Electrophotographic photosensitive member and electrophotographic apparatus, device unit and facsimile machine using the same 失效
    电子照相感光构件和电子照相设备,设备单元和使用其的传真机

    公开(公告)号:US5466550A

    公开(公告)日:1995-11-14

    申请号:US329381

    申请日:1994-10-25

    IPC分类号: G03G5/05 C08G5/14

    CPC分类号: G03G5/0542

    摘要: An electrophotographic photosensitive member has a conductive support, and a charge generating layer and a charge transporting layer. The charge generating layer contains an acetal resin obtained from a reaction of polyvinyl alcohol, alkyl aldehyde having a structure shown in Formula (1) below, and aryl aldehyde having a structure shown in Formula (2) below:R--CHO (1)wherein R is a substituted or unsubstituted, chain or cyclic alkyl group, andAr--CHO (2)wherein Ar is a substituted or unsubstituted aryl group. The electrophotographic photosensitive member is used in electrophotographic apparatus, device units and facsimile machines, while ensuring superior electrophotographic characteristics and an excellent image free from fog.

    摘要翻译: 电子照相感光构件具有导电性支持体,电荷产生层和电荷输送层。 电荷产生层含有通过聚乙烯醇,具有下述通式(1)所示结构的烷基醛与下式(2)所示结构的芳基醛的反应获得的缩醛树脂:R-CHO(1)其中 R是取代或未取代的链或环状烷基,Ar-CHO(2)其中Ar是取代或未取代的芳基。 电子照相感光构件用于电子照相设备,设备单元和传真机,同时确保优异的电子照相特性和优异的图像无雾。